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In the thesis, a series of novel single and multi-armed oxadiazole bridging ligands and pyridyl-4, 5-imidazole dicarboxylic acid ligands have been synthesized. The coordination chemistry of these novel ligands with transition metal ions was investigated. In addition, two 1, 3, 4-oxadiazole bridging ligands end-capped by chelating Schiff-base coordination sites have been designed and synthesized. The coordination chemistry based on one of the two ligands with metal ions was primarily investigated.

本文报道了一系列新颖的含1， 3， 4-Oxadiazole杂环的单臂及多臂有机配体，研究了它们与过渡金属离子的配位反应化学；合成了吡啶基-4，5-咪唑二羧酸有机配体，研究了它们在水热条件下与过渡金属离子的配位反应化学；另外，还合成了1， 3， 4-Oxadiazloe杂环桥联的双Schiff-base有机配体，初步探讨了其与过渡金属离子的配位反应化学。

In order to develop a liquid oxidation desulfurization technique, the characteristic of desulfurization of sodium Phosphomolybdate absorbent system was investigated by the method of dynamic tail-gas H,S concentration detection and the regeneration behavior of the same system was investigated by the method of redox poteatial detection.

以液相氧化脱硫工艺开发为目的，采用尾气H2S浓度动态监测法研究了磷钼杂多化合物脱硫体系的脱硫特性；采用氧化还原电位监测法研究了该体系的再生规律结果表明，磷钼酸钠体系的脱硫性能随温度升高而有所降低，随进气H2S浓度的提高而相应降低，随吸收剂浓度的提高而显著增强。

In this study, the antioxidant components, antioxidative activity of five species of Davalliaceae plants and two polypodiaceae plants were investigated first by microtiter spectrophotometric and fluorescent methods. Then the protective effects of these plants on 6-OHDA-induced neuronal damage in B35 cells were investigated.

本实验采用俗名为骨碎补的五种骨碎补科与两种水龙骨科之近源植物作为实验材料，进行抗氧化成分含量与活性评估，并以离体方式探讨其对6-OHDA所诱导神经细胞损伤之保护作用与机制。

In order to solve the problems of complex cellulose production process and serious pollution, The paper investigated the solubility of cotton stalk cellulose in ionic liquid N-ethyl pyridinium bromide. The structural differences between cotton stalk cellulose and cellulose regenerated from the ionic liquid were investigated using infrared spectroscopy and chemical analysis. Recovery ratio of ionic liquids was also studied.

为解决纤维素生产加工过程复杂且污染严重问题，试验探讨了棉秆纤维素在离子液体溴代N-乙基吡啶中的溶解性能，采用红外光谱等手段对棉秆纤维素在离子液体中溶解和再生前后的结构变化进行了分析，并探讨了离子液体的回收。

The preparation of avermyctin emulsions in water was achieved by mixing the surfactants polyoxyethylene (10) octylphenyl ether (OP10), polyoxyethylene styrenated phenol ether (602), and polyoxyethylene (40) castor oil ether (EL-40) with polyoxyethylene (20) castor oil ether (EL-20), separatively. Emulsion stability was investigated by analyzing the hydrophile-lipophile balance, critical micelle concentration, and surface tension. Then, the surfactants of polyoxyethylene polyoxypropylene styrenated phenol ether (1601), block copolymer (L64), and octyl phenyl polyoxyethylene phosphonate were added to the emulsion made by blending EL-40 and EL-20, separatively. The stability of the emulsions was investigated further and discussed in terms of droplet size, surface tension, and zeta potential.

首先将辛基酚聚氧乙烯醚(OP10)、苯乙烯基酚聚氧乙烯醚(602)和蓖麻油聚氧乙烯(40)醚(EL-40)分别与蓖麻油聚氧乙烯(20)醚(EL-20)复配制备阿维菌素水乳剂，从亲水亲油平衡值、临界胶束浓度、表面张力等方面分析了二元表面活性剂复配对乳液稳定性的影响；其次，在EL-40与EL-20复配基础上，将苯乙烯基酚聚氧乙烯聚氧丙烯醚(1601)，嵌段共聚物(L64)和辛基酚聚氧乙烯醚磷酸酯分别添加到乳液中，从粒径、表面张力和zeta电势等方面考察三元表面活性剂复配对乳液稳定性的影响。

Four aspects of research achievements include:(1)several imaging correction methods and strained estimation methods for biological tissues elasticity imaging were investigated as well as elasticity reconstruction and phantom, in vitro and in vivo elasticity imaging experiments;(2)in the fields of biological microsystem and perfusion evaluation for microvascular system, three kinds of microbubbles whose shell are albumin, sugar ester and surfactant respectively were designed and produced, then the methods to estimate the thickness of their shells were presented, moreover, the interacting mechanism of ultrasound contrast agents and tissues, as well as protein drug delivery under the condition of ultrasound sonification were studied in the molecular level;(3) At the aspect of high intensity focused ultrasound therapy system, we designed and constructed the 256-element HIFU transducers using 1-3 composite materials. And furthermore we developed the integrated HIFU system with 256-element HIFU transducers. And we made preliminary and important progresses in the research of HIFU bioeffect, lesion estimation, techniques of monitoring and imaging and characterizing of structure of HIFU transducer;(4)The real-time method of voice source regeneration based on compensative regulation of physiological parameters was investigated in the field of medical rehabilitation. We addressed the physiology and biophysics of vocalization, modeled voice source regeneration based on compensative regulation mechanism, and put forward an integrated evaluation about the speech rehabilitation and the regenerated voice source; Sixty-one archived journal papers were published, as well as ten in international journals, and eighteen publications were embodied by SCI.

成果包括：（1）在生物组织弹性成像方面，研究了多种图像校正方法和应变估计方法，进行了弹性重构和仿体、离体及在体超声弹性成像实验研究；（2）在生物微系统和微血管血流灌注成像方面，制备了三种不同包膜超声造影微泡，研究了纳米包膜厚度检测与估计方法以及不同纳米包膜造影微泡断裂与药物释放机制，并在分子层次上开展了超声与生物组织相互作用机制以及蛋白质药物超声乳化微囊包裹的研究；（3）在阵列式高强聚焦超声治疗与监控成像技术方面，设计制作了新的HIFU换能器，解决了256阵元单焦点和多焦点合成HIFU治疗系统关键技术问题，并在HIFU生物效应与创伤性评价方法、HIFU过程监控成像技术和薄层复合结构与HIFU 换能器界面特性评价等方面的研究取得了初步而重要的进展，具有重要应用前景；（4）在语音听觉系统特别是嗓音康复方面，研究了基于发声系统补偿调节机制的实时多模式嗓音源再生方法和发声生理，建立基于神经、肌肉和空气动力系统的综合补偿调节模型，提出了相应的评价系统。

Four aspects of research achievements include:(1)several imaging correction methods and strained estimation methods for biological tissues elasticity imaging were investigated as well as elasticity reconstruction and phantom, in vitro and in vivo elasticity imaging experiments;(2)in the fields of biological microsystem and perfusion evaluation for microvascular system, three kinds of microbubbles whose shell are albumin, sugar ester and surfactant respectively were designed and produced, then the methods to estimate the thickness of their shells were presented, moreover, the interacting mechanism of ultrasound contrast agents and tissues, as well as protein drug delivery under the condition of ultrasound sonification were studied in the molecular level;(3) At the aspect of high intensity focused ultrasound therapy system, we designed and constructed the 256-element HIFU transducers using 1-3 composite materials. And furthermore we developed the integrated HIFU system with 256-element HIFU transducers. And we made preliminary and important progresses in the research of HIFU bioeffect, lesion estimation, techniques of monitoring and imaging and characterizing of structure of HIFU transducer;(4)The real-time method of voice source regeneration based on compensative regulation of physiological parameters was investigated in the field of medical rehabilitation. We addressed the physiology and biophysics of vocalization, modeled voice source regeneration based on compensative regulation mechanism, and put forward an integrated evaluation about the speech rehabilitation and the regenerated voice source; Sixty-one archived journal papers were published, as well as ten in international journals, and eighteen publications were embodied by SCI.

中文摘要：成果包括：（1）在生物组织弹性成像方面，研究了多种图像校正方法和应变估计方法，进行了弹性重构和仿体、离体及在体超声弹性成像实验研究；（2）在生物微系统和微血管血流灌注成像方面，制备了三种不同包膜超声造影微泡，研究了纳米包膜厚度检测与估计方法以及不同纳米包膜造影微泡断裂与药物释放机制，并在分子层次上开展了超声与生物组织相互作用机制以及蛋白质药物超声乳化微囊包裹的研究；（3）在阵列式高强聚焦超声治疗与监控成像技术方面，设计制作了新的HIFU换能器，解决了256阵元单焦点和多焦点合成HIFU治疗系统关键技术问题，并在HIFU生物效应与创伤性评价方法、HIFU过程监控成像技术和薄层复合结构与HIFU 换能器界面特性评价等方面的研究取得了初步而重要的进展，具有重要应用前景；（4）在语音听觉系统特别是嗓音康复方面，研究了基于发声系统补偿调节机制的实时多模式嗓音源再生方法和发声生理，建立基于神经、肌肉和空气动力系统的综合补偿调节模型，提出了相应的评价系统。

The effect of characteristics, including concentration and flow velocity of absorbent and feeding gas, on the CO_2 absorption process has been widely investigated. And the active materials of different concentration, including Potassium phosphate tribasic、 Potassium tetraborate、 N-methyldiethanolamine、 2-Amido-2-methyl-l-propylacohol and Piperazine, were added in the absorbent, of which the effect has also been investigated.

主要考察了气液流速及其浓度等操作参数对CO_2吸收性能的影响；同时研究了在氨基酸盐吸收剂中添加各种活化剂，包括磷酸钾、硼酸钾、N-甲基二乙醇胺、2-氨基-2-甲基-1-丙醇和哌嗪对CO_2分离效果的影响；并对膜组件运行的稳定性进行了初步考察。

The separation performance of these membranes for thiophenic sulfurs from n-hexane was evaluated. The competitive adsorption of thiophenic sulfurs on these membranes was investigated by varying the loaded ions, the ion concentration and the activation temperature. The regeneration of used membranes was also investigated.

所制得的膜经过负载金属离子改性后用于模拟汽油中噻吩类二元硫化物的分离，研究了不同负载离子种类、负载离子浓度和活化温度对二元硫化物竞争吸附的影响，同时还考察了膜的再生效果。

The experimental results show the validness of the mechanism analyses.2. According to the generation mechanism of the leak acoustic signal, the characteristics of the leak acoustic signal are investigated. The auto correlation technology is adopted to descript the leak signal characteristics due to the ability to analyze the coherence of time series. A new procedure to identify the leak acoustic signal from the disturbed noises is proposed based on the conjunction of correlation and approximate entropy algorithm.3. The principle and application in leak location of the correlation and the adaptive filter techniques are introduced. The problems of the traditional leak location methods are analyzed.4. In order to establish the leak detection signal model, the leak acoustic propagation characteristics are investigated experimentally.

从泄漏声产生机理出发，分析了管道泄漏处湍流拟序结构与空泡间相互作用的机理，认为在该机理作用下，泄漏声信号产生过程具有&不可重复&的特征；由于相关函数具有分析时间序列拟序结构的能力，且近似熵从统计的角度区别时间过程的复杂性，因此，提出将信号相关分析和近似熵理论相结合的方法，提取泄漏声信号&不可重复&的特征，辨识管道泄漏故障发生；在实际检测现场，由于各种管内和管外固定声源噪声(如阀门噪声、工地施工噪声等)常导致泄漏误判和漏点定位错误，重点分析了管内固定噪声源的产生机理和特征，为复杂干扰环境下的泄漏辨识提供理论支持。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了