查询词典 mesityl

Objective: To establish a method for detection of mesityl oxide in the air of workplace by GC chromatography.

目的：建立工作场所空气中异亚丙基丙酮的采样和测定方法。

Objective: To establish a method for mesityl oxide in the air of workplace by GC -MS.

目的 建立工作场所空气中异亚丙基丙酮气质联用测定方法。

The method meets the requirements of Regulation of Studies on the Determination of Toxicants in the Air of Workplace. It is suitable to determine the mesityl oxide in the air of workplace.

本方法各项指标达到《工作场所空气中有毒物质检测方法研制规范》要求，适用于工作场所空气中异亚丙基丙酮的测定。

The method is meet the requirements of Regulation of Studies on the Determination of Toxicants in the Air of Workplace.It is suitable to determine the mesityl oxide in the air of workplace.

本方法各项指标达到《工作场所空气中有毒物质检测方法研制规范》要求，适用于工作场所空气中异亚丙基丙酮的测定。

The unit can be used to sample most containerized liquid wastes, except those containing ketones, nitrobenzene, dimethylformamide, mesityl oxide, and tetrahydrofuran.

Nasco的 COLIWASA液体废品取样器可以收集的取样样品类型包括：粘度的，有腐蚀性的，有波动性和固体形状的样品。

Methods: Mesityl oxide in the air was sampled by active carbon tube and desorbed by the solvent of carbon disulfide which included 1% methanol, then separated by FFAP capillary column, and finally detected by hydrogen flame detector. The experimental study was conducted according to the requirements of Regulation of studies on the determination of toxicants in the air of workplace.

工作场所空气用活性炭管采集，经1%甲醇的二硫化碳溶液解吸，FFAP毛细色谱柱分离，氢火焰离子化检测器检测，按照《工作场所空气中有毒物质检测方法研制规范》的要求进行方法研究。

Results: The good linear range of method was 10 to 1000μg/ml (T=0.9999) with the correlation coeffivient of 0.9999, and the limit concentration in air was 0.2 mg/m^3 with the average relative standard deviation less than 5%(n=6). The average sampling rate ranged from 96.6 to 100%, and the breakthrough capacity of l00mg activated charcoal was 4.7mg. The average desorption rate was 97.6%, and mesityl oxide absorped in activated charcoal tube was stable for 7 days and can be detected accurately with other gas coexisting in the air of workplace.

结果：异亚丙基丙酮浓度在10~1000μg/ml内呈良好线性关系，相关系数0.9999，最低检出浓度为0.2mg/立方公尺，相对标准偏差＜5%(n=6)；气体采样效率≥96.6%，100mg活性炭对异亚丙基丙酮的穿透容量为4.7mg，平均解吸效率97.6%；活性炭样品室温下可保存7天；丙酮、丁酮、异佛尔酮、苯、甲苯、二甲苯等共存物不干扰测定。

Methods: Mesityl oxide in the air was sampled by active carbon tube and desorbed by the solvent of carbon disulfide which included 1% methanol, then separated by HP-5 capillary column,and finally detected by mass detector.

工作场所空气用活性炭管采集，经1%甲醇的二硫化碳溶液解吸，HP-5毛细色谱柱分离，气质联用仪检测。

A new organic compound, trans-2--5-dimesitylborylthiophene (abbreviated as DMASBT, 5) with dimesitylboryl, dimethylamino and styryl-thiophene as electron acceptor, electron donor and conjugate bridge respectively, was synthesized. Its crystal structure determined by X-ray diffraction method indicates that the B-C bond between B atom and it bridge is obviously shorter than those of between B atom and mesityl groups. This remarkably strengthened B-C bonding can be regarded as an evidence of additional p-7t conjugation between the B atom and n bridge.

合成了以含硼基团为电子受体，以二甲胺基为电子给体，以苯乙烯基噻吩为共轭桥的新化合物2-[（4'-N，N-二甲胺基）苯乙烯基]-5-二米基硼-噻吩 trans-2-[(4'-N， N-dimethylamino) styryl]-5-dimesitylboryl-thiophene（简写为DMASBT，5）。X射线衍射方法测定其单晶结构表明，硼原子与π共轭桥之间的硼碳键相对于其它的硼碳键明显缩短，硼与π共轭桥之间存在除了σ键之外的p-π共轭作用。

The steoreselectiviy showed the E selectivity in most of cases and Z selectivity was presented in larger substituents like mesityl and 1-naphthyl.

进一步增大烯上的取代基则可以得到Z选择性的烯炔产物。利用如此的方式，也许还可以用来合成含烯炔的高分子。

The dissecting of samples in group2 were difficult. The root of pulmonary artery and ascending aorta failed to be unfolded because fibrous tissue was tough, right and left fibrous trigone were too firm to be solved by hand. Cardiac muscle fibers couldn't be stripped along myofibrillar trajectory since they were prone to break because of their friability.

组2的心脏解剖困难，表现为纤维组织坚韧，游离肺动脉非常困难；徒手无法松解左、右纤维三角，肺动脉和主动脉根部的游离非常困难；心肌纤维坚硬、质脆，解剖时容易断离成碎块，无法沿纤维走行方向剥离。

We have battled against the odds in a province that has become increasingly violent.

我们对在一个争夺日益激烈省的可能性。