查询词典 methanol

As for acetalation, we research the effects of acid kinds, acid quantity, temperature solvents on it and get the conclusions that the optimized acid is sulfuric acid, the optimized temperature is 65 °C, the reaction time is five hours, and the material ratio of sulfuric acid to methylglyoxal to methanol is 0.028:1:6.837.

在醛保护一步中，研究了酸种类、酸用量、温度及其溶剂的影响，得到了本反应的较好条件是：酸为浓硫酸，反应温度为65℃，反应时间为5小时，浓硫酸：丙酮醛：甲醇的配比为0.028：1：6.837，反应收率可达81%。

The synthesis of dimethyl fumarate was studied from maleic anhydride and methanol with phospho molybdic acid as the catalyst and bromate as the isomerization catalyst by one-step in this short paper.

采用固体杂多酸磷钼酸为催化剂，溴酸盐为异构化剂，经顺酐一步合成了富马酸二甲酯，探讨了醇酐比、反应时间、催化剂的量、异构化剂的量以及异构化时间对合成DMF收率的影响，并确立了最佳反应条件。

Methods The HPLC was performed on Lichrospher C18 (200 mm × 4.6 mm, 5μm) column. The mobile phase consisted of methanol and 0.02 molL^(-1) monobasic potassium phosphate buffer (60:40). The flow rate was 1.0 mlmin^(-1). The detection wavelength was set at 333 nm.

以汉邦Lichrospher C18 (200 mm×4.6 mm，5μm)为色谱柱，以甲醇-0.02 molL^(-1)磷酸二氢钾溶液（用磷酸调节pH值至4.2）60：40）为流动相，UV检测波长333 nm，流速1.0mlmin^

Methods: The HPLC with a C18 column (150mm×4.6mm, 5μm) was used. Methanol-0.05mol/L Potassium phosphate monobasic buffer solution-Acetic acid glacial (40:60:1) was used as mobile phase. The flow rate was 1.0mL/min, and the detection wavelength was at 333nm.

采用高效液相色谱法，用C18色谱柱(150mm×4.6mm， 5μm)，以甲醇-0.05mol/L磷酸二氢钾溶液-冰乙酸(40：60：1)为流动相，流速为1.0mL/min，检测波长333nm。

The chromatography conditions were as follows: methanol - 0.1mol/L monobasic potassium phosphate (50∶50) as mobile phase, flow rate being 1.0ml/min and detecting wavelength was 290nm.

方法采用高效液相色谱法，色谱柱为Diamonsiltm C18柱；流动相：甲醇-0.1 mol/L磷酸二氢钾水溶液（50∶50）；流速：1.0 ml/min；检测波长：290 nm。

MethodsHigh Performance Liquid Chromatography was performed Diamonsil C18. The chromatography conditions were as follows: methanol - 0.1mol/L monobasic potassium phosphate (50∶50) as mobile phase, flow rate being 1.0ml/min and detecting wavelength was 290nm.

方法采用高效液相色谱法，色谱柱为Diamonsiltm C18柱；流动相：甲醇-0.1 mol/L磷酸二氢钾水溶液（50∶50）；流速：1.0 ml/min；检测波长：290 nm。

Either methanol or other suitable solvent, such as ethylene glycol monomethyl ether, may be used as the diluent.

可能是甲醇或者其他合适的溶剂，例如二乙醇甲醚，可以用做稀释剂。

Influences of reaction temperature, catalyst concentration, molar ratio of methanol to propylene oxide and reaction time on conversion of propylene oxide, yield and selectivity of propylene glycol monomethyl ether were studied.

在反应温度为120～130℃、催化剂用量为0.20%～0.30%、甲醇与环氧丙烷摩尔比为3/1～5/1的反应条件下，环氧丙烷的转化率在98％以上，丙二醇甲醚的选择性达95％，收率达93％，产品中伯醚的选择性为92％～93％。

Influences of reaction temperature, catalyst concentration, molar ratio of methanol to propylene oxide and reaction time on conversion of propylene oxide, yield and selectivity of propylene glycol monomethyl ether were studied.

研究了甲醇与环氧丙烷在固体碱催化剂MAF存在下非均相合成丙二醇甲醚的过程。

Norbornene-2,3-dicarboxylic acid monomethyl ester was prepared by using 5-norbornene-2,3- anhydride and methanol as raw materials and toluene as solvent.

以5-降冰片烯-2，3-二酸酐和甲醇为原料，正交试验法合成了5-降冰片烯-2，3-二羧酸单甲酯，并对产物结构进行了表征。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。