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To optimize the compounding of the photo-sensitive resin, a novel prepolymer was synthesized and token by FT-IR. The prepolymer was an alicyclic epoxy acrylate, which was synthesized from the alicyclic epoxy resin.

为了优化光敏树脂配方，作者又合成了一种光敏树脂组分中的主体树脂并经傅立叶红外光谱表征，该树脂是以脂环族环氧树脂为原料合成的脂环族环氧丙烯酸酯。

The alkaline-earth metal complexes with mucic acid was successfully prepared via gel formation and characterized by elemental analysis,FT-IR measurements.

采用凝胶法合成了碱土金属—粘液酸配合物的晶体。

The azo derivatives were hydrolyzed on the condition of alky to get end products. The structures of azo derivatives of 4-ASA and intermediate products were characterized by melting point, TLC, MS, FT-IR, 1H-NMR and 13C-NMR spectra properties in details.

本课题探索了一条4-ASA偶氮化合物的多步合成工艺，得到了目标产物三个，对合成的目标产物和中间产物用熔点、薄层色谱法、MS、FT-IR、1H-NMR和13C-NMR进行了详细的表征，确定了它们的结构。

Rosin allyl alcohol ester was analyzed and characterized by TLC, IR and GC-MS.

利用TLC、IR和GC-MS对目标产物进行了分析和表征。

The polymer of rosin allyl alcohol ester was synthesized by microwave irradiation heating and routine heating method. The structure of the polymer was identified by IR, UV.

采用微波加热和常规加热方法聚合得到聚松香丙烯醇酯，分别对聚合物进行了红外、紫外、软化点和热失重分析。

Quinclorac and allyl alcohol as raw materials, 3, 7-dichloro-8-quinolinoxylic acid allyl ester was obtained when catalyst is oil of vitriol or super solid acid SO〓/TiO〓. Using both catalysts, organic synthesis technology process was made respectively, and the ester was analyzed and characterized by IR spectrum and NMR spectrum Through experiment, both preparing conditions were optimized and discussed respectively.

以TiO〓为载体负载SO〓制备出固体超强酸催化剂，确定了SO〓/TiO〓催化剂制备的技术路线，以丙酸正丁酯为探针实验，考察了新型固体酸催化剂SO〓/TiO〓的催化活性及制备条件对催化活性的影响，对影响其催化效果的工艺条件进行了优化，并探讨了影响的规律性。

FT-IR and curve-fitted results of amide I band are in good agreement with the analyses of CD spectra.

红外光谱定量结果表明大黄酸与人血清白蛋白结合改变了蛋白质的构象。

Using mordern physical chemistry techniques (such as XRD、 TG-DTA、 IR、 XPS and 〓Xe-NMR)、 chemical adsorption techniques (NH〓-TPD、 H〓-TPD、 TPO、 TPR etc.) and pulse flow microreaction of n-hexane、 methylcyclopentene and n-hexane containing 0.2ppm thiophene, we studied mainly the following three points:(1). the changes occured during the calcination pretreatment of Pt ammine complex supported on β and L zeolites;(2). the effect of structure and acidity-basicity of zeolite on the dispersion and electron state of Pt particles; and (3). the influence of second metal component on the reactivity of nhexane aromatization and sulphur-resistance of Pt/L zeolite catalyst. Several interesting and valuable results are obtained and summerized as follows

本论文运用各种近代物理表征方法(XRD、BET、TG-DTA、IR、XPS和〓Xe-NMR)、化学吸附技术(NH〓-TPD、H〓-TPD、TPO、TPR等)和正己烷、甲基环戊烷及含噻吩正己烷的脉冲微反等方法，着重研究了(1)载Pt的β和L沸石在分解预处理过程中发生的变化；(2)沸石载体结构及酸碱性对Pt粒子分散及电子状态的影响；(3)第二金属组份对载Pt沸石催化剂上正己烷芳构化及抗硫性能的影响等，得到了某些有意义的结果。

A novel synthetic approach of 3,3'-azobis(6-amino-1,2,4,5-tetrazine) was firstly devised. Taking 3,6-bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine as a primary material, DAAT was synthesized by high pressure ammonolysis and potassium permanganate oxidation. Compared with the four-step reaction in the literature, this new approach was reduced to two steps with a yield of 58.1%. The intermediate and DAAT were characterized by elemental analysis, IR and NMR spectra.

自行设计了3，3'-偶氮双(6-氨基-1，2，4，5-四嗪)新合成路线、采用3，5-双(3，5-二甲基吡唑-1-基)-1，2，4，5-四嗪为原料，由文献报道的4步反应缩减为2步，经高压氨解、高锰酸钾氧化合成了DAAT，总收率大幅提高，达到58.1%，并采用元素分析、红外光谱、核磁共振光谱等进行了结构表征。

Dendritic p-t-butylcalix arene amide derivatives with terminal amino groups of the first and second generations were synthesized from the ammonolysis of ethyl calixylacetate with 1, 6-diaminohexane and Michael addition of methyl acrylate. Their structures were confirmed by IR, 1H NMR.

通过扩散法，采用氨基对丙烯酸甲酯的Michael加成反应和酯基的酰胺化反应交替进行，合成了4种树枝型对叔丁基杯芳烃酰胺衍生物(n=6，8)。

You can do some assertiveness training.

你可以进行一些自信训练。

We were well on the path to making a rear-wheel-drive global platform," says Mays."

我们正致力于建立一个后轮驱动的平台，"Mays这样说道。"