查询词典 methylene azure

The profession technique means that handicraft product produce the azure stone to model the craft and have the metal alloy die-casting, the resin models, the low temperature metal alloy model, washes to press etc. Numerous productions means, among them even own the most large- scale azure stone of domestic raw material produce, the azure stone craft gift takes off the foundry art article production base.

工艺品生产的专业技术手段有琉璃成型工艺、有合金压铸、树脂成型、低温合金成型、冲压等众多的生产手段，其中更拥有国内最大规模琉璃原料生产、琉璃工艺礼品脱蜡铸造艺术品生产基地。

In our research on study chemical reaction of active methylene compounds and brom-acetophenone. Because of brom-acetophenone is compound that contain carbonyl and halogen ,which will take place electrophilic substitution and nucleophilic addition. When active methylene compounds are ethyl acetoacetate and β-diketone, controlling reaction condition, we have found that mono-substitution's production and di-substitution's. production is isolated; active methylene compounds are acetoacetanilide and acetoacetanilide derivate, pyrrolidin-2-one derivants were obtained by substitution and close-ring reaction .but there is no report about it.

本文是让活泼亚甲基类化合物与溴代苯乙酮发生化学反应，由于溴代苯乙酮是含有羰基的卤代烃结构，它可以发生亲电取代和亲核加成反应，当活泼亚甲基类化合物为乙酰乙酸乙酯和β-二酮时，控制反应条件可以发生单取代和双取代两种产物；当活泼亚甲基类化合物为乙酰乙酰芳胺类化合物来反应时，溴代苯乙酮中的羰基与氨基会发生分子内的关环反应生成吡咯烷-2-酮衍生物，这在以前的研究中是没有发现的。

Composition of suspension will chang from titanium monoxide to titanium dioxide during standstill procedure. Experimental results show that the proposed method can successfully prepare the anatase phase of titanium dioxide .In the photocatalysis experiment, the prepared titanium dioxide nanofluid absorbs the Ultraviolet when light wavelength was 360 to 380 nm. Adsorption experimental results show that the efficiency of absorbing methylene blue using TiO2 is higher than that for TiO2 (Degussa P-25) or ZnO. Depigmentation of methylene blue experimental using TiO2 can depigmentize methylene blue reach 100% in 60 min.

悬浮液所含之奈米颗粒在静置过程中，成份方面会由似一氧化钛转变为二氧化钛；在结晶组成方面，所制备之二氧化钛颗粒之结晶组成为锐钛矿结构；在光催化方面，所制备之奈米二氧化钛悬浮液在光波长360nm~380nm时产生吸收紫外光现象，在吸附实验中本制程所制备的二氧化钛颗粒的吸附效果优於商用的二氧化钛及氧化锌，在亚甲基蓝的脱色实验中本制程所制备的二氧化钛颗粒能在60分钟内达到脱色率100%。

First, a chlorinator was self-designed in this paper, and dichloride of 2-methyl-1-propene was synthesized by 2-methyl-1-propene reacted with chlorine fast in this reactor. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the yield and selectivity of dichloride of 2-methyl-1-prop-ene were more than 65% and 80% respectively. Second, the preparation of 2-methylene-1, 3-propanediol, which dichloride of 2-methyl-1-propene reacted with alkali was investigated. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the conversion of dichloride of 2-methyl-1-propene was 100%. Moreover the preparation of MPO, which 2-methylene-1, 3-propanediol reacted with hydrogen, in presence of Al_2O_3-Pd catalyst, was gotten, and the product was appraised.

本文在氯化反应过程中，自行设计制作出了氯化管式反应器，在该反应器中异丁烯和氯气迅速混合反应生成二氯异丁烯，根据该氯化反应特征利用正交试验和单因素试验考察了有关因素的影响并优化得到了最佳工艺条件，二氯异丁烯的总收率达65％以上，选择性达80％；接着，对二氯异丁烯进行水解反应制得了2-甲烯-1，3-丙二醇，讨论了相关因素对水解反应的影响，并通过正交试验和单因素试验得到了较佳工艺条件，二氯异丁烯的转化率达100％；同时还对制备的2-甲烯-1，3-丙二醇在常压下采用三氧化二铝负载钯催化剂催化加氢得目的产物MPO，并对产品进行了鉴定，从而打通了整个工艺路线。

In the part two, we reported the classical Knoevenagel condensation between aromatic aldehydes and acyclic active methylene compounds or cyclic active methylene compounds containing heteroatom such as (2-thio)barbituric acid, Meldrum's acid using ionic liquids as reaction medium.

在第二部分中我们研究了离子液体中开链活性亚甲基化合物、杂环类活性亚甲基化合物如(2-硫代)巴比妥酸、Meldrum's酸与芳香醛之间的Knoevenagel缩合反应。

In the culture solutions with 15 mgL^(-1) methylene blue and 5 mgL^(-1) safranine T respectively, Spirulina subsalsa 8 days decoloration efficiencies to methylene blue and safranine T are 98.9% and 95.6%, respectively.

当番红花红T浓度为5mgL^(-1)时，盐泽螺旋藻对番红花红T的8天脱色率为95.6%。

The condensation of aromatic aldehydes with active methylene compounds like malononitrile, cyanoacetamide and ethyl cyanoacetate has been found to proceed very efficiently at room temperature giving excellent yields, but the condensation of heteroaromatic,α,β-unsaturated and aliphatic aldehydes with active methylene compounds proceeded smoothly in 50~65℃ with good yields and the reactions of aromatic, aliphatic ketones as well as p-phthalaldehyde with malononitrile also proceeded in 75~85℃ with moderate yields.

芳香醛与活泼亚甲基化合物如丙二腈、氰基乙酸乙酯、氰基乙酰胺的缩合在室温下即能顺利进行，获得了很高的收率；而对于杂环芳醛、α，β-不饱和的醛以及脂肪醛与活泼亚甲基化合物的缩合，需在50~65℃下进行，也取得了很高的收率；对于脂肪酮、芳香酮以及二元醛与丙二腈的缩合在75~85℃下也能顺利地进行，获得中等以上的收率。

Analysis of the spectrum obtained by means of homonuclear H,H-correlation spectroscopy revealed a coupling between the methylene group with a chemical shift of 2.08 ppm and the methylene group at 2.42 ppm as well as the proton at 3.76 ppm, as expected for a glutamic acid moiety.

作为独立的肽中一部分的亮氨酸和亮氨酸基之间的区别可以通过将13C 化学位移和从其它单个氨基酸中获得的化学位移进行对比后得出。

The α-methylenecyclopentanone, as an isostere of α-methylene-γ-lactone, within the molecules of diterpenes may be as effective as α-methylene-γ-lactone towards various sulfhydry-containing enzymes.

然而，由于α-亚甲基-γ-丁内酯结构内在的化学活性太强，尽管这些合成的小分子化合物仍具有抗癌或抗炎活性，但并没有达到降低毒性，提高选择性的目的。

OBJECTIVE, To study the direction, route and num- ber of SLCs and their relationship with SLN after subareolar injection of methylene blue and technetium 99m sulfur colloid （^99m Tc-SC）, and to explore the mechanism of sentinel lymph node biopsies produce false negative results in breast cancer patients and the method to improve the detectable rate, METHODS: ^99m Tc-SC was injected preoperatively, and methylene blue was injected by the same subareo-lar route just after anesthetic induction, and then SLNB was carried out according to SLCs in 93 breast cancer patients.

目的：通过乳晕下联合注射^99m Tc-SC和亚甲蓝，研究前哨淋巴通道的行走方向、途径、数量及其与前哨淋巴结之间的关系，以探讨乳腺癌SLNB出现假阴性的机制，并提出提高其检出率、减少假阴性的方法。

This immediately brings us to the next part of this article: creating an output "replace function".

下面进入文章的第二部分：建立一个"缓存处理函数"。

He was elected as an International Ornithological Committee member in 2002 during the 24th IOC held in Beijing.

现为中国鸟类学会理事和WPA 专家组成员。2002年被推选为国际鸟类委员会委员。