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Then the aluminium sulfates were prepared by sulfation and salt formation, and their IR spectra were analyzed.

在此基础上再经硫酸酯化和成盐修饰制备了各自的硫酸酯碱式铝盐。

Then the aluminium sulfates were prepared by sulfation and salt formation, and their IR spectra were analyzed.

对制得的几种碱式铝盐进行了红外光谱分析和有机硫含量、铝含量及样品制酸力等部分理化性质的测定。

By sulfating synthesized Zr-HMS zeolite, a SO〓/Zr-HMS was prepared. It is proved that it possess superacidity by the experimental results of indicator method, NH〓-TPD, TG and IR.

硫酸化处理后制得SO〓／Zr—HMS，指示剂法测定它的酸强度大于-13.75；NH〓—TPD，TG和IR表征也证明它具有超强酸性。

The characteristics of light sulfurized and esterified castor oil ①It's shown by the IR and LC-MSD that the sulfurized castor oil esterified with acid anhydride on 12-hydroxyl forms single, di and tri-esters.

流变性能：使0.5％S、1％S、2％S和3％S轻度硫化蓖麻油的粘度从327增加到545，粘度指数从135减小到100；倾点从-25℃上升到-15℃；碘值从90.6mgI／100g减小到88.5mgI／100g，测定实际的硫含量从0.412％增到2.6％；表明不饱和程度在减小。

The synthetic product was proved by IR and MS. The translation ratio of nitrobenzene was about 90%by titrating amino group value. The selectivity of p-aminophenol was 80%.

合成产品通过IR、MS确认其结构，并通过滴定氨基值计算出硝基苯的转化率为90％左右，产品的选择性达80％。

The products were identified by IR,NMR,MS and elemental analysis. In our method,K.OH was used in place of NaOH to synthesize benzyl ester of 3,5-dimethyl-4-hydroxybenzoic acid,2',6'-dimethyl-4'-(n-succinimidyloxycarbonyl) phenyl-acridinium-9-carboxylate was purified on a silica gel column with chloroform/ethylacetate(4:l,v/v) as eluent and further purified by triturating with hexane/acetone(2:l,v/v).The luminescence produced by DMAE-NHS is a flash light with maximumemission at 0.4s and decay half-time of 0.9s. The luminescence intensity is 6.11x10 cps/mol,which is affected by the composition of trigger and surfactant.

DMAE·NHS的合成是本论文的关键和难点，我们对文献方法进行改进：文献方法用氢氧化钠与3，5-二甲基-4-羟基苯甲酸反应制得3，5-甲基-4-羟基苯甲酸钠，再用3，5-二甲基-4-羟基苯甲酸钠与苄氯作用制备3，5-二甲基-4-羟基苯甲酸苄酯，我们用氢氧化钾代替氢氧化钠，使合成取得成功；在合成2'，6'-二甲基-4'-苯基-吖啶-9-甲酸酯时，文献方法对粗产品进行两次硅胶柱层析纯化，第一次柱层析用氯仿/乙酸乙酯(4：1，Ⅴ：Ⅴ)作溶剂和淋洗剂，第二次柱层析用己烷/丙酮(2：1，Ⅴ：Ⅴ)作溶剂和淋洗剂，按照文献方法得到的不是所需要的化合物，我们只进行第一次柱层析纯化，然后用己烷/丙酮(2：1，Ⅴ：Ⅴ)进行研磨，过滤，洗涤，除去溶于己烷/丙酮(2：1，Ⅴ：Ⅴ)的部分，得到所需要的产品。

The linear range of the method was 0.002 5-0.015 μg/mL for Ir with t...

方法的线性范围为0.002 5~0.015μg/mL，检出限为6.38×10-6μg/mL。

At any relative humidity,including the one at which a given conformation is stable, three to four IR absorption bands were detected .

多肽的水合行为远比报导的复杂，在三个阶段中都不是纯单一结构组分，在任何一个RH下都存在3－4个吸收组分。

In this work, a full optimal calculation on the molecular geometry and electronic structure of C24H30O8 has been performed using density functional theory methods at B3LYP/6-31G(superscript *) level. The solvent effects of C24H30O8 have also been investigated based on Onsager self-consistent reaction field model in chloroform, acetone, DMSO and water. On the basis of optimized geometry in gas phase the vibration analysis is carried out and the IR principle peaks scaled by 0.9613 are in good agreement with experimental.

采用密度泛函理论方法，在B3LYP/6-31G水平下全优化得到了该化合物的分子几何构型和电子结构；依据Onsager自恰反应场模型考察了其在氯仿、丙酮、二甲亚砜及水等溶剂中的溶剂化作用；基于气相优化结构进行了B3LYP/6-31G振动分析，用0.9613校正后的主要红外光谱与实验符合得很好。

ResultsThe purity of compound was 98%. IR showed Naproxin was conjugated to Phaeophorbide in acid anhydride.

结果HPLC测定其纯度为98％，红外光谱显示脱镁叶绿酸和萘普生形成了酸酐交联。

Nowadays, most of research are to build a transmutative Petri Nets through adding controlling place sets, controlling arc sets and controlling policy to the basic Petri Nets, while the Controlled Petri Nets could be used to argue many controlling theory problems conveniently and to induce many logically and physically supervisory and solve the Event Feedback Controlling Problems and State Feedback Controlling Problem in DEDS supervisory theory.

目前大多数的研究表现为在变形后的受控Petri网基础上，利用各种方法求得各种逻辑型、结构型控制器，解决DEDS监控理论中的事件反馈控制问题与状态反馈控制问题。

On one hand, there are discussions with the works council and union about extension of short time working up to the end of September.

一方面，有讨论，工程理事会和联盟关于延长工作时间短至9月底。