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The invention relates to a preparation process for synthesizing polyethylene terephthalate 1, 3- terephthalate catalyst, which comprises adding titanic acid ester, germanium compounds and cobalt compound into liquid dispersed phase of organic solution, wherein the total weight concentration is 4-10%, and preparing the catalyst through mechanical stirring or ultrasonic wave mixed ligand for 10-60 minutes in 0-120 DEG C, wherein the adding content of titanic acid ester, germanium compounds and cobalt compound are respectively 200-500ppm, 50-300ppm and 100-400ppm of reaction monomer mass of terephthalic acid or dimethyl terephthalate.

本发明涉及一种合成聚对苯二甲酸1，3-丙二醇酯催化剂的制备方法，将钛酸酯、锗化合物和钴化合物加入到有机溶剂的液体分散相中，总重量浓度为4～10％，在0-120℃通过机械搅拌或超声波混配10-60min制得；钛酸酯、锗化合物和钴化合物加入量分别是对苯二甲酸或对苯二甲酸二甲酯反应单体质量的200-500ppm、50-300ppm、100-400ppm；用此催化剂制备PTT产品，酯化和缩聚反应时间相对于单独使用钛酸四丁酯缩短了30-60min，产品特性粘数0.70-1.05dL/g，色相b值在2-6之间，切片可用于加工新型合成纤维及工程塑料产品。

In accordance with the needs for preparation against war, China has identified cities and regions for the conduct of civil air defense, and urban civil air ''.

中国根据战备需要，确定开展人民防空工作的城市和地区，把城市人民防空作为人民防空的重点。

In this paper, the SOL-GEL method for growing ZrO2 film is studied. The composition, structure and electric features of Zirconium Oxide are analyzed. These are all the preparation work for studying MFIS FET.

文中研究了运用SOL-GEL方法制备ZrO2介质层的方法，并且对制备的介质层的成份、结构、电特性进行了分析，为研制MFIS作了准备。

Zeolite Y sieves are used for preparation of ECL sensor for the first time by immobilizing tris (2, 2'-bipyridyl) ruthenium Ru (bpy 〓 in their supercages, which is achieved through the ion exchange properties of the sieves.

Ru〓固定于分子筛修饰碳糊电极的电化学发光与可更新无试剂海洛因传感器研究制备了一种能简单、快速、灵敏地测定海洛因的电化学发光传感器。

The results indicate that polyborazine precursor prepared at 150℃ for 10 h and propylamine/isopropylamine molar ratio 2:1, could possess nearly linear molecule skeleton and he prone to melt spinnability. When melt at 90℃, the precursor fibers are prepared with average diameter 10-20μm and BC1.27 N1.52 H structure. After curing process and sintered in NH3 at 1200℃, the near-stoichiometric BN fibers was obtained, which proved this precursor is apt for preparation of BN fibers.

结果表明，当正丙胺／异丙胺摩尔比为2：1，聚合温度为150℃，反应时间为10h时，合成产物具有近似线性分子结构，熔点为90℃，具有良好的成丝性，可获得平均直径10~20μm，组成为BC1.27N1.52H的先驱体纤维，先驱体纤维再经不熔化处理及1200℃氨气高温锻烧等工艺可获得近化学计量比的氮化硼纤维。

Many methods for sample preparation have been applied in stable isotope measurements of ostracode shells from lake sediments. However, for stable isotope measurements of biocarbonate samples, different methods will probably affect the resolution, reproducibility and inter-laboratory comparison of the measurement results.

由于湖泊生物碳酸盐样品不同的前处理方法可能会影响到稳定同位素测试结果的重现性和辨析率以及实验室之间数据的可比性，采用有效的方法对介形虫壳体进行预处理是保证介壳稳定同位素刚试的一个关键环节。

OBJECTIVE:To optimize the extraction process for the preparation of Paeonia lactiflora formula granules and establish an HPLC method for the determination of Paeoniflorin in the samples.

目的：优化白芍配方颗粒的制备工艺，建立其中芍药苷的含量测定方法。

A new approach for preparation of open tubular capillary column coated with zirconium phosphonate for isolating phosphopeptides is described in this paper.

本课题发展的方法为一种利用键合磷酸锆开管毛细管柱的制备及用于快速富集磷酸肽的新方法。

Calcium montmorillonite was prepared by purifying LeXi bentonite with wet method two times. After purification, sodium modification of Ca-M was studied. A series of Fe/Cr-pillared montmorillonites were prepared with conventional method using sodium montmorillonite as experimental materials, and synthesis condition of Fe/Cr-PILM was studied and optimized. In order to shorten the preparation cycle of PILM by overleaping the step of sodium modification of Ca-M, the pretreatment technique for Ca-M has been pointed out for the first time. A series of PILMs were prepared with hydrothermal method using pretreated Ca-M as starting materials, which show that pretreatment of Ca-M is feasible.

然后，本文以莱西膨润土为原料，用二次湿法提纯了-2μm的钙基蒙脱石，对其进行了钠化改型研究；以改型后的钠基蒙脱石为原料，新型的铁、铬复合离子为柱化剂，研究并优化了常规离子交换法制备PILM的工艺；为了简化PILM的制备工艺，我们首次提出了蒙脱石的预处理工艺，希望通过预处理后可以省去蒙脱石的钠化工艺，以Ca-M为原料直接合成PILM。

For the first time we synthesized nanoscale metal hydrides of lanthanum, neodymium, samarium, dysprosium, and ytterbium with high efficiency under mild condition by complexometric catalysis instead of traditional preparation at high temperature and high pressure. It is for the first time that we synthesized lanthanide organic compounds with catalysts or initiating agents at atmosphere and ambient temperature,and some of them are new compounds. Nanometric lanthanide metal powders are prepared by thermal decomposition of the compounds in vacuum. Differently from the traditional method, size of the products prepared by our method is less than 40nm, and the activity of the reaction is very high. They are pyrophoric at atmosphere. They can make some reactions without activity or low activity show extremely high activity .We investigated influent regulations of methods, conditions to scale and special surface.

我们首次成功地用络合催化等方法取代需在高温高压下进行的传统方法，在温和条件下高效率地合成出纳米尺寸镧、钕、钐、镝、镱的金属氢化物；首次在常压常温的条件下，通过催化、引发等方法合成镧系金属有机化合物，再将其真空热分解成功地制备了纳米尺寸的镧、钕、钐、镝、镱等金属粉末；与传统方法不同，这些方法得到的产品基本颗粒尺寸小于 40 nm，遇到空气燃烧，具有极高的化学反应活性，使原来活性很低甚至观察不到活性的反应大幅度提高反应速率和产率；考察了制备方法、制备条件等因素对晶粒尺寸、比表面积大小等的影响规律。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。