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In the thesis, we wish to report the synthesis and structures of a series of new type rigid conjugated nanometer-sized fulvene ligands, and coordination polymeric compounds based on both metal-carbon and metal-heteroatom interactions and also H-bonded supramolecular architectures generated from this new type of fulvene ligands.

基于此，我们合成了一系列刚性共轭的纳米级富烯类配体，并以之与过渡金属离子反应合成了同时基于金属-碳和金属-杂原子两种键合作用的有机-无机配位高聚物及以氢键作用为驱动力的超分子聚集体。

Among them,the chemosensory properties of two molecular tweezers derived from diethoxycarbonyl glycoluril for metal ions were studied by fluorescent spectroscope.It was found that they both exhibited selective recognition towards Fe~(3+)among 13 metal ions investigated in DMF/CH_3OH(50:1, v/v)with fluorescence quenching,and formed 1:1 stoichiometry complex with Fe~(3+).

通过荧光光谱滴定考察了其中两个二乙基酯基甘脲分子钳异构体对13种不同金属离子的识别作用，研究表明在DMF/MeOH(50：1 v/v)中，它们能够很好地选择性地识别Fe~(3+)离子，与Fe~(3+)离子形成1：1的复合物并且呈现荧光淬灭效应，可作为Fe~(3+)的荧光化学传感器。

According to the determination of fluorescence properties,mononuclear metal complexes have fluorescence properties,while heteronuclear metal complex does not have fluorescent properties.

根据荧光性能的测定，单核金属配合物具有荧光性能，异核双金属配合物没有荧光性能

The molecular sieve is prepared in the steps: at the room temperature, hexadecyl trimethyl ammonium bromide is mixed and dissolved with the sodium hydroxide, and is added with TEOS in dropping way, and simultaneously added with Me metal salt water solution and lanthanum nitrate solution in dropping way; the pH value of the mixed solution is adjusted by acetic acid to be 10 to 11, and is mixed for 1 to 2 hours after being stabilized; the sol is moved into a polyfluortetraethylene bottle to be heated and crystallized for 2 days in the oven at the temperature of 100 DEG C; after filtering, washing and drying for nights, and being calcined in a muffle at the temperature of 550 DEG C for 3 to 7 hours, the dual-metal-atom improved MCM-41 mesoporous molecular sieve is obtained.

该分子筛的制备为室温下，将十六烷基三甲基溴化铵和氢氧化钠混合溶解，搅拌并滴加入TEOS，同时滴加入Me金属盐水溶液和硝酸镧溶液并搅拌，用乙酸调节pH值至10～11，稳定后搅拌1～2小时，溶胶转入聚四氟乙烯瓶中在100℃下烘箱水热晶化2天，经过滤、洗涤、干燥过夜，马弗炉550℃焙烧3-7h，得双金属原子改性MCM-41介孔分子筛产品。

Different from the conventional catalyst immobilization methods, the self-supporting strategy utilizes homochiral metal-organic coordination polymers generated by self-assembly of chiral multitopic ligands with metal ions without using any support.

与传统的负载模式不同，手性自负载催化剂通过含双或多官能团的手性配体与金属通过自组装形成一类有机-无机聚合物，因此无需使用任何载体，即能够有效地实现手性催化剂的回收和再利用。

A 2.8-inch (7.112 cm) homochromous flexible display was fabricated on a plastic substrate, which showed a luminance of 120 cd/m2 at a drive-voltage of 12 V. A top-emitting FOLED was fabricated on a metal substrate. The efficiency of FOLED is close to OLED on a glass substrate, and the CIE coordinates are about (x=0.69,y=0.31). The color purity of the top-emitting device on metal substrate is much improved.

在聚合物衬底上成功制备了2.8 inch（7.112 cm）的128×64单色FOLED显示屏，在驱动电压12 V时屏体亮度达到120 cd/m2；在金属衬底上，采用顶发光技术制备了FOLED元器件，顶发光器件与相对同发光层结构底发光器件有相近的电流效率，色坐标（x=0.69，y=0.31），色纯度优于相同发光层结构的底发光器件。

Process for the preparation of phosphatidylserine of formula wherein R and R independently represent a saturated, mono-unsaturated or polyunsaturated acyl C10-C30, X=OH or OM where M=alkaline or alkaline earth metal, ammonium, alkylammonium including the transphosphatidylation reaction between phosphatidylcholine of the general formula wherein R and R and X have the above specified meanings, R=CH2-CH2- NH2 o CH2-CH2-N(CH3)3 and Serine in D, L or racemic form catalysed by the phospholipase D enzyme, characterised in that said reaction is carried out in a hydroalcoholic medium containing an aliphatic alcohol and in the presence of bivalent metal oxide.

本发明涉及制备式CH 2 OR 1 CHOR 2 CH 2 O-P-OCH 2 -CH(NH 2 )-COOHX的磷脂酰丝氨酸的方法，其中R 1 和R 2 独立地表示饱和的、单不饱和的和/或多不饱和的酰基C 10 -C 30 ，X＝OH或OM，其中M＝碱或碱土金属、铵、烷基铵，该方法包括通式CH 2 OR 1 CHOR 2 CH 2 O-P-OR 3 X的磷脂酰胆碱其中R 1 和R 2 以及X具有上述特别的含义，R 3 ＝CH 2 -CH 2 -NH 2 或CH 2 -CH 2 -N (CH 3 3 与D、L或外消旋形式的丝氨酸之间的转磷脂酰化反应，该反应是通过磷脂酶D酶催化的，其特征在于所述的反应是在包含脂族醇的含水醇介质中并且在二价金属氧化物的存在下进行的。

On base of analysis to simulation result, it was point out the main cause making dissimilar metal"s bonding so difficult was metal"s inharmonic plastic deformation. The distribution and changement of stress and strain on interface and in workpieces were analyzed.Making use of experiment and simulation result, main factors that influence welding property of cold pressure welding were discussed.

通过对模拟结果的分析，说明了异种金属冷压焊较同种金属冷压焊困难的原因主要是界面处两种材料的径向和轴向的不协调塑性变形；直观地显示了冷压焊过程中工件内部及界面处的应力应变分布及变化情况。

The law how these factors influence the joint"s property was pointed out. A formula about the relationship between extrusion times and contamination remainder was founded. Main reason to bimetal"s inharmonic deformation was the difference of their mechanical property. Thereby, the empirical formula showing the relation between metal combination"s mechanical property and quality of joint was constructed. Integrated influence of extrusion times and metal"s mechanical property to quality of cold pressure welding joint was discussed.

在模拟结果分析和实验的基础上，对影响异种金属冷压焊焊接性的工艺因素进行了分析；探讨了诸因素对接头性能的影响规律，并且建立了挤压次数与界面污染物残留量之间的数学表达式；指出了两种材料力学性能差异是造成不协调塑性变形的主要原因，并且建立了材料力学性能与其冷压焊焊接性之间的经验公式；定性的讨论了挤压次数及材料力学性能对冷压焊接头性能的综合影响。

The characteristics and application of the main mining methods of China's metal mines and their improvement and application prospect are discussed. In view of the existing technical basis and the trend of the demand of China's economical development on metal mines' resource, the future development of mines is prospected. Several feasible concepts are given such as the development orientation of mathematical mine and artificial intelligency, optimization of the hauling system of open pit mining and open...

讨论了我国金属矿山主要采矿方法的特点、应用情况、得到的改进及应用前景，针对现有的技术基础以及我国经济发展对金属矿资源的需求趋势，对未来矿山的发展进行了展望，重点提出了数字矿山、人工智能等发展方向，及进行露天开采运输系统优化和地下开采露天化几种可行性的设想，为我国采矿工作研究者提出了几种新的课题。

I can still vividly recall the impressive scenes you gave. You were among my friends and relatives who accompanied me from my house to the seaport and when the porters were slow to show up, you obligingly carried my suitcase for me.

你对我的种种感人情意，使我记忆犹新，那天你随着我的亲友从家里送我上轮船，搬运工迟迟不来，你毅然替我提着皮箱上船。

St. Nicholas became the patron saint of Russia, where he was famous for his red cape, flowing white beard, and bishop's mitre.

圣尼古拉成了俄罗斯人的守护神，在那里，他以身披红斗篷，留着飘逸的白胡须，戴着主教法冠而闻名。