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Ti-Si composite materials are mixed at atomic scale, and Ti-O-Si bond appears in all of the samples with different TiO2 content; the mixed oxides are mainly existed in the form of amorphous pattern, anatase appears when the TiO2 content is more than 80%, but compared with the intension of pure TiO2, it has not integrate structure. The acetic content has great influence in the specific area and crystal structure of the mixed oxides. 20TiSi has good heat stability, still possesses 11m2/g after calcined at 1100℃; calcinations on the large scale of temperature does not cause the break of Ti-O-Si bond, TiO2 is well dispersed in 20TiSi calcined at 1100℃, and it still existed in the form of amorphous.

结果表明：制得的Ti-Si复合氧化物具有很高的比表面积，在TiO_2含量为10％时达到681.5m~2／g，Ti原子进入Si-O四面体结构中，形成Si-O-Ti键，复合氧化物的稳定性好，当TiO_2含量低于60 wt％时，以无定型形式存在；当含量为80％时，出现锐钛矿型TiO_2，但与纯TiO_2相比晶型不完整：醋酸对Ti-Si复合氧化物的比表面积、晶型都有很大的影响；TiO_2含量为20％的20TiSi经1100℃高温焙烧后，仍有较高的比表面积(11m~2／g)，稳定性好，在较宽的温度范围内焙烧，没有引起Ti-O-Si键的断裂，分散度高，没有出现晶型TiO_2。

Its bonding characterization and stability are discussed. The results show that these complexes are covalence complexes and that both the in-plane σ-bond and the in-plane π-bond in these complexes play an important role. The ESR spectra of VO -Ser system, VO -Ser-Phen system and VO -Ser-Bipy system in binary solvent glycol/water (V/V=1: 1) solution at various acidities (pH=1～14) have been observed at low temperature. It is found that in different pH ranges different structural complexes are formed.

测定了五种氨基酸席夫碱铜配合物的室温多晶粉末ESR谱、在不同溶剂中的室温及低温溶液ESR谱，确定配合物的配位环境；对室温溶液谱中观察到的二级效应和驰豫效应给予了理论解释、计算了驰豫参数；根据低温ESR波谱，计算了配合物的成键特性及稳定性，发现此类配合物为共价型配合物，平面内σ配键和平面内π配键均起重要作用。

The monosaccharides in LBP-4 identified by GC were xylose , galactose , mannose , Rhamnose , glucose and arabinose with the molar ratio of 4. 45: 1. 20: 1. 0: 0.98: 0.90: 0.85. The content of calcium, magnesium, zinc and iron in LBP-4a were 127. 9070mg·g〓, 32. 3953mg·g〓, 0.3845mg·g〓 and 0.2930mg·g〓, respectively. The content of galacturnic acid in LBP-4a was 55. 45% while the content of protein is 3. 80%. According to IR spectra, it contains -COOH group,-NH- roup,-OH group,-NH〓 group and β-D-glucose. The backbone of sugar residues chain in LBP-4a were contained 1→6 indican bond according to periodate oxidation and the results of β-elimination reaction indicated that the chain of polysaccharides and protein were connected by O-linked chemical bond. The photograph of LBP-4a got by laser scanning confocal microscope and scanning electron microscope showed that the LBP-4a combined both with each other and with itself in its crystalloid. The crystalloid was flake and anisotropic.

由LBP-4a的红外光谱图知：LBP-4a中含有-COOH、-OH和-NH〓或-NH-基团，糖链中含有β-D-吡喃葡萄糖；高碘酸氧化实验知LBP-4a糖链中不具有连二羟基和连三羟基结构的单糖残基：具有连二羟基结构的单糖残基：具有连三羟基结构的单糖残基=57.0：16.2：1，六碳糖残基的连接中含有1→6连接的糖苷键；通过β消去反应证明LBP-4a中多糖链和氨基酸间为-O-型连接；由激光扫描共聚焦显微镜和扫描电镜对LBP-4a结晶观察结果推测：LBP-4a结晶中同时存在分子间和分子内结合的现象，LBP-4a分子相互结合时，并不是无规则的相互缠绕形成无规线团结构，而是形成片层结构，并且LBP-4a结晶可能具有各向异性的性质。

With the self-emulsifying aqueous polyurethane containing polymeric double bond in the lateral chain acted as macromolecular emulsor and reactant for acrylate monomer polymerization, controlling the reaction amount of polymeric double bond so that adjusting the chemical bond linkage degree between polyurethane and acrylate, core-shell type interpenetrating polymer network structural aqueous acrylate polyurethane hybrid dispersion was synthesized, which is now a new type molecular composite technology for aqueous polyurethane.

利用侧链含可聚双键的自乳化聚氨酯水分散体作为丙烯酸酯单体聚合反应的高分子乳化剂和反应物，通过控制聚氨酯水分散体侧链上参与共聚的双键数目，调节聚氨酯和丙烯酸酯的化学键合程度，制备得到核壳型互穿网络结构丙烯酸聚氨酯杂合水分散体是一种新颖的复合改性技术。

After heat treatment at 1100C in air, the elements of the substrate and the bond coat diffuse and the diffusion of Ni is an uphill diffusion. The layer of r " phase and the layer of A12O3 or NiAl2O4 were formed at the interface of the substrate and the bond coat and at the interface of the bond/top coat, respectively. The thickness of the r " phase and the oxide layer increases with the increase of the time of the heat treatment.

经1100℃热处理，基体和底层中元素发生了相互扩散，并在界面析出γ'相，γ'的存在使界面的结合为冶金结合；在底层／面层界面由于底层被氧化和Al与ZrO_2氧化还原反应形成Al_2O_3等氧化物，Y'和氧化物的厚度随热处理时间延长而增加。

The study showed that interaction of co-carbonization of coal tar pitch and lean coal was the coaction of physical bond and chemical interaction, in which the bond state of coke interface was improved by physical bond, and coal tar pitch varied the carbonization behavior of lean coal through chemical interaction with the increase of the blending ratio of coal tar pitch, the caking property of coal blend was greatly improved, OTI value of coke was increased, while ISO value was reduced.

其中物理融合表现在使焦炭界面结合状态改善，化学相互作用表现在煤沥青使贫煤的炭化性能发生变化。随煤沥青配比的增加，配煤黏结性有较大改善，焦炭OTI值增大，ISO值减小。

The quantitative relationship between isomer shift, refractive index and chemical bond parameters were established. The calculated results indicated that the change of crystal parameters and bond length will alter the covalency of chemical bond and peripheral electron density of Fe2+ nuclear, which in turn leads to the change of the isomer shift and refractive index.

根据计算结果发现，晶胞参数及化学键长的变化引起化学键共价性、Fe2+核附近电子云密度的变化等，最终导致同质异能位移的改变，计算结果与实验数据之间较好的一致性验证了此理论的准确性和普适性。

China Government Bond Depository Trust and Clearing Co., Ltd (hereinafter referred to as the CDC) provides DVP settlement services for participants in the inter-bank bond market through the Central Bond Business System (hereinafter referred to as the Bookkeeping System) and the PBC's Large-Value Payment System (hereinafter refers to the Payment System).

二、中央国债登记结算有限责任公司通过中央债券综合业务系统和中国人民银行大额支付系统的连接，为银行间债券市场参与者提供券款对付结算服务。

Theoretical calculations on a series of N-H…O=C hydrogen bond trimers were carried out using the MP2 method. We investigated the effect of substituents in hydrogen bond donor molecules on their hydrogen bond strength.

使用MP2方法研究了氢键三聚体中N-H…O=C氢键强度，探讨了氢键受体分子中不同取代基对N-H…O=C氢键强度的影响。

Junk Bond A bond that is rated by a ratings agency as being below investment grade and investment in the bond is high risk.

垃圾债券被信用级别评定机构评定为低于投资级别的投资风险高的债券。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。