查询词典 method of synthesis

The dynamic characteristics of stochastic truss structures and stochastic frame structures are analyzed by using Random Factor Method. Then, from the expressions of structural random response of the frequency domain, the computational expressions of the mean value, variance and variation coefficient of the mean square value of the structural displacement and stress response under the stationary random excitation or non-stationary random excitation are developed by means of the random variable's functional moment method and the algebra synthesis method.

考虑压电智能桁架结构物理参数、几何参数、结构阻尼和外荷载、闭环系统控制电压分别或同时为随机变量，构建了结构在随机力作用下的动力响应分析模型，提出了求解方法，推导出结构动力响应随机变量的数字特征计算表达式，通过算例验证了所建模型和所提求解方法的正确性和有效性。

objective to determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of edaravone, by gas chromatography.methods sample solution was injected on a gdx column (0.18 mm～0.25 mm) with nitrogen as the carrier gas.the residue was calculated by the external standard method.results the linearity was good over the range of 25 μg/ml～400 μg/ml,with the correlation coefficient of acetone being 0.996 and the average recovery 96.8%.conclusions the method was proved to be simple,rapid,practical and highly sensitive.it is an efficient method for the quality control of acetoacetic ester.

摘要］ 目的：用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量。方法：采用固定相为二乙烯苯乙基乙烯苯型高分子多孔小球（直径为0.18 mm～0.25 mm），氮气为载气，用外标法测定乙酰乙酸乙酯中残留丙酮的含量。结果：该方法在丙酮浓度范围在25 μg/ml～400 μg/ml内呈良好的线性关系，响应曲线相关系数为0.996，平均回收率为96.8%。结论：本法简便，快速、实用，灵敏度高，可有效地用于乙酰乙酸乙酯的质量控制。

In order to reduce the non-specific binding between oligonucleotides and bases mutation caused by the complicate secondary structure of DNA and excessive PCR amplification, a frequently phenomenon in one-step gene synthesis, we used a two-step method including assembly PCR and digestion-ligation step to synthesis Aspergillus niger lipase gene lipA.

本研究主要针对一步法长片段基因合成中复杂结构的非特异性配对和过多的PCR引入碱基错配等问题，采用二步法(组装PCR和酶切-酶连)合成了黑曲霉脂肪酶基因lipA。

Moreover, seven ruthenium phenanthroline derivatives were also synthesized. The synthesis of Ru3Cl2 and Ru2AqphenCl2 have not yet been reported, and a new and effective method for the synthesis of Ru32 was also investigated.

本文第二章主要内容是以邻菲咯啉为原料，合成四种刚性结构强的邻菲咯啉衍生物：二吡啶基吩嗪，四吡啶基吩嗪， 10.11-1.4-萘酮－2，3；2'，3'－二吡啶基吩嗪，对羟基苯基并[4，5]-邻菲咯啉。

Calcium montmorillonite was prepared by purifying LeXi bentonite with wet method two times. After purification, sodium modification of Ca-M was studied. A series of Fe/Cr-pillared montmorillonites were prepared with conventional method using sodium montmorillonite as experimental materials, and synthesis condition of Fe/Cr-PILM was studied and optimized. In order to shorten the preparation cycle of PILM by overleaping the step of sodium modification of Ca-M, the pretreatment technique for Ca-M has been pointed out for the first time. A series of PILMs were prepared with hydrothermal method using pretreated Ca-M as starting materials, which show that pretreatment of Ca-M is feasible.

然后，本文以莱西膨润土为原料，用二次湿法提纯了-2μm的钙基蒙脱石，对其进行了钠化改型研究；以改型后的钠基蒙脱石为原料，新型的铁、铬复合离子为柱化剂，研究并优化了常规离子交换法制备PILM的工艺；为了简化PILM的制备工艺，我们首次提出了蒙脱石的预处理工艺，希望通过预处理后可以省去蒙脱石的钠化工艺，以Ca-M为原料直接合成PILM。

Both Fas and NO can lead chondrocyte apoptosis respectively and cause articular cartilage destruction. IGF-Ⅰ, TGF-β, bFGF, BMP and other growth factors are polypeptide agents that can influence cell activity by signal convection. They can accelerate chondrocyte proliferation and proteoglycan synthesis, play the local regulation action on formation and plerosis of bone and cartilage tissue by autocrine or paracrine. They have the ability to induce cartilage formation. Some investigations showed that growth factors can influence chondrocyte metabolism, synthesis of specific Ⅱ type collagen and proteoglycan by co-operation and inhibition. 1. 3 Situation of OA therapeutics The therapeutic methods of OA mainly comprised non-drug treatment, drug treatment, operation treatment, tissue and genetic engineering, et al. Drug treatment is the chief method among them.

若其活性发生改变，则将导致关节软骨基质成分的丢失和进行性破坏；软骨细胞凋亡与OA的发病密切相关，Fas与NO可各自独立介导软骨细胞凋亡，造成关节软骨破坏；IGF-Ⅰ、TGF-β、bFGF、BMP等生长因子是一组通过细胞间信号传递影响细胞活动的多肽因子，具有促进细胞生长、增殖与合成等作用，可通过自分泌或旁分泌方式对骨和软骨的形成和修复起局部调节作用，可促进软骨细胞增殖、分化与蛋白多糖的合成，具有较强的诱导软骨形成的能力，研究表明多种生长因子相互促进、相互抑制，以协同或拮抗方式影响软骨细胞代谢，影响软骨细胞特异性Ⅱ型胶原和蛋白多糖的合成分泌。

This paper bases on frequency-hopped and frequency synthesis theories, and through demonstrating three schemes of frequency synthesis, the paper selects one of these schemes that uses DDS spiriting up PLL and improves on the method according to the practical target and synchronously, the paper analysis the capability of the output signal and the conversion time of the frequency.

本文在对跳频理论及频率合成理论分析的基础上，在讨论三种频率合成方案后，设计完成了一种适于本课题的DDS激励PLL的混合方案，并对频率合成器主要性能中的输出信号的噪声特性和频率转换性能做了研究分析。

The type synthesis and kinematic analysis of secondary counterbalancing GLMs are carried out with the above-mentioned structure synthesis method and GTTM respectively.

用所提类型综合的方法对抽油机二次平衡GLM进行了结构综合；用广义型转化法对GLM进行了运动分析，并对方案进行了选优。

A method and apparatus for conversion of solid and liquid fuels to a synthesis gas, steam and/or electricity in which about 10% to about 40% of a solid fuel and/or a liquid fuel is introduced into a gasifier and gasified, resulting in formation of a synthesis gas.

一种将固态和/或液态燃料转变为合成气体、蒸汽和/或电的方法和装置，其中固态和/或液态燃料的约10％到40％内的燃料导入气化器被气化，形成合成气体。

Synthesis of methylene-4,4'-di catalyzed by zinc oxide Various metal oxide were investigated in the synthesis of methylene-4,4'-di from ethyl carbamate, and a serious of ZnO/SiO2 catalysts were prepared by deposition-precipitation method.

氧化锌为催化剂合成4，4'-二环己基甲烷二氨基甲酸乙酯以氨基甲酸乙酯和4，4'-二环己基甲烷二胺的反应体系为研究对象，在考察多种金属氧化物活性的基础上，使用沉积沉淀法制备了一系列硅胶负载氧化锌催化剂，并对其催化性能进行了研究。

She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了，但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场，你等着挨绳子吧！