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The observation of SEM, EDAX and IR analysis showed that the conformation of MPPE was changed, the surface and section of MPPE were rough and accidented, the specific surface area of MPPE was increased, and magnetic powders, HAP and other additives were separated in polyethylene polymer. The removal rates of Phenol by using PPE and MPPE were 82％, 93％, the removal rates of TOC could reach 78％, 89％ respectively, when the phenol wastewater at 120mg/L concentration was treated with aerated process for 14 hours. The removal rates of Phenol were 85％, 90％, the removal rates of TOC reached 80％, 86％ respectively when the phenol wastewater at 350mg/L was treated for 35 hours. The weight of biofilm formation on MPPE was 64％ and 34％ higher than that on PPE at this two wastewaters.

质量浓度为120mg/L的含苯酚废水在好氧生物填料柱中处理14 h后，PPE和MPPE对苯酚去除率分别为82％和93％，TOC去除率分别为78％和89％；质量浓度为350mg/L的含苯酚废水处理35h后苯酚去除率分别为85％和90％，TOC去除率分别为80％和86％；两种不同质量浓度的含苯酚废水降解后MPPE上微生物挂膜量分别比PPE提高约64％和34％。

The acetated and hydrogenated urushiol dimer has been separated,and studied by hetero-J resolved 2D-NMR,homo- and heteronuclearchemical shift correlation 2D-NMR and long-range coupled chemicalshift correlation 2D-NMR.The results show that the urushiol dimerare most diphenyl and alkyl phenyl ether structures.Furthermore,IR and MS data also has conformed this structures.

本文将酶催化预聚后的生漆，催化加氢后，乙酰酯化，再进行离心旋转薄层层析，分离得到二聚体主要组分，用异核J分辨谱，同核化学位移相关，异核化学位移相关，远程偶合异核化学位移相关等2D—NMR技术，全面研究了其结构，得到了联苯型和烷基芳醚型聚合结构的结论。

_6P_2W_(17)VO_(62) catalyst was prepared and characterized by FTIR,and synthesis of fraistone over as-synthesized catalyst from ethyl acetoacetate and 1,2-propylene glycol was investigated.

制备了Dawson型磷钨钒酸铵催化剂，用FT-IR分析方法对催化剂进行了结构表征，并以乙酰乙酸乙酯与1，2-丙二醇为原料催化合成了苹果酯-B。

Yields from chiral bisoxazolines (5a) with diethyl oxalate using NaOCH〓 as base for the first time. The structures of chiral multioxazolines and their intermediates, multi (β-hydroxylamide) s, were characterized by 〓H NMR, IR, mass spectra and elemental analysis. The catalytic activities and enantioselectivities of chiral multi (β-hydroxylamide) s (4) and chiral multioxazolines (5～8) were investigated by using acetophenone and β-acetonaphthone as former chiral ketone, KBH〓 or NaBH〓 as reductive reagent in chapter three.

在此基础上，对合成方法作了创新，以羧酸或酯为原料，在无催化剂的条件下与手性α-氨基醇反应，通过回流分水或脱醇的方法，一步反应合成了手性多噁唑啉（5～8），产率为89.2%～98.4%；以手性双噁唑啉（5a）为原料，在NaOCH〓的作用下，与草酸二乙酯反应，首次合成了呋喃类双嗯唑啉（6a），产率为72.9%～75.6%。

Chemiluminescent immunoassay is one of the advanced immunoassay ofnon-radioisotopic immunoassay because of its high sensitivity, wide dynamic range,high accuracy, stable labeled protein, full automation and extensive application field.CLIA using acridinium ester derivatives as chemiluminescent label has advantages oflow background, high signal-to-noise ratio, no need of catalyst and simpleluminescence system. Different aspects associating the DMAE·NHS-based CLIA were studied in thisthesis, including synthesis of acridinium ester, chemiluminescentcharacteristics of DMAE·NHS, labelling antibody or streptavidin with DMAE·NHS,two-site sandwich chemiluminescent immunoassay for TSH, two-sitesandwich chemiluminescent immunoassay involved biotin-streptavidinsystem for TSH, and competitive chemiluminescent immunoassay usingbiotin-streptavidin system for TT〓. The desired acridinium ester, DMAE·NHS, was synthesized according to thereference method with some modifications. The products were identified by IR, NMR,MS and elemental analysis. In our method, KOH was used in place of NaOH tosynthesize benzyl ester of 3,5-dimethyl-4-hydroxybenzoic acid,2',6'-dimethyl-4'-(n-succinimidyloxycarbonyl) phenyl-acridinium-9-carboxylate waspurified on a silica gel column with chloroform/ethylacetate(4:1, v/v) as eluent andfurther purified by triturating with hexane/acetone(2:1, v/v).

DMAE·NHS的合成是本论文的关键和难点，我们对文献方法进行改进：文献方法用氢氧化钠与3，5-二甲基-4-羟基苯甲酸反应制得3，5-二甲基-4-羟基苯甲酸钠，再用3，5-二甲基-4-羟基苯甲酸钠与苄氯作用制备3，5-二甲基-4-羟基苯甲酸苄酯，我们用氢氧化钾代替氢氧化钠，使合成取得成功；在合成2'，6'-二甲基-4'-苯基-吖啶-9-甲酸酯时，文献方法对粗产品进行两次硅胶柱层析纯化，第一次柱层析用氯仿／乙酸乙酯(4∶1，V∶V)作溶剂和淋洗剂，第二次柱层析用己烷／丙酮(2∶1，V∶V)作溶剂和淋洗剂，按照文献方法得到的不是所需要的化合物，我们只进行第一次柱层析纯化，然后用己烷／丙酮(2∶1，V∶V)进行研磨，过滤，洗涤，除去溶于己烷／丙酮(2∶1，V∶V)的部分，得到所需要的产品。

Efficacious drugs were made of these species for treatment of cough, phlegm, breathe heavily, especially, to cure lung disease. We have investigated on the Chemical constituents of Adenophora stenanthina subspecies xifengsis collected from Gansu Qingyang, and twenty four compounds were isolated from ethanol extraction by chromatography technigues. Twenty compounds were identified by means of chemical and spectra methods（IR, FAB-MS, EI-MS,〓,〓, DEPT , among which three compounds were new as 3βvanilloyloxy-stigmast-5-ene-7β-one; 3β-Vanilloyloxy-stigmast-5-en-7 β-ol; 3β-vanilloyloxy-stigmast-5-en-7β, 15 〓-diol.

我们对采自甘肃庆阳的西峰沙参Adenophorastenanthina subsp.xifengensis）进行了化学成分的研究，利用现代层析手段从该植物的乙醇浸膏中分离出二十四个化合物，经化学方法和波谱技术（红外，质谱，核磁共振谱）鉴定了二十个化合物的结构，其中三个为新的化合物，它们分别是：豆甾-5-烯-7-酮-3β-香草酸酯；7β-羟基-豆甾-5-烯-3β-香草酸酯；7β，15ξ-二羟基-豆甾-5-烯-3β-香草酸酯。

From the results of IR and XPS spectrocopy. The cationic sol components H〓SiO〓 and 〓 of the solution trend to adsorp on the surface of electronegative aegirine because of electrostatic acctraction each other, and interrupted the collector's reaction with Fe〓 on the surface. Hence the flotation of aegirine was decreased, on the other hand, there is electrostatic repulsion between the surface of hematite and the cationic sol H〓SiO〓.〓, Which has advantage to dispersion of hematite particles, therefore, the hematite flotation is achieved sucessfully with anionic collector.

根据红外光谱和XPS测试结果可知，在弱酸性介质中，活性硅酸胶体抑制剂中荷正电的胶团H〓SiO〓及〓由于电性吸引而选择性地覆盖在荷负电的钠辉石表面，从而阻碍了阴离子捕收剂与表面Fe〓的配位作用，导致钠辉石的浮游被抑制；而赤铁矿表面由于荷正电，与矿浆中的H〓SiO〓、〓等硅酸胶团存在着电性排斥作用，有利于赤铁矿颗粒的稳定分散，所以赤铁矿能够被脂肪酸捕收剂吸附而选择性上浮。

Your life is your own affa ir.

你的生活是你自己的事。

After 30 and 45 days of composting, FT-IR spectra exhibited a decrease of intensity of peaks assigned to polysaccharides and in the aliphatic region.

在堆肥30至45天后，傅里叶转换红外光谱显示峰值密度在脂肪族区域的减少归因于多聚糖的变化。

The fluorinated alkoxide can then react with a variety of substrates.

以核磁共振仪、气相质谱仪与FT-IR进行样品鉴定。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。