查询词典 method of synthesis

A simple and efficient method for the synthesis of N3-functionalized 3,4-dihydropyrimidinones by aza-Michael addition reactions of 3,4-dihydropyrimidinones toα,β-ethylenic compounds catalyzed by KF/Al_2O_3 is described.

研究结果表明：DHPMs类化合物可与α，β-不饱和羰基化合物发生Michael加成反应，产物只有N3位功能化的DHPMs，而没有N1位的产物。

Synthesis of glycidol and epoxidized polyurethane and their characterization;2. Improvement in Hyperbranched Poly glycidol Hydroxyl Groups' Conversion by Protection Method;3. The structure of glycidol was confirmed by IR and 1HNMR.

以一氯代丙二醇为原料，与碱性化合物在低温作用下合成了缩水甘油，并通过IR、1HNMR对其进行了结构表征。

This paper introduced the typical application of glyoxylic acid in the synthesis of fine chemical products and the basic manufacture method.

本文介绍了乙醛酸在精细化学品合成中的典型应用和乙醛酸的基本生产方法，并比较了不同生产方法的各自特点，同时分析了乙醛酸的市场情况，指出了高质量乙醛酸将具有良好的市场前景。

The solid product was characterized by N2 adsorption-desorption, XRD, TEM and hydrothermal stability test. These results indicated that small amounts of HPMo in the synthesis media could reduce the amount of liquid in-organic acid and crystallization time greatly. And SBA-15 sieves prepared in this method exhibited an excellent hydrothermal stability, as its hexagonally ordered mesostructure was maintained after treated in 100 ℃ water over 72 h.

N2吸附-脱附、XRD、TEM和水热稳定性实验等检测结果表明：用这种方法不仅可以大幅度降低合成SBA-15分子筛所需液体酸的用量和缩短晶化时间，同时反应产物SBA-15在100 ℃的水中处理72 h后仍然保持六方有序的介孔结构。

A method for the synthesis of lappaconitine hydrobromide by the reaction of dibromoalkyl with lappaconitine is presented.

报道了以双溴代烷烃和刺乌头碱合成刺乌头碱氢溴酸盐的方法。

The process does not depends on catalytic hydrogenization method, has simple reaction condition, high reactant yield all over 75%, can use TLC to track the whole reaction process, and is more suitable to the transformation of function group in the organic synthesis field as the result of N-Boc or N-Cbz derivative is easy to loss protective reaction, which has spreading application prospect.

该方法不依赖于催化氢化方法，反应条件简单，反应产物产率高，均在75％以上，反应过程可用TLC进行跟踪，且由于N-Boc或N-Cbz衍生物更易发生去保护反应，在有机合成领域更适宜于官能团的转化，具有广阔的应用前景。

In order to reduce synthesis times and prepare zeolite membrane with high quality. In chapter three, a good seed layer was prepared on the substrate surface by vapor phase transformation method and then subjected to microwave heating. The highly compact NaA membranes obtained above were composed of intergrown crystals.

为了减少合成次数，降低膜的厚度，制备出高质量的NaA分子筛膜，本论文第三章采用汽相预涂纳米晶种的方法在载体上制备出高质量的纳米晶种层，然后在微波加热条件下合成出高度致密的NaA分子筛膜，膜是由高度孪生的晶体组成。

Supported solid bases and metal oxide catalysts were prepared successfully by isochoric impregnation and the co-precipitation method, and were used for synthesis of biodiesel from transesterification of rapeseed oil and methanol. The high active solid base catalysts: KF/Al2O3, ZnO/La2O3 and La2O3 were found in this paper.

本文用等体积浸渍法和共沉淀法制备了负载型和金属氧化物型固体碱催化剂，并应用于催化菜籽油与甲醇酯交换合成生物柴油的反应，筛选出了高活性的KF/Al2O3，ZnO/La2O3和La2O3三种固体碱催化剂。

A mild and convenient method for the synthesis of 4(3)-substituted 3(4)-nitro-1H-pyrroles and 3-substituted 4-methyl-2-tosyl-1H-pyrroles from nitroolefins and tosylmethyl isocyanide in ionic liquid 1-butyl-3- methylimidazolium bromide was developed.

本文以离子液体－溴化1-丁基-3-甲基咪唑为溶剂，采用对甲苯磺酰基甲基异腈与硝基烯反应生成4(3)-取代-3(4)-硝基-1-氢吡咯或3-取代-4-甲基-2-对甲苯磺酰基-1-氢吡咯。

This synthetic method paves another new way for synthesis and functionalization of novel ladderlike polymers.

FTIR，1H-NMR，29Si-NMR，XRD，DSC，VPO及溶解性实验表明合成的梯形聚倍半硅氧烷具有很好的梯形结构。

In the United States, chronic alcoholism and hepatitis C are the most common ones.

在美国，慢性酒精中毒，肝炎是最常见的。

If you have any questions, you can contact me anytime.

如果有任何问题，你可以随时联系我。