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Two synthetic routes of Caffeine have been determined and investigated after the analyzing and trying for the literal synthetic methods. In one route, the target compound was prepared from chloroacetyl chloride through six steps, the total yield is 50.5 %. In another route, the target compound was obtained from cyanoacetic acid through six steps, the total yield is 45%.
对目前咖啡因工业生产工艺进行了研究,并分析了咖啡因工业生产中所存在的问题,本文提出两条可行的工业化合成路线:一条是以氯乙酰氯为起始原料,经过六步反应制得目标化合物,总收率50.5%;另一条是以氰基乙酸为起始原料经过六步反应制得目标化合物,总收率45%。
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In order to develop antibacterial peptide biologics for prevention and control of endometritis of dairy cow,a pair of primers was designed and synthesized according to the sequence of bovine antibacterial peptide gene published in GenBank.The total RNA was purified from the dairy cow endometrial cells with the Total RNA Isolation Kit.
为研发防治乳牛子宫内膜炎的抗菌肽生物制剂,根据已发表的牛抗菌肽基因序列设计了1对引物,用试剂盒提取乳牛新鲜子宫内膜总RNA,经RT-PCR扩增,将克隆的抗菌肽BNBD5基因全长编码区的cDNA连接到原核表达载体pET30a中,经IPTG诱导原核表达,通过Western-blot检测融合蛋白BNBD5的表达水平。
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The P. flagellaria clonal population distributing in the Songnen grassland was studied,and we observed the season dynamics of petiole length and the total stolon length as well as pattern of spacer length,compared the numbers of maternal ramets,daughter ramets and single ramets as well as the yearly dynamics of total biomass in 3 years (2003,2005,and 2006). Furthermore,we analyzed the correlation between population quantative character and the community's quantative character.
以松嫩草地羊草草甸内分布的蔓委陵菜无性系种群为研究对象,观测了叶柄长度、匍匐茎总长度的季节动态以及间隔子长度分布格局,比较了3个年份(2003、2005、2006年)的种群母株数、分株数、独立株数和总生物量年间动态,分析了种群数量特征与其所分布的群落的数量特征之间的相关关系。
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In order to decide picking period of leaves of indocalamus as well as reasonably utilize them, the contents of glucide , proteit, total flavonoids, total lactones and metal elements in leaves of Indocalamus latifolius, Indocalamus tessellates and Indocalamus guangdongensis var.
为确定箬叶的适宜采摘期和有效开发利用箬叶资源,分别测定阔叶箬竹叶、箬竹叶、柔毛箬竹叶冬季和夏季、不同生长土壤环境下的糖类、蛋白质、总黄酮、总内酯和金属元素含量。
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Another result of the study is that the total rate of entering a higher school is 74 percent, 69 percent, and 86 percent. For educational opportunities, the second group is most unequal when the rate of entering a higher school increases up by 50 percent. Through the analysis of logical regression beta b, the change in the inequality of opportunities of years of education in Taiwan is mainly influenced by various sharp structures of a total rate of entering a higher school, and not by the inequality of educational resources. When the rate of entering higher school is nearly 50 percent, the opportunity of years of education is most inequal.
本研究进一步分析各年代的整体国中后升学机率,分别为74%,69%,86%,以第二组年代的升学机率最接近50%,教育机会也最不均等;而根据逻辑回归系数 b 值的分析结果,发现台湾地区民众教育资源分配之不平等性并没有明显一致的变化趋势,前述受教育年数的机会不平等性之变迁,并非受教育资源分配不平等性的影响,而主要受到整体升学率不同的钜视结构影响,在升学率最接近50%时,受教育年数的教育机会最不均等。
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JEYS has litholytic effect in vitro; JEYS has choleretic effect and could decrease Ca2+, total bilirubin, and total cholesterol in biles.
中药复方JEYS有体外溶解胆结石的作用,有利胆和降低胆汁中钙离子、总胆红素和总胆固醇的作用。
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Results The results showed that the total cantharidin contents in the samples of Meloidae were 1 to 9 times the free cantharidin contents. The total cantharidin contents were generally higher than 2.0% of dry body weight and the free cantharidin contents were all less than 1.7% of dry body weight in Mcloidac.
芫菁体内总斑蝥素的含量为游离斑蝥素含量的1-9倍,总斑蝥素的含量一般多于虫体干重的2.0%,而游离斑蝥素的含量均低于虫体干重的1.7%。
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Abstract] Objective To evaluate the advantages of laparoscopic total mesorectal excision in the treatment of rectal cancer.Methods Procedure of laparoscopic total mesorectal excision were performed in 8 patients with rectal cancer.
摘要] 目的评价腹腔镜下直肠癌根治术的优越性方法在腹腔镜下对8例直肠癌实行全系膜切除术并对手术方法和临床效果进行分析。
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The total scores and anxiety and happin ess satisfaction subscale of PHSS in the male middle school students of the Han nationality group was significant higher than that of the Zang nationality group .The total scores,intellect and school state and physical appearance subscale of PHSA in the female middle school students of the Zang nationalty group were sig n ificant lower than that of the Han nationality group.
汉族男性中学生的PHSS总分及焦虑分量、幸福与满足分量表明显高于藏族组,2组其余各分量表比较统计学上无显著性差异;藏簇女性中学生的PHSS总分及智力与学校情况分量表,躯体、外貌分量表均明显低于汉族组(P.05),2组其余各分量表比较在统计学上无显著性差异。
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The results show that all aluminum anodizing sludges were slightly neutral to acidic and mainly consist of more than 50% Al2O3; the similar total contents of Cu, Pb, Zn, Ni, Cd, and Cr in the 7 samples were found, namely, the concentrations of Pb, Cd were relatively lower, but that of Cu, Zn, Ni, and Cr were higher; the leaching tests indicate that all the samples were classed as nonhazardous wastes; but each of metals in the sample shows very different leaching behavior, possibly depending on their total contents and the final pH of leachates.
结果表明,铝型材污泥属于中性偏酸性物质,主要由Al2O3组成,含量在50%以上。各试样中Cu、Pb、Zn、Ni、Cd及Cr的总含量的分布趋势基本是一致的,其中Pb、Cd的含量较低,Cu、Zn、Ni及 Cr的含量较高。浸出毒性试验表明铝型材污泥属于非危险废物,但污泥中各重金属的浸出特性又各自不同,可能主要与它们在试样中的总含量和浸出液的最终pH值有关。
- 推荐网络例句
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This one mode pays close attention to network credence foundation of the businessman very much.
这一模式非常关注商人的网络信用基础。
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Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.
扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。
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There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.
双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。