查询词典 method of synthesis

According to the characteristics of the electrocatalysis synthesis process, and based on the causes of ionic membrane pollution, a kind of effective cleaning method in-situ of polluted membrane was presented.

根据电催化合成过程特点，从离子膜被污染的原因分析入手，提出了有效的污染膜原位清洗法。

The paper considers that urban planning methodology is composed with three parts. They are philosophy foundation, noetic methodology and operational methods. The philosophy foundation of urban planning methodology under the framework of multi-rationality composes of Marxist philosophy with materialistic dialectic and historical dialectic as the core, western philosophy such as humanism, verificationism, and historism etc., oriental philosophy centralized on synthesis and unison. The noetic methodology of urban includes micro logical noetic methods macro visual noetic methods and micro-macro creative noetic methods. The urban planning operational method includes the route, process and techniques needed in practice.

其中，城市规划方法的哲学基础是在总体的复合理性框架之下，由以辩证唯物主义和历史唯物主义为核心的马克思主义哲学，人本主义、实证主义、历史主义等西方哲学以及强调综合调和、天人合一的东方哲学思想所构成；城市规划思维方法体系，是城市规划过程中思考问题的角度及处理问题的方法论的总和，包括微观的逻辑思维方法、宏观的形象思维方法和宏微结合的创造性思维方；城市规划操作方法体系是直接用于城市规划实践的方法归纳和概括，包括城市规划的方法路线、程序组织、技术方法等等。

In this paper, the 3-D finite element relocating mesh method is used to calculate the temperature field and the thermal creep stress field of spillway dam and mid level outlet dam in certain roller compacted concrete gravity dam, sensitivity analysis have been down with different parameters, such as placing temperature, the location of cooling pipe, cooling temperature, time for water supply, ascended-layer of concrete, intermissive time and different placing time, and the commendatory construction scheme have been put forward in such analysis; according by the test result on the two scheme of concrete aggregate combination (basalt as coarse aggregate and limestone as fine aggregate, basalt as coarse aggregate and basalt as fine aggregate), simulation analysis on temperature field and thermal creep stress field of the commendatory construction scheme have been down, and analysis have also been down on temperature field and thermal stress field of the two different aggregate combination, the result indicates that the spillway dam and mid level outlet dam which adopted these two aggregate combination can both satisfy the require of design crack resistance in concrete, furthermore limestone as fine is better than basalt as fine aggregate; the effect of summer water storage and winter water storage on the temperature field and thermal stress field have been analyzed, comparing with winter water storage, in summer water storage scheme the maximum tensile stress at abnormal concrete in upstream fill is decreased by 0.1～0.3MPa and there are no evidence change of the maximum tensile stress at other parts, which indicate that summer water storage is avail for the crack resistance of upstream fill; according to the simulation calculating result and comparing temperature simulation calculating results and temperature controlling measures of some similarity projects both completed and construction, synthesis appraise have been carried to the design temperature controlling measures of dam, and the temperature controlling measures of this project have been brought forward, all these have great reference value on the design of temperature controlling measures and the optimization of the construction scheme.

本文采用三维有限元浮动网格法仿真计算程序，对某碾压混凝土重力坝的溢流坝段和中孔坝段分别进行了三维有限元温度场和温度徐变应力仿真计算分析，对浇筑温度、冷却水管的布置方式、冷却水温、通水时间、浇筑升程和间歇时间、不同开始浇筑日期等参数进行了敏感性分析，在此基础上提出了推荐的施工方案；根据两种骨料方案(玄武岩粗骨料+灰岩细骨料方案；玄武岩粗骨料+玄武岩细骨料方案)的混凝土性能试验研究成果，对推荐的施工方案进行了温度场和温度徐变应力仿真计算，并对比分析了两种不同骨料情况下的温度场和温度应力，结果表明溢流坝段及中孔坝段采用上述两种骨料均能满足混凝土的抗裂设计要求，且灰岩细骨料优于玄武岩细骨料；计算分析了夏季蓄水和冬季蓄水对坝体温度场和温度应力的影响，夏季蓄水方案与冬季蓄水方案相比，坝体上游变态混凝土区域最大拉应力小0.1～0.3MPa，其他部位最大拉应力无明显变化，夏季蓄水对坝体上游面混凝土的抗裂有利；根据仿真计算成果并通过比较国内一些已建和在建的类似工程的温度仿真计算成果及采取的温控措施，对大坝的设计温控措施进行了综合评价，并提出了该工程的温控措施，对温控设计和优化施工方案具有重要参考价值。

Completion of the synthesis involved displacement of the remaining alcohol through a three-step, telescoped sequence featuring an efficient cleavage of an aryl mesylate, and a practical method for introduction of the isobutyric acid fragment.

完成剩余的位移所涉及合成酒精通过三个步骤不胜顺序展出了高效率的卵裂甲磺酸芳、而实际的方法引入异丁酸片段。

In this thesis, we describe a facile and economical synthesis of-abscisic acid from keto-isophorone and 3-butyn-2-ol through ketalization, oxidization, Witting-Horner reaction, reduction with chromium sulfate and other steps in 13% total yields. Compared to the previous routes, the starting materials are more commercially available and cheaper and the synthetic process is more easily controlled in our method, but the yield of this route is still to be improved.As to isostere principle, cyclopropyl and methyl vinyl are a couple of isostere.

本论文设计并完成了一条全新的外消旋脱落酸(1)全合成路线，从廉价的工业原料氧化异佛尔酮和丁炔醇出发，经过缩酮化反应、氧化反应、Wittig-Horner反应、CrSO_4选择性还原反应以及水解等七步反应实现了脱落酸的全合成，总产率达13％，与以往路线相比，该路线所用试剂廉价、合成路线简单，但产率有待提高。

A reversed-phase high performance liquid chromatographic method was established for determination of isothiocyanates in human urine , which used the reaction of propyl isothiocyanate with 1,2-benzenedithiol as reference instead of the synthesis of 1,3-benzodithiole-2-thione.

省去合成1，3 苯二硫杂环五烯 2 硫酮这一步骤，直接用异硫氰酸丙基酯与1，2 苯二硫酚反应作标准，建立了尿液中异硫氰酸酯的反相高效液相色谱测定方法。

Hybrid mesoporous molecular sieve materials with hexagonal mesoporous structure and covalent bonded polyoxometalates were synthesized based on tetraethoxysilane anti lacunary polyoxometalate, SiW11, via sol-gel method in the presence of triblock copolymers P123 as the structure-directing agent. The influences of molar ratio of inorganic precursors and aging temperature on the structure and the loadings of SiW11 in the hybrid materials were investigated. Some reaction details in the synthesis were revealed.

用嵌段共聚物P123为模板剂，正硅酸乙酯和缺位结构的多金属氧酸盐SiW11为无机前驱体，由溶胶－凝胶法合成了具有六方结构和SiW11共价键联的介孔分子筛杂化材料SiW11/SBA-15，着重考察了无机前驱的配比和老化温度对杂化材料结构及SiW11负载量的影响。

Use the method that the article determines to authority is worth, methylic to synthesis acrylic acid the course of two kinds of chemical industry of armour ester, namely different butene law (I-C4) and propylene law (C3) undertook green spends evaluation and analysis, make clear I-C4 law course more green.

采用本文确定权值的方法，对合成甲基丙烯酸甲酯的两种化工路线，即异丁烯法(i-C4)和丙烯法(C3)进行了绿色度评价和分析，表明i-C4法路线更为绿色。

In this paper, the synthesis of polyamide acid resin, with 4, 4′-diam-inodiphenyl ether and pyromellitic dianhyride as monomers and dimethylacetamide as solvent, is reported; the preparation of polyimide fiber from PAA resin by dry- spinning method is described; and the effects of various factors of operating conditions upon the mechanical properties of the fiber is discussed.

本文报导了用4，4′—二氨基二苯醚与苯均四酸酐作单体，在N，N′—二甲基乙酰胺溶剂中合成聚酰胺酸树脂，以及用该树脂经干纺法制备纤维和制备过程中各项参数对纤维力学性能的影响。

A series of SiW_(12)/AC catalysts with different silicotungstic acid loadings supported on acti- vated carbon which was treated with 10% HNO_3 solution were prepared by an impregnation method and the catalytic performance of SiW_(12)/AC for the synthesis of trioxane were investigated.

以10%硝酸溶液处理过的活性炭为载体，采用不同质量分数的硅钨酸SiW_(12溶液为浸渍液，制备了不同负载量的SiW_(12)/AC催化剂，考察了催化剂在合成三聚甲醛中的催化性能，并用XRD、FT-IR、NH_3- TPD、BET、TG-DSC等手段对SiW_(12)/AC催化剂晶粒大小、催化剂表面的酸量及酸强度、比表面积及热稳定性等微观特性进行了表征。

She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了，但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场，你等着挨绳子吧！