查询词典 method of synthesis

As far as we know, no information of this synthesis method on boron suboxide films has ever been reported. Series measurements were performed to study this kind boron suboxide nanofilms prepared by PLD.

我们在制备方法上作了突破：以PLD方法得到类HP-HT的条件制备得到boron suboxide薄膜并对它进行了一系列的观测鉴定和分析研究。

Monochloroethylene carbonate is prepared by chlorination of ethylene carbonate with sulfuryl chioride ,a solution of monochloroethylene carbonate in ethylene carbonate is reacted with triethylamine to give vinylene carbonate.A parameter design method was applied to select the optimum synthesis conditions.63.3％ and 78％ yields superior to the conventional for monochloroethylene carbonate and vinylene carbonate were obtained respectively,and the process was also simplified .

以碳酸乙烯酯为原料，用磺酰氯作为氯化剂生成一氯代碳酸乙烯酯，三乙胺为脱卤化剂在碳酸乙烯酯溶剂中合成碳酸亚乙烯酯，对一氯代碳酸乙烯酯和碳酸亚乙烯酯制备的工艺参数进行优化，收率分别达到63.3％和78％，均超过了传统方法，且简化了工艺，缩短了反应时间，易于工业化生产。

An efficient and new method for the synthesis of symmetrical dibenzyldiselenides is described.

这是一种非常有效的合成二硒醚的新方法。

The new method is a synthesis of the best features of the old methods.

新方法是综合旧方法的长处而成的。

The existence of pointwise robust convergent algorithm and uniformly robust convergence is next investigated. We propose an optimal l〓 robustness synthesis method for structured perturbations system by taking advantage of the famous Small Gain Theorem.

证明了最优l〓辨识算法的存在性；证明了黑箱辨识存在辨识算法使全局误差收敛于有界区间；提出并证明了逐点鲁棒收敛算法的存在性；证明了一致鲁棒收敛算法的存在性。

Macroporous tributyl amine aminating strongly basic anion exchange resin-a phase transfer catalyst with high catalytic activity for nucleophilic substitution,which was screened out via combinatorial chemistry method –was used to catalyze the nucleophilic substitution reactions for synthesis of benzyl acetate,benzyl propionate,benzyl butyrate and benzyl valerate.

用组合化学方法筛选出的对无外加碱条件下的亲核取代催化活性最高的聚合物季铵盐–三丁胺胺化强碱性阴离子交换树脂为相转移催化剂，催化合成了乙酸苄酯、丙酸苄酯、丁酸苄酯、戊酸苄酯等羧酸苄酯。

DATA SYNTHESIS: Diabetes had been seriously threatening human health, and islet cell transplantation was a possible method that could cure the diabetes, however there was not enough islet resource so that people started to look for other vicariousness resource of islet cells.

资料综合：糖尿病是严重威胁人类健康的疾病之一，胰岛细胞移植是治愈糖尿病的可能方法，但由于胰岛细胞数量有限，不能满足临床需要，人们开始寻找胰岛细胞的可替代资源。

Imino-1, 3-thiazetidines is the basic structure of a kind ofbioactive herbicide and insecticide. Our method has advantage in synthesis highly substituted2-imino-1, 3-thiazetidines, therefore it has practical value to some extent. We also researched the reactions catalyze by active zinc dust.

提供了成四员噻吖丁啶杂环衍生物的方法。2-亚胺基-1，3-噻吖丁啶是一类具有生物活性的除草剂及杀虫剂的核心结构，我们的方法在合成多取代的2-亚胺基-1，3-噻吖丁啶方面有一定的优越性，从而具有一定的实用价值本文另一部分的工作是探讨锌粉催化的反应。

Objective To determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of Edaravone, by gas chromatography.Methods Sample solution was injected on a GDX column (0.18 mm～0.25 mm) with nitrogen as the carrier gas.The residue was calculated by the external standard method.

摘要］ 目的：用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量方法：采用固定相二乙烯苯乙基乙烯苯型高分子孔小球（直径为0.18 mm～0.25 mm），氮气为载气，用外标法测定乙酰乙酸乙酯中残留丙酮的含量。

Different aspects associating the DMAE-NHS-based CLIA were studied in this thesis,including synthesis of acridinium ester,chemiluminescent characteristics of DMAE-NHS,labelling antibody or streptavidin with DMAE-NHS,two-site sandwich chemiluminescent immunoassay for TSH,two-site sandwich chemiluminescent immunoassay involved biotin-streptavidin system for TSH,and competitive chemiluminescent immunoassay using biotin-streptavidin system for TLVThe desired acridinium ester,DMAE-NHS,was synthesized according to the reference method with some modifications.

目前国内尚未见有关DMAE·NHS的合成及其应用于CLIA的研究报导，本论文研究了吖啶酯DMAE·NHS的有机合成方法，DMAE·NHS的发光性能，DMAE·NHS及其与抗体偶联物的热稳定性，DMAE·NHS标记TSH单克隆抗体和链亲和素，TSH CLIA，TSH BAS-CLIA和TT_4 BAS-CLIA。

In the United States, chronic alcoholism and hepatitis C are the most common ones.

在美国，慢性酒精中毒，肝炎是最常见的。

If you have any questions, you can contact me anytime.

如果有任何问题，你可以随时联系我。