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Result:There were IR and DCI existed in the patients which appeared as the elevation of the absolute value of ISI,〔Ca2+〕t and CE-cAMP and decrease of the activity of the ion pump in the erythrocytic membrane. 15 of the 31 patients had hyperinsulinemia. The indexes mentioned above were almost the same in CHDs with hypertension and those without hypertension.

结果:CHD患者存在IR和钙离子代谢障碍,表现为ISI绝对值、红细胞总钙浓度、cAMP浓度升高和红细胞膜离子泵活性下降;31例CHD中15例(48%)有高胰岛素血症;上述指标在有、无并发高血压者间相比无显著性差异。

HPLC, IR and released〓 analysis indicated that the biodegradation products of the regeneratedcellulose films mainly contain oligosaccharides, cellobiose,glucose, arabinose,erythrose, glycerose, glycerol, and organic acid, the end products were 〓 andwater.

高效液相色谱和IR结果示出再生纤维素膜的主要降解产物为寡糖、纤维二糖、葡萄糖、阿拉伯糖、赤藓糖、甘露糖、甘油及有机酸,最终产物为二氧化碳和水。30℃时纤维素膜一个月后可以被培养基中的菌完全代谢掉。

By means of GPC,IR,GC-MS,~(13)CNMR,~1HNMR,Methylation analysisetc,structural properties of PST-1 were identified as follows:The Mwof PST-1 was 3.44×10~6 Da and its optical rotation was _D~(20)=+0.110°(c0.1, H_2O); PST-1 constituted 8 simple sugars and the molar ratio was 2,4-Dimethoxy-Mannose:Rhamnose:Ara-binose:Xylose:Galactose:D-Galacturonic acid:Mannose:D-glucuronic acid=2%:5%:24%:9%:3%:1%:46%:10%;The chief bone of PST-1 was 1,3,6-linked-β-D-Man residue and the side chains contained Furanoid and Pyranoid residues.

结合GPC、旋光度测定、IR、GC-MS、~(13)CNMR、~1HNMR、高碘酸氧化法、Smith降解以及甲基化方法等分析测试方法,得到PST-1的单糖组成及结构表征,实验结果如下:红豆杉多糖PST-1是重均分子量为3.44×10~6 Da的支链多糖,旋光度为20D=+0.110~0(c0.1,H_2O);PST-1单糖组成为:2,4-Dimethoxy-Mannose:Rhamnose:Arabinose:Xylose:Galactose:D-Galacturonic acid:Mannose:D-glucuronic acid=2%:5%:24%:9%:3%:1%:46%:10%;PST-1的骨架结构为:具有1,3,6-连接的β-D-甘露糖残基骨架,侧链分枝包括非还原末端的呋喃型α-L-阿拉伯糖残基、吡喃型α-L-阿拉伯糖残基、β-D-木糖残基、β-D-甘露糖残基、2,4-二氧甲基-β-D-甘露糖残基和α-D-葡萄糖醛酸残基;侧链的糖残基也可能存在2,5-二氧-取代呋喃型α-L-阿拉伯糖基、3-氧-取代的β-D-木糖残基、6-氧-取代的α-D-半乳糖醛酸残基、6-氧-取代的α-D-半乳糖残基、4-氧-取代的α-D-葡萄糖醛酸残基和2-氧-取代的α-L-鼠李糖残基,同时后者也可能穿插在主链上。

Nanosized CPF(Conjugated Polymer of Furfuryl alcohol)/ZnO composite catalyst was prepared through in-situ polymerization and heat conversion. The thermal stability, morphologies, size, structure and optical absorption properties of the CPF/ZnO material were characterized by TG-DTA, TEM, XRD, XPS, IR and UV-Vis techniques.

通过原位聚合-热转化两步法,利用ZnO纳米微粒和糠醇制备出了具有大共轭结构的高分子和ZnO的纳米复合催化材料;用TG-DTA、TEM、XRD、XPS、IR和UV-Vis等技术对其热稳定性、形貌、尺寸、结构及吸光特性等进行了表征,以亚甲基蓝溶液的催化降解研究了该材料在自然光条件下的催化性能。

Catalytic Synthesis of Methyl Furoate by Peroxhydrogen and Sulphate Acid;2. Using hydrochloric acid as a cheap catalyst,perfume methyl furoate was synthesized from methanol and furoic acid prepared from furfural,and was characterized by GC,IR and 1H-NMR.

从糠醛出发,由制备的糠酸和甲醇反应,在盐酸催化下,合成了香料糠酸甲酯,并用IR、1HNMR、GC等进行了表征;探讨了包括高纯度糠酸的制备在内的反应影响因素,在醇酸物质的量之比为 5∶1、催化剂体积占甲醇体积 13。

Using hydrochloric acid as a cheap catalyst,perfume methyl furoate was synthesized from methanol and furoic acid prepared from furfural,and was characterized by GC,IR and 1H-NMR.

从糠醛出发,由制备的糠酸和甲醇反应,在盐酸催化下,合成了香料糠酸甲酯,并用IR、1HNMR、GC等进行了表征;探讨了包括高纯度糠酸的制备在内的反应影响因素,在醇酸物质的量之比为 5∶1、催化剂体积占甲醇体积 13.0 %、反应时间 3h的最佳工艺条件下,酯化收率为81 0 %,收率比硫酸法、某些固体超强酸法

Synthesis of glycidol and epoxidized polyurethane and their characterization;2. Improvement in Hyperbranched Poly glycidol Hydroxyl Groups' Conversion by Protection Method;3. The structure of glycidol was confirmed by IR and 1HNMR.

以一氯代丙二醇为原料,与碱性化合物在低温作用下合成了缩水甘油,并通过IR、1HNMR对其进行了结构表征。

The improved puberty PCOS-IR rat model has following characteristic:Retained the high androgen syndrome and/or the high LH syndrome as the endocrine characteristics;Simultaneously it had sugar fat metabolism unusual, such as the insulin resistance,the redemptive high insulin blood sickness as well as cholesterol ascension.Has the abdomen obese characteristic----In particular fat pad which around reproductive organ obvious increased;The ovary increased obviously,Ovarian cortex accumulated,the number in ovary pouch expansion graafian follicle were remarkable increased, ovulation suppression.

一、改良青春期PCOS-IR大鼠模型具有以下特征:1、保留了高雄激素血症和/或高LH血症等内分泌特征;同时有胰岛素抵抗,代偿性高胰岛素血症以及总胆固醇升高的糖脂代谢异常。2、具有腹部肥胖的特征——尤其是生殖器周围脂肪垫明显增加;3、卵巢明显增大,皮质增厚,卵巢内囊性扩张卵泡数目显著增加,排卵抑制。

There is synergistic interaction maximum while the mixed ratio of KGM and Guran gum is 60/40,the total polysaccharide concentration 1%, TP 80℃ and salt ionic (Ca2+)concentration 0.1mol/L.Interraction machanism between molecules and molecules of two polysaccharide were investigated by FT-IR .

当总糖浓度为1%,魔芋胶与瓜尔豆胶的共混比例为60/40 ,制备温度为80℃,体系盐离子(Ca2+)浓度为0.1mol/L 时可得到协同相互作用的最大值,从FT-IR 谱图上分析了两种多糖分子间相互作用的机理。

The synthesized PCU was then characterized by infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, small-angle X-ray scattering, and tensile strength measurement. The IR showed that the polymer synthesized by the above two methods both have the polycarbonate-urethane structure and the tensile measurement showed good mechanical performance of the polymer. The DSC and TGA data showed that there is an obvious soft-hard glass transition area, which indicated the existence of the micro-phase separation structure. The extent of the phase separation was affected by the ratio of starting materials, the molecular weight of PCD, and the polymerization method. The decomposition upon heating was observed in two steps. SAXS result showed that the radius (r_2), the distance between domains (d_2), and gyral radius (R_2) of hard segment micro-domain were fairly affected by the starting materials ratio and soft segment content.

IR结果表明两种方法合成的聚合产物均具有聚碳酸酯聚氨酯的结构;拉伸实验表明聚合产物具有良好的力学性能;DSC、TG结果表明,聚合物呈现出较为明显的软硬段玻璃化转变区,表明存在微相分离的结构,相分离的程度受原料配比、软段分子量、聚合方法的影响,其热分解分为明显的两个阶段; SAXS结果表明,聚合物原料配比、软段含量的变化对硬段微区回旋半径R_2,微区间距d_2,微区半径r_2影响不大其值分别为9.5(A|°、29、7.4,但对软段的微区半径及间距影响较大,随着软段含量的增大,软段微区的半径r1和间距d1都增大。

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然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

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