查询词典 method of synthesis

A new way of synthesis 2-methoxy-4'-trifluoromethyl acetophenone by the method of crossed ester condensation was investigated in the overall yield of higher than 85%.

本文提出了一种新的方法——交叉酯缩合法合成2-甲氧基-4'-三氟甲基苯乙酮。

The method of dimension synthesis for the path of connecting rods of crank slider mechanism with predetermined time scale by using rotation angle operator of connecting rods is proposed in this paper.

提出了利用连杆转角算子对带有预定时标的曲柄滑块机构连杆轨迹进行尺度综合的方法。

In order to obtain the best synthesis temperature of cordierite by the method of direct sintering, samples were synthesized with pressed raw blocks respectively at controlled temperatures of 1310℃,1350℃ and 1400℃.

为了研究采用直接烧结法合成堇青石的最佳合成温度，对压成的生料块分别在最高合成温度为1300℃，1350℃，1400℃下进行合成，通过对比不同合成温度下得到的样品X射线衍射图，确定出采用直接烧结法合成堇青石的最佳合成温度。

In this paper,a design method of two dimensional Linear Phase Nearly Perfect Reconstruction filter banks based on a new class of cosine modulation systems is presented,which can be described as follow: firstly,the Parks-McClellan algorithm is adopted for designing the prototype filter,then by employing cosine modulation,a series of analysis and synthesis filters can be obtained,accordingly a one-dimensional LP-NPR filter banks can be constructed;Secondly,cascading two one-dimensional LP-NPR filter banks in the form of tree structure and using the unimodular transformation,a two dimensional nonseparable LP-NPR filter banks can be obtained.

提出了一种基于一类新余弦调制系统的二维线性相位-近似完全重构滤波器组的设计方法，设计过程分为两个步骤：首先采用Parks-McClellan算法来计原型滤波器，再经过余弦调制能到一系列的线性相位分析和综合滤波器，从而可以构造一维LP-NPR滤波器组；然后利用树状结构来结合两个一维LP-NPR滤波器组，并运用单位模变换，可以得到二维不可分离LP-NPR滤波器组。

The method of liquid phase synthesis of dioxane from the cyclodehydration of diethylene glycol catalyzed by ASP-type solid acidic catalysts was studied.

研究了ASP型固体酸催化剂一缩乙二醇环化脱水合成1，4-二氧六环的液相反应。

The major contributions of this thesis include:(1) proposing a new kind of optimal feedback control, followed by its application to chaos targeting and stabilization of high period unstable periodic orbits ;(2) stabilization of unstable fixed point in chaotic systems using some kind of nonlinear feedback control, and giving sufficient condition for the existence of the controller as well as the synthesis procedure;(3) analyzing the robustness of optimal control in chaotic Lur'e systems under the help of H〓 control theory;(4) finally and most importantly, introducing a novel method of information storage based on discrete time chaotic systems as the application of chaos control, and systematically studying different schemata for implementation, providing a theoretic basis for the design of such new kind of information storage devices with large capacity.

本文的主要工作包括，提出一种新的最优反馈控制，并将之应用于混沌引导控制及混沌系统高周期不稳定周期轨道的镇定控制；针对不动点镇定控制的一类非线性反馈控制器，文中给出该类反馈控制存在的充分条件及设计步骤；文中还利用非线性H〓鲁棒控制理论对Lur'e混沌系统中的最优线性反馈控制进行鲁棒性分析；最后，也是最重要的，作为混沌控制的应用，文中提出一种基于离散时间混沌系统的信息存储方法，系统地分析、研究了实现这种信息存储的不同方案，为以后进行这种新型大容量存储器设计提供了一定的理论依据。

In order to obtain the thermodynamic data of the synthesis of ethyl methyl carbonate from dimethyl carbonate and diethyl carbonate, the standard molar enthalpies of formation, Gibbs free energy and molar heat capacity under constant pressure are calculated by the method of Benson group contributions.

为了得到碳酸二甲酯和碳酸二乙酯酯交换合成碳酸甲乙酯反应的热力学数据，用Benson基团贡献法计算了相关物质的标准摩尔生成焓、吉布斯自由能和摩尔定压热容。

The way of synthesis of piperazine using the industrial ethylenediamine as rawmaterial is applicable, the Higher activity and selectivity of K-ZSM-5 catalyst prepared by the method of ion-exchange was obtained.

离子交换法制备的K-ZSM-5分子筛作为脱氨环化反应的催化剂具有较好的活性和选择性。

A new method of solvent-thermal synthesis of Meso-tetra(4-carboxyphenyl) zincporphyrin complexs, using the propionic acid and the DMF as solvents and the salt of zinc, catalyst-;pyrrol,4-carboxybenzaldehyde, as reagents.

报道了用丙酸和DMF作溶剂和催化剂，直接用吡咯，4 羧基苯甲醛，锌盐合成Meso 5，10，15，20 四锌卟啉配合物的新型方法———溶剂热合成。

Phenyl or m -tolyl selenoamides reacted with functionalized α-haloacetic acid in 1∶1 or 1∶2 molar ratio with no catalyst in various alcohols to undergo a selenium transfer reaction. This reaction in dif-ferent molar ratios furnished the same C—Se—Se—C coupling products with a special structure bis diselenide. A new and facile method for synthesis of such bis(alkoxycarbonyl-methyl) diselenides with the advantages of mild reaction conditions, high yields, easy availability of starting materials and good chemical selectivity was provided.

芳基硒代酰胺与氯乙酸在各种醇中无催化剂下以1∶1和1∶2的比例投入，发生硒转移反应，不同原料投入比下的反应生成了同一种C—Se—Se—C偶联产物——具有多功能团的二烷氧羰基甲基二硒醚，提供了一种新的合成二烷氧羰基甲基二硒醚的简便方法，且反应具有条件温和、产率高、原料易得和选择性好等优点。

In the United States, chronic alcoholism and hepatitis C are the most common ones.

在美国，慢性酒精中毒，肝炎是最常见的。

If you have any questions, you can contact me anytime.

如果有任何问题，你可以随时联系我。