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The molecular structures of these derivatives were characterized by IR and 1HNMR respectively. The UV absorption and photoluminescent properties were also studied.

探讨了反应条件对合成恶二唑衍生物的影响，研究了恶二唑衍生物的紫外光谱和荧光光谱性能。

Seven of them have not been reported.Their structures were confirmed by IR,~1HNMR,MS,and element analysis. 4.Meanwhile,the green methylation procedure of imides was developed by using dimethyl carbonate as methylation reagent.A series of imides,for example,phthalimide,3,4-dibromo-maleimide and succincide were used for substrates.The effects of DABCO(1,4-diazabicyclo [2.2.2]octane)and DBU(1,8-diazabicyclo[5.4.0]undec-7-ene)as a catalyst in this kind of reactions were investigated.2-Bromo-3-(1-methylindolyl-3-yl)-1-methyl-1H-pyrrole-2,5-dione was prepared by using dimethyl carbonate,which further expanded the use of dimethyl carbonate,as a green agent in organic synthesis.

在以硫酸二甲酯为甲基化试剂对3，4-二溴马来酰亚胺进行N-甲基化反应合成3，4-二溴-N-甲基马来酰亚胺的同时，以碳酸二甲酯为甲基化试剂，对3，4-二溴马来酰亚胺、邻苯二甲酰亚胺、琥珀酰亚胺等酰亚胺类化合物的N-甲基化反应进行了研究；考察了1，4-二氮杂双环[2.2.2]辛烷，1，8-二氮杂双环[5.4.0]十一碳-7-烯、碳酸钾和四丁基溴化铵等作为催化剂对碳酸二甲酯N-甲基化反应的反应时间和收率等的影响，并应用碳酸二甲酯为甲基化试剂，合成了N-甲基-3-溴-4-(1-甲基-吲哚-3)-马来酰亚胺。

There were abundant networks of NPY-Ir nerve fibers in the pial mater. It is expected that NPY released from these nerve fibers might be one source of Y〓-R ligands in SMCs, especially in the arteries under second branchs and in the arterioles.

在软脑膜中有密集的含NPY-Ir神经纤维网，所分泌的NPY可能是脑动脉（特别是第二级分支以下的小动脉和微动脉）平滑肌细胞中〓受体的配体来源之一。

The directly computed theoretical harmonic force field was scaled with a set of scaling factors transferred from related molecules to obtain a prediction of fundamental frequencies. The mean deviation between prediction and experimental IR spectrum of γ-picolinic acid in solid phase was 20cm^-^1(23cm^-^1 for in-plane modes, 11cm^-^1 for out-of-plane ones).

直接理论计算的谐性力场经由相关分子转移来的校正因子校正后，得到的振动基频的预测值和固体样品红外光谱实验值之间的平均偏差为20cm^-^1(面内振动23cm^-^1，面外振动11cm^-^1)。

The adsorption mechanism was studied by IR spectrometry, and results indicate that adsorption of picric acid is primarily physical adsorption.

通过红外光谱图，分析了聚酰胺对苦味酸的吸附机理主要属于物理吸附。

The structure of PIK-Ⅱ was characterized by FT-IR and 1H NMR.

由红外和核磁氢谱等表征了PIK-Ⅱ结构，表征结果与目标结构相吻合。

First, organic pillared montmorillonite were prepared in which three kinds of organic quaternary ammonium salts were used as pillaring agent. Physiochemical properties of organic pillared montmorillonites were characterized by XRD, FT-IR, TG-DTA. Furthermore their characters that have been testified are excellence.

首先用三种有机季胺盐作为柱撑剂制各出有机柱撑蒙脱石，并通过XRD、FT-ZR、TG-DTA等测试手段对其进行了表征，并且对制备的有机柱撑蒙脱石进行了性能测试，证明其性能优良，说明利用干法制备有机柱撑蒙脱石是切实可行的。

Layered double hydroxides pillaring with organic anion s CoAl-LDH are directly synthesized by a homogeneous precipitation method using the urea as a precipitiant,and the LDH products have been characterized through XRD,FT-IR,TGA and TEM.

以尿素为沉淀剂用均匀沉淀法直接合成有机阴离子柱撑水滑石(LayeredDoubleHydroxides，LDH)及CoAl水滑石等，并用XRD，FT-IR，TGA，TEM等分析手段对所合成的水滑石进行了表征。

In this dissertation , Physical and chemical properties of raw material was studied first, then sodium model-modification of it was researched. Next, preparation of FILM in traditional process using montmorillonite after model-modification was in research. After that, we studied the preparation of PILM in hydrothermal process using montmorillonite without being model-modified. Finally, products in experiments were characterized and Analyzed by XRD, IR, DTA.

根据目前国内外的发展现状，针对存在的问题，本课题做了以下几个方面的研究：首先对采用的基质材料的物化性进行了研究；然后研究了其钠化改型的工艺方法；接下来研究钠化后的蒙脱石用常规工艺合成PILM；在此基础上提出并研究了水热法制备PILM和其柱化剂的新工艺；最后对制备的试样通过XRD、IR、DTA等进行了分析和表征。

The short time oxidized product is insoluble in common organic solvents and water, but the water-soluble derivatives were obtained after hydrolysis under a basic condition. It′s IR spectrum is similar with that of C60 polyhydric derivatives. The extensive oxidation product of C60 is water-soluble without any further dispose.

一种产物在有机溶剂及水中均不溶，但经碱性水解后得到水溶性产物，其红外光谱与C60羟基化合物相似；在长时间通O3条件下，得到水溶性的C60氧化产物。

Nowadays, most of research are to build a transmutative Petri Nets through adding controlling place sets, controlling arc sets and controlling policy to the basic Petri Nets, while the Controlled Petri Nets could be used to argue many controlling theory problems conveniently and to induce many logically and physically supervisory and solve the Event Feedback Controlling Problems and State Feedback Controlling Problem in DEDS supervisory theory.

目前大多数的研究表现为在变形后的受控Petri网基础上，利用各种方法求得各种逻辑型、结构型控制器，解决DEDS监控理论中的事件反馈控制问题与状态反馈控制问题。

On one hand, there are discussions with the works council and union about extension of short time working up to the end of September.

一方面，有讨论，工程理事会和联盟关于延长工作时间短至9月底。