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Synthesis of Antidote of N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane BI Hong-mei, ZHANG Jin-yan, LIANG Ying, SHEN Yong (College of Arts and Sciences Heilongjiang August First Reclamation University, Daqing 163319, Heilongjiang, China) Abstract: N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane was synthesized by one pot method with isopropanolamine, cyclopentanone and dichloroacetyl chloride. The optimum reaction conditions obtained are as follows:the proportion in moles of the above materials is 1∶1∶1.2, reaction solvent is toluene, reaction temperature is -15 to -10 ℃,reaction time is 3 h, under the optimum condition, the yield of the compound is 50.0%.

除草剂解毒剂N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷的合成毕洪梅，张金艳，梁英，沈勇(黑龙江八一农垦大学文理学院，黑龙江大庆 163319)摘要：以33%的氢氧化钠水溶液为缚酸剂，异丙醇胺、环戊酮和二氯乙酰氯为原料，采用&一锅法&合成了N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷，采用正交实验法得到最佳反应条件：反应原料摩尔比为1∶1∶1.2，苯作溶剂，反应的温度为-15 ℃~-10 ℃，搅拌时间为3 h，产率达到50.0%。

Gimelbrant et al. determined the proportion of human genes that can be expressed monoallelically, in patterns that are epigenetically stable (for example, chemical modifications of DNA, such as cytosine methylation, that do not alter the sequence but are heritable within cell populations).

Gimelbrant等确定部分人类基因，能够单等位基因性表达，在表达模式上，后生同类物稳定（例如，化学修饰的DNA ，如胞嘧啶甲基化，不改变序列，但内细胞群是可遗传的）。

Although a substantial proportion of cancers currently regarded as of primary ovarian origin arise in the fimbriated end of the fallopian tube, this site cannot account for all of these tumours, some of which are most likely derived from components of the secondary Mullerian system.

虽然当前认为的原发性卵巢肿瘤很大比例出现在输卵管伞部，该部位不能解释全部肿瘤，一些肿瘤更可能来自第二苗勒系统的成分。

Keratin, due to its high proportion of valuable protein, could be used e.g. as a nutrition in feed.

角蛋白因其含有较高的有利用价值的蛋白，可以增加食物中的营养。

The experiment result shows that favorable colour development performance can be achieved for the adhesive with polyvinyl alcohol as major component and the waterproof quality can be improved when the carboxyl tetraphene latices was mixed into the adhesive in a certain proportion.

实验发现，使用聚乙烯醇为主体的胶粘剂可使热敏纸获得良好的发色性能，胶粘剂中混入一定比例的羧基丁苯类胶乳可以使热敏纸的防水性能得到改善。

The results are as follows: The present proportion of ledum palustre in the forest area is 74863 hectare; the leaves which can be picked is 1125Kg per hectare and 841796 tons per year; the ledum palustre oil which can be extracted is 4208.98 tons per year due to the lowest oil producing rate (0.5%).

其结果如下：林区现有杜香林面积 74863 公顷；根据每年再生可利用蓄积测算，每公顷可采杜香叶径 1125 公斤，每年可采杜香叶径 841796 吨；以最低出油率 0.5%计算，每年可提炼杜香油 4208.98%吨。

Serum creatinine elevations were noted in a proportion of patients, most of whom also had multiple risk factors for renal damage such as concomitant use of nephrotoxic immunosuppressants.

血清肌苷酸上升在一部分患者身上被注意到，他们中的大多数对于肾脏损害有成倍的风险例如对于损害肾脏的免疫抑制剂伴随物的使用。

In the experiments, some facters such as the proportion of tetraethyl orthosilicate to coupling agents and distilled water to tetraethyl orthosilicate,the concentration of ammonia,reaction time and reaction temperature were controlled.

研究了正硅酸乙酯与偶联剂的比例、水硅比、氨水用量、反应温度与反应时间等因素对包覆效果的影响，其中重点讨论了偶联剂的添加方式对成膜效果的影响。

The sol-gel solution was prepared by mixing ethyl orthosilicate, absolute alcohol and 0.1molL^(-1) HCl in a definite proportion, and adding an appropriate amount of silicotungstic acid as active material, strring for 30min and then standing for 24h at room temperature.

溶胶－凝胶溶液系将正硅酸乙酯、无水乙醇及0.1molL^(-1)盐酸按一定比例混合后加适量的硅钨酸作为活性物质，搅拌30min混匀后在室温放置24h配成。

An inorganic acid, such as perchloric acid, containing the largest proportion of oxygen in a series of related acids.

一种无机酸，如各种相关酸中含氧量最大的酸

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。