查询词典 methyl-ethyl ether

The results of our research showed that the chinaberry seed oil, two emulsion formulations of crude toosendanin, Margosan-O, azadirachtin, AZT(NR-2), AZAL-S, petrolem ether extract of the leaf of Tagetes erecta, methyl extract of the root of Tagetes erecta, methyl extract of the whole plant of Bidens pilosa, the oil of Ageratum conyazoides and polygodial had potent toxicity to the larvae of Anopheles sinensis, Culex quinquefasciatus and Aedes albopitus.

中华按蚊Anopheles sinensis、致倦库蚊Culex quinquefa-sciatus和白纹伊蚊Aedes albopictus都是我国重要的传病蚊种。本研究首次证实下列植物的提取物对上述三种蚊虫有毒杀作用：(1)苦楝：苦楝油；(2)川楝：川楝素乳剂、蔬果净；(3)印楝：Margosan-O、印楝素、AZT(NR-2)、AZAL-S；(4)万寿菊：叶石油醚提取物、根甲醇提取物；(5)三叶鬼针草：整株植物甲醇提取物；(6)百花草：精油；(7)水蓼：Polygodial。

The preparation process of equisetum pratense total alkaloid includes the following steps: coarse pulverizing equisetum pratense to obtain rough powder, methyl alcohol percolation to obtain percolate, recovering methyl alcohol, concentrating, degreasing by means of petroleum ether, alkalifying concentrate, CHCl3 extracting, soda lye washing, neutral water washing, recovering CHCl3 to obtain rough alkaloid, adsorption by using silica gel column, eluting, recovering solvent so as to obtain refined EPR.

该发明是通过两个步骤来实现的：第一步，提取草问荆总碱，流程：草问荆粗粉――渗漉液――浓缩液(析胶、石油醚脱脂、氨水碱化)――碱化浓缩液(CHCl3萃取)――CHCl3层――CHCl3液(回收CHCl3)――粗生物碱――吸附硅胶柱――精致EPR。第二步，选择实验试剂、仪器、用小鼠作为实验对象，进行中枢神经系统实验，研究作用及作用机制。

Under the catalyst, the polymerization retarder, the including water medicinal preparation existence condition, the methylacrylic acid and the polyethylene glycol single methyl ether (400) direct esterification synthesis methylacrylic acid polyethylene glycol single methyl ether (400) ester, and the influence factors of the catalyst, polymerization retarder, including water medicinal preparation has mellowly carried on the comparison.

摘要在催化剂、阻聚剂、带水剂存在的条件下，由甲基丙烯酸与聚乙二醇单甲醚(400)直接酯化合成甲基丙烯酸聚乙二醇单甲醚(400)酯，并对酸醇比、催化剂、阻聚剂、带水剂等影响因素进行了比较。

The research indicated that under the compound use of hydroquinone and methyl quinone or independent use of phenothiazines or nitrogen oxygen free radical made the polymerization retarder, opposite-methyl-phenylsulfon made the esterification catalyst, toluol made the backflow including water condition, the acid mellowly compared to when it was 1.15, the production rate of the synthesis methylacrylic acid polyethylene glycol single methyl ether (400) ester may achieve 98.9%, was extremely similar to the overseas product functional group structure.

研究表明，在氢醌、甲醌复合使用或者单独使用吩噻嗪、氮氧自由基哌啶酮作阻聚剂，对甲苯磺酸作酯化催化剂、甲苯作回流带水的条件下、酸醇比为1.5时，合成的甲基丙烯酸聚乙二醇单甲醚(400)酯产率可以达到98.9%，与国外产品官能团结构十分相似。

In this paper, eleven benzothiazole derivatives such as N, N, N′, N′-tetra (2-benzothiazolyl) methyl-1, 2-ethanediamine,(2-benzothiazolyl) methyloxy benzene, 2,4-dichloro( 2-benzothiazolyl) methyloxy benzene, O-di(2-benzothiazolyl) methyloxybenzene, P-di(2-benzothiazolyl) methyloxy benzene, 3-(2-benzothiazolyl) pyridine were synthesized by means of conventional method or MWI technology and a single crystal of di (2-benzothiazolyl ) methyl ether was obtained.

本文分别用常规合成法和微波辐射法合成了N，N，N′， N′-四(2-苯并噻唑基)甲基-1，2-乙二胺、(2-苯并噻唑基)甲氧基苯、2，4-二氯-(2-苯并噻唑基)甲氧基苯、邻-二(2-苯并噻唑基)甲氧基苯、对-二(2-苯并噻唑基)甲氧基苯、3-(2-苯并噻唑基)吡啶等11 个苯并噻唑类化合物并得到二(2-苯并噻唑基)甲基醚单晶。

To be different from the already chloromethylation catalyst, it has a certain amount of moisture wet, which will not produce huge amounts of doughtic cancerogenic chloromethyl methyl ether during and after the reaction.4,4\'-bisbiphenyl, 1,4-bisbenzene, 1,4-bis(chloro- methyl)-2,5-dimethylbenzene, 1,5-bis-2,4-dimethylbenzene, 4-(chlor- omethyl)-1,2-dimethylbenzene, 1,2-bis-4,5-dimethylbenzene, 5,8-bis-1,2,3,4-tetrahydronaphthalene, 3,3\',5-tris-4,4\'-bisbiphenyl and 3,3\', 5,5\'-tetrakis-4,4\'-bisbiphenyl were synth- esized by using this new catalyst. Results indicated that when the reaction temperature was 55～60℃, the reaction time was 12h, the catalyst which consists of the concentration of 80%H_2SO_4, HAc and Lewis acid, the amount of Lewis acid 0.15 mol(nLewis:nbiphenyl=1.5:1), yield of biphenyl chloromethylation product 4,4\'-bis(chrolomethylbiphenyl can reach a maximum 85%.

采用这种催化体系完成了4，4′-二氯甲基联苯、对二氯甲基苯、1，4-二氯甲基-2，5-二甲基苯、1，5-二氯甲基-2，4-二甲基苯、4-氯甲基-1，2-二甲基苯、1，2-二氯甲基-4，5-二甲基苯、5，8-二氯甲基-四氢萘、3，3'，5-三氯甲基-4，4'-二甲基苯和3，3'，5，5'-四氯甲基-4，4'-二甲基苯的合成，结果表明：在反应条件为：反应温度55～60℃，反应时间12h，选择80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.15mol(和原料比为1.5：1)，反应效果最好，联苯氯甲基化产物(4，4′-二氯甲基联苯)收率为85%；在反应条件为：反应温度70℃，反应时间8h，80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，苯的氯甲基化产物收(来源：ABd0C论文eded网www.abclunwen.com)率为75%；在反应条件为：在反应条件为：反应温度40℃，反应时间10h，60%H_2SO_4和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，对二甲苯氯甲基化产物(1，4-二氯甲基-2，5-二甲基苯)收率为78.5%；在反应条件为：反应温度35℃，反应时间10h，60%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，间二甲苯氯甲基化产物(1，5-二氯甲基-2，4-二甲基苯)收率为81.5%。

From the point view of product distribution, conversion of dimethyl ether and energy consumption, with RCD plasma DME conversion was higher and was hardly affected by the residence time of dimethyl ether, and hydrogen, carbon monoxide and unsaturated hydrocarbons with RCD plasma were more than those with DBD plasma.There was no liquid product with RCD plasma, but the liquid product obtained with DBD plasma consisted of aldehydes, alcohols and methoxy-containing organic compounds, for instance, formaldehyde, methyl alcohol, dimethoxy ethane and so on.Moreover, most compositions of liquid product were methoxy-containing compounds, and the liquid product selectivity was as high as 32.23%.However, energy consumption for the reaction with DBD plasma was more than that with RCD plasma.

从产物分布、转化率及能耗上看，利用RCD所获得的二甲醚的转化率高，几乎不受二甲醚停留时间的影响，且氢气、一氧化碳和不饱和烃的含量大，几乎没有液相产物，而利用DBD能获得较多的液相产物，包括一些醇、醛和含有甲氧基的有机化合物，如甲醛、甲醇和二甲氧基乙烷，且大部分组成都是含有甲氧基的化合物，液相产物的选择性高达32.23％，但是能耗较大。

The result showed that the thermal decomposition temperature of chlorinated paraffin reached 133℃ by adding 0.3% composite stabilizer in which the weight percentages of ethylene glycol diglycidyl ether, methyl stannic, triphenyl phosphate, exoxidized soybean oil were 72%, 3%, 10%, 15%, respectively. It is 15℃ more than that of using pure ethylene glycol diglycidyl ether.

结果表明：当复合稳定剂中乙二醇二缩水甘油醚、甲基锡、亚磷酸三苯酯、环氧大豆油的质量分数分别为72%，3%，10%，15%，复合稳定剂的添加量为氯化石蜡的0.3%时，氯化石蜡的热分解温度为133℃，比单独使用乙二醇二缩水甘油醚提高了15℃，热稳定效果较好。

Importance of methyl ether plant construction in our province with one step method on the basis of coal is expounded from main uses,production methods and economic benefits of methyl ether as well as the advantage of coal resources in our province.

从二甲醚的主要用途、生产方法、经济效益，以及山西省煤炭资源优势等方面，论述了用煤基一步法生产二甲醚的重要意义。

As raw chemical materials, produce acetone, hydrogen peroxide, methyl isobutyl ketone, isobutyl ketone, 2-Propanol, diisopropyl ether and isopropyl alcohol ether, isopropyl chloride, isopropyl and fatty acids and fatty acid chloride as isopropyl.

作为化工原料，可生产丙酮、过氧化氢、甲基异丁基酮、二异丁基酮、异丙胺、异丙醚、异丙醇醚、异丙基氯化物，以及脂肪酸异丙酯和氯代脂肪酸异丙酯等。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。