查询词典 methyl-glyoxal

Compounds were determined from more than 3 stages, including germacrene D, caryophyllene, phenol, 2, 6-bis (1, 1-dimethylethyl)-4-methyl-,β-elemene,γ-elemene, 1-octanol, 2-butyl-, dibutyl phthalate, cyclohexane, 1-ethenyl-1-methyl-2-(1-methylethenyl)-4(1-methylethylidene)-and butyl caprylate.

其中，3个时期以上能检测到相同的化学成分有9种，分别是大牻牛儿烯D、丁香烯、2，6-二叔丁基－4-甲基苯酚、β-榄香烯、γ-榄香烯、2-丁基－1-辛醇、邻苯二甲酸二丁酯、1-乙烯基－1-甲基－2-（1-甲基乙烯基）－4-（1-甲基亚乙烯基）环己烷和辛酸丁酯。

1-phenyl-3-methyl-4-caprylpyrazolone-5 was synthesized from 1-phenyl-3-methyl-pyrazolone-5 and caprylyl chloride, and some extraction parameters were investigated such as the acidity, the concentration of Sr, the time of the extraction and the thinners.

通过1-苯基-3-甲基-吡唑啉酮-5与辛酰氯合成萃取剂1-苯基-3-甲基-4-辛酰基吡唑啉酮-5，并对其萃取Sr的影响因素，如酸度、Sr浓度、萃取时间和稀释剂等进行研究。

The factors that affected the degradation rate of methyl red are discussed, including the concentration of methyl red, the kind of electrolyte, the concentration of sodium bromide, the anodic current density, the material of electrode, the cathodic current density and the flow rate of oxygen at the catholyte.

探讨甲基红浓度、电解质种类、电解质浓度、阳极电流密度、电极材料、阴极电流密度与阴极室氧气流量等因表对甲基红电分解的影响。

To be different from the already chloromethylation catalyst, it has a certain amount of moisture wet, which will not produce huge amounts of doughtic cancerogenic chloromethyl methyl ether during and after the reaction.4,4\'-bisbiphenyl, 1,4-bisbenzene, 1,4-bis(chloro- methyl)-2,5-dimethylbenzene, 1,5-bis-2,4-dimethylbenzene, 4-(chlor- omethyl)-1,2-dimethylbenzene, 1,2-bis-4,5-dimethylbenzene, 5,8-bis-1,2,3,4-tetrahydronaphthalene, 3,3\',5-tris-4,4\'-bisbiphenyl and 3,3\', 5,5\'-tetrakis-4,4\'-bisbiphenyl were synth- esized by using this new catalyst. Results indicated that when the reaction temperature was 55～60℃, the reaction time was 12h, the catalyst which consists of the concentration of 80%H_2SO_4, HAc and Lewis acid, the amount of Lewis acid 0.15 mol(nLewis:nbiphenyl=1.5:1), yield of biphenyl chloromethylation product 4,4\'-bis(chrolomethylbiphenyl can reach a maximum 85%.

采用这种催化体系完成了4，4′-二氯甲基联苯、对二氯甲基苯、1，4-二氯甲基-2，5-二甲基苯、1，5-二氯甲基-2，4-二甲基苯、4-氯甲基-1，2-二甲基苯、1，2-二氯甲基-4，5-二甲基苯、5，8-二氯甲基-四氢萘、3，3'，5-三氯甲基-4，4'-二甲基苯和3，3'，5，5'-四氯甲基-4，4'-二甲基苯的合成，结果表明：在反应条件为：反应温度55～60℃，反应时间12h，选择80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.15mol(和原料比为1.5：1)，反应效果最好，联苯氯甲基化产物(4，4′-二氯甲基联苯)收率为85%；在反应条件为：反应温度70℃，反应时间8h，80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，苯的氯甲基化产物收(来源：ABd0C论文eded网www.abclunwen.com)率为75%；在反应条件为：在反应条件为：反应温度40℃，反应时间10h，60%H_2SO_4和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，对二甲苯氯甲基化产物(1，4-二氯甲基-2，5-二甲基苯)收率为78.5%；在反应条件为：反应温度35℃，反应时间10h，60%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，间二甲苯氯甲基化产物(1，5-二氯甲基-2，4-二甲基苯)收率为81.5%。

With the yield of methyl monochloroacetate as evaluating standard,the synthesized condition of methyl chloroacetate was optimized through orthogonal experiment.

以氯乙酸母液和甲醇为基本原料，固载磷钨酸为催化剂，通过连续酯化的方法制备了氯乙酸甲酯；以氯乙酸甲酯的质量收率为基准，采用三因素三水平正交实验的方法对酯合成的条件进行了优化。

The use of chemically-methyl phenol and chloroacetic acid to synthesize methyl-phenoxyacetic acid.

利用化学方法将间甲基苯酚和氯乙酸合成为间甲基苯氧乙酸。

The main products are formic acid, propionic acid, methyl acetate, morpholine, imidazole, methyl chloroformate, 1,2-pentanediol, nylon and engineering plastic.

代理BASF和HONEYWELL优质产品散水化工品：甲酸，丙酸，醋酸甲酯中间体：吗啉，咪唑，氯甲酸甲酯，1，2－戊二醇，尼龙和工程塑料。

In addition, a benzene, toluene (0.32%), was also detected in 80% ripening fruit. In 90% ripening fruit were detected 27 kinds of aroma components belonging to 2 categories. Among the components, 17 were esters, and 10 alkenes. Of the 17 esters, methyl octanoate is the highest (21.00%), followed by ethyl hexanoate (17.64%), methyl hexanoate (14.34%). Of the 10 alkenes cis-β-ocimene is the highest (1.00%), followed by à-copaene (0.81%) and trans-ocimene (0.48%).

在9成熟果实中检测到2类共27种香气成分，分别是酯类17种和烯类10种；在酯类中，相对含量最高的是辛酸甲酯(25.27%)，其次是辛酸乙酯(21.00%)、己酸乙酯(17.64%)、己酸甲酯(14.34%)；在烯类中相对含量较高的有β-顺式－罗勒烯(1.00%)、à-蒎烯(0.81%)和反式－罗勒烯(0.48%)。

Our main products include 5-Methyl-2-pyrazinecarboxylic acid series, Guanine series, Folic acid series, Methyl Cyanoacetate and Ethyl cyanoacetate series, we also have made great contribution in the development of cardiovascular drug, stomach drug, anti-inflammatory drug and antidepressants, such as Nizatidine, Acipimox, Glipizide, Zaltoprofen and Pregabalin, which have been put into production on large scare.

公司主要产品有5-甲基吡嗪-2-羧酸系列，鸟嘌呤系列，叶酸，氰乙酸甲酯，氰乙酸乙酯系列，在心血管药、胃药、消炎药、抗抑郁药等新品开发上有重大建树，先后研制成功，形成批量生产，如尼扎替丁、阿西莫斯、格列吡嗪、扎托洛芬、普瑞巴林，同时具备为客户定制化学品的能力。

Synthesis of Antidote of N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane BI Hong-mei, ZHANG Jin-yan, LIANG Ying, SHEN Yong (College of Arts and Sciences Heilongjiang August First Reclamation University, Daqing 163319, Heilongjiang, China) Abstract: N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane was synthesized by one pot method with isopropanolamine, cyclopentanone and dichloroacetyl chloride. The optimum reaction conditions obtained are as follows:the proportion in moles of the above materials is 1∶1∶1.2, reaction solvent is toluene, reaction temperature is -15 to -10 ℃,reaction time is 3 h, under the optimum condition, the yield of the compound is 50.0%.

除草剂解毒剂N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷的合成毕洪梅，张金艳，梁英，沈勇(黑龙江八一农垦大学文理学院，黑龙江大庆 163319)摘要：以33%的氢氧化钠水溶液为缚酸剂，异丙醇胺、环戊酮和二氯乙酰氯为原料，采用&一锅法&合成了N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷，采用正交实验法得到最佳反应条件：反应原料摩尔比为1∶1∶1.2，苯作溶剂，反应的温度为-15 ℃~-10 ℃，搅拌时间为3 h，产率达到50.0%。

My first article for Screen Power Magazine, which is to this day is the official magazine of Jackie Chan, was a DVD review of the Hong Kong actioner Gen-X Cops, starring Nicholas Tse and Daniel Wu.

我的第一篇文章为屏幕力量杂志，在对这天是Jackie Chan 正式杂志，是香港actioner Gen X 警察的DVD 回顾，担任主角Nicholas Tse 和丹尼尔吴。

His lips grazed hirs, Now what are you going to do?

他的唇使吃草了 hirs，现在你将要做什麼？