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The Suzuki reaction, the coupling of organoborate compounds with organic electrophiles catalyzed by Palladium complexes, is a valuable Csp2-Csp bond forming reaction. The reaction has been drawing increased attention in that the reaction permit the use of organoboron compounds that are thermally stable and inert to water and oxygen.In this section microwave promoted Suzuki reaction of phenylboronic acid with benzyl halides catalyzed by Pd(PPh3)2Cl2 DMF/H2O(v/v=10 : 2) was first reported.

第四章:微波辐射下Pd配合物催化端烯与芳卤偶联反应研究本章中我们在微波辐射条件下,研究了PdclZ(P Ph3):催化端烯与芳卤的偶联反应,合成出了七种乙烯基化合物;并分别考察了微波辐射功率、辐射时间、原料配比、和PTc等因素对反应的影响,优选出了较佳的反应条件,并根据文献及实验结果,讨论了可能的反应机理。

Four phenylalanine derivatives were synthesized with this approach. The condition of the condensation reaction was optimized. The side reaction of the Curtius reaction was studied and a urine by-product was isolated and characterized.b. Through the detailed study of the behavior of various N-acetyl phenylalanine methyl esters under the condition of the Bischler-Napieralski reaction, it was found for the first time that the formation of benzyl oxazole derivatives was a competitive approach with the normal B-N reaction.

一、基于Bischler-Napieralski反应设计了以苯丙氨酸衍生物为原料的路线,在这条路线的研究中,主要取得了以下结果:、建立了一条以芳香醛和丙二酸单甲酯为原料,通过缩合、氢化、Curtius等反应制备苯丙氨酸甲酯的通用合成路线,对其中的缩合反应条件及Curtius反应中的副反应进行了深入的研究,利用这条路线合成了四个芳环取代的苯丙氨酸单甲酯衍生物。

The side reaction of the Curtius reaction was studied and a urine by-product was isolated and characterized.b. Through the detailed study of the behavior of various N-acetyl phenylalanine methyl esters under the condition of the Bischler-Napieralski reaction, it was found for the first time that the formation of benzyl oxazole derivatives was a competitive approach with the normal B-N reaction. A convincing mechanism was suggested and a rule governing the reaction was summarized.c.

一、基于Bischler-Napieralski反应设计了以苯丙氨酸衍生物为原料的路线,在这条路线的研究中,主要取得了以下结果:、建立了一条以芳香醛和丙二酸单甲酯为原料,通过缩合、氢化、Curtius等反应制备苯丙氨酸甲酯的通用合成路线,对其中的缩合反应条件及Curtius反应中的副反应进行了深入的研究,利用这条路线合成了四个芳环取代的苯丙氨酸单甲酯衍生物。

The results show that:First, concentration of hydrogen peroxide have the most obvious influence to oil yield and carbon black yield,with the increase of concentration of hydrogen peroxide the oil yield first increase then decrease,when concentration of hydrogen peroxide is 8.19% or so,the oil yield reach to the biggest value, and with the increase of concentration of hydrogen peroxide carbon black yield decrese;Then,reaction time have more obvious influence to oil yield and carbon black yield,oil yield increase but carbon black yield decrease with the increase of reaction time;Thirdly,reaction tempreture have some influence to oil yield and carbon black yield,samely,oil yield increase but carbon black yield decrease with the increase of reaction tempreture;Finally,reaction pressure does almost no influence on oil yield and carbon black yield.

研究结果表明:过氧化氢质量浓度对产油率和炭黑产率的影响最为显著,产油率随过氧化氢质量浓度的提高先提高后降低,在过氧化氢质量浓度为8.19%左右时达到最大值,炭黑产率随过氧化氢质量浓度的提高而降低;反应时间对产油率和炭黑产率的影响也比较显著,产油率随反应时间的增加而提高,炭黑产率随反应时间的增加而降低;反应温度对产油率和炭黑产率也有一定的影响,产油率随反应温度的提高而相应地提高,炭黑产率随反应温度的提高而降低;在本文实验范围内,反应压力对产油率和炭黑产率基本上没有影响。

In this paper, firstly using natural fatty acids including lauric acid, myristic acid, palmitic acid etc. and disproportionated rosin as starting materials, the acyl reaction of starting materials with SOCl_2 respectively, and then using Schotten-Baumann condensation: on the reaction conditions of alkalescence, condensation of acylchloride with amino acid (sarcosine, glycine, alanine etc.), and then acidification, saltation. A series of anionic surfactants of N-acyl amino: sodium N-fatty acyl sarcosinate (SFS-12, SFS-14, SFS-16); sodiun N-fatty acyl glycinate(SFG-12, SFG-14, SFG-16); sodium N-fatty acyl alaninate(SFA-12, SFA-14, SFA-16)and sodium N-disproportionated rosinoyl aminatewere prepared. During the preparation of N-acylamino acid, the reaction conditions of acylchloride with amino acid condensation were identified by optimizing the synthetic conditions of N-lauroyl sarcosine: mol ratio of amino acid to acylchloride 2:1, reaction taken place in a solvent composed by acetone/water 2:1, acylchloride and 20% NaOH were slowly added to the reaction mixture at the same time while maintaining the pH at 9~10, after completion of adding maintaining reacting for 2.5h at 25℃.

首先以月桂酸、肉豆蔻酸、棕榈酸等天然脂肪酸和歧化松香为原料,与氯化亚砜反应制得酰氯,然后采用Schotten-Baumann 缩合法路线,即在碱性条件下,酰氯和氨基酸(肌氨酸、甘氨酸、丙氨酸等)缩合,经过酸化、成盐,合成一系列氨基酸型阴离子表面活性剂:脂肪酰肌氨酸钠,即月桂酰肌氨酸钠(SFS-12)、肉豆蔻酰肌氨酸钠(SFS-14)、棕榈酰肌氨酸钠(SFS-16);脂肪酰甘氨酸钠,即月桂酰甘氨酸钠(SFG-12)、肉豆蔻酰甘氨酸钠(SFG-14)、棕榈酰甘氨酸钠(SFG-16);脂肪酰丙氨酸钠,即月桂酰丙氨酸钠(SFA-12)、肉豆蔻酰丙氨酸钠(SFA-14)、棕榈酰丙氨酸钠(SFA-16);N-歧化松香酰基氨基酸钠(sodium N-disproportionated rosinoyl aminate),即N-歧化松香酰基肌氨酸钠(sodium N-disproportionated rosinoyl sarcosinate ,简称SDRS)、N-歧化松香酰基甘氨酸钠(sodium N-disproportionated rosinoyl glycinate,简称SDRG)、N-歧化松香酰基丙氨酸钠(sodium N-disproportionated rosinoyl alaninate,简称SDRA)。

The researching content was as follows: 1. When AlClx/HY zeolite be used as catalyst, the effects of the ratio of 2-methylnaphthalene to tetramethyl benzene, catalyst concentration, reaction temperature and reaction time on the conversion (based on 2-methylnaphthalene), yield and selectivity (both based on 2,6-DMN) were discussed. In addition, by orthogonal experiment, the optimum reaction conditions were determined at the same time. The optimum reaction conditions : the molar ratio of 2-methylnaphthalene and tetramethyl benzene =1:1, reaction temperature was 400℃.

具体研究如下: 1、以AlClx/HY型分子筛为催化剂,研究原料配比(2-甲基萘与均四甲苯的摩尔比)、反应温度和反应时间对2-甲基萘的转化率、目的产物2,6-DMN的收率和选择性的影响,并通过正交实验确定了该催化剂体系下的最佳反应条件为:原料的摩尔比为(2-甲基萘:均四甲苯)=1:1,反应质量空速为6h-1,反应温度为400℃。

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我们的产品是钛、镍、钼、钽、锆等稀贵金属材料加工;管、棒、丝、带、板、箔、网、饼环及合金制品;反应设备(500L反应釜、钛钢复合反应釜、钛外盘管加热反应釜、镍钢复合反应锅);换热器(钛列管式换热器、钛板式换热器、镍换热器、钛螺旋板式换热器);复合板(钛钢复合板、钛铜复合板、钛铝复合板成品);配件及加热器(钛网蓝、钛法兰、钛螺母钛过滤器、钛泵、钛盘管、阳极、钛离心机、钛加热器、各种非标设备及配件。

The phase equilibrium data of SBO-FAME-Methanol, SBO-FAEE-Ethanol and Glycerol-FAEE-Ethanol systems were measured. The results indicated that it involved two different stages: liquid-liquid-solid reaction stage and liquid-solid reaction stage. When the molar ratio of methanol to oil is 12:1 at 65℃, the turning point is at a 55% biodiesel yield. The liquid-liquid-solid reaction model was proposed based on the double-membranes theory. It indicated that the process is reaction and mass transfer controlled together at the first stage, and the second stage is reaction controlled. The predictions of the model are matched with the experimental results.In the end, the acid was extracted using methanol and ethanol from jatropha curcas l oil.

测定了生物柴油制备过程中的SBO-FAME-Methanol、SBO-FAEE-Ethanol、Glycerol-FAEE-Ethanol三组分相平衡数据,表明固体碱催化过程分为液-液-固和液-固两个反应阶段,在醇油摩尔比为12:1、65℃的初始反应条件下,转化率达到55%时,为第一阶段向第二阶段的转折点;基于双膜理论建立了固体碱催化制备生物柴油的非均相液-液-固反应模型,表明两个反应阶段分别为传质、反应共同控制和反应控制,模型计算值与实验值吻合较好。

The copper-catalyzed 1,3-dipolar cycloaddition of alkynes with azides is a typical example of "click" reaction.1 Since the reaction enjoys the advantages of high efficiency and regioselectivity and requires mild reaction conditions and simple purification procedures, it has become a versatile synthetic tool with applicability in diverse areas including bioconjugation and surface modification.2 The click reaction has also been utilized in polymer science with emphasis on the functionalization of preformed polymers through postpolymerization approaches.3 The effort of developing the reaction into a new polymerization technique, however, has met with only limited success.

登录后回答可以获得经验值奖励,并可以查看和管理所有的回答。登录|铜催化1,3偶极环加成反应的炔烃与叠氮化物是&点击&自reaction.1典型的例子反应享有高效率的优势和区域选择性并要求反应条件温和,简单净化程序,它已成为一个多功能综合工具在包括生物耦合和不同领域的适用性表面modification.2的点击反应亦是利用聚合物科学与功能化的重点通过postpolymerization approaches.3预制聚合物发展到一个新的聚合反应的努力技术,然而,只取得有限的成功。

The progress levels of symptoms after pathogen infection showed that interaction of gray leaf spot pathogen and host has differentiation or polymorphism. The progress levels of symptoms is different.The aggressively has polymorphism. The pathogenicity of different isolates in same cultivar has polymorphism, or the host reaction type of same isolate in different cultivars has polymorphism.The host reaction type has differentiation. There are seven types of host reaction in cultivar and inbred after infected by GLS pathogen:Rectangular lesion without chlorotic halo, Rectangular lesion with chlorotic halo,Irregular lesion without chlorotic halo,Irregular lesion with chlorotic halo, Spot lesion with chlorotic halo,Rectangular and irregular lesionand Rectangular and spot lesion. The host reaction type is coalesced lesion when disease severely. Frequency of each reaction types is different.

通过对玉米灰斑病菌侵染后的显症过程的系统观察,可在组织水平上说明该病菌与寄主互作反应存在分化或多样性:玉米灰斑病菌不同菌株侵染后显症过程表现出明显的差异;玉米灰斑病菌在侵袭力上存在多样性,菌株间对同一种品种的致病性表现多样化,或者同一菌株对不同品种侵染引起的寄主反应表现为多样性;病斑反应型的分化,玉米灰斑病菌侵染玉米品种或自交系后,主要有7种病斑反应类型,即RH型、RN型、IRH型(不规则形具褪绿晕圈病斑)、IRN型(不规则形无褪绿晕圈病斑)、SH型、RI型(长矩形与不规则形混合病斑)和RS型(长矩形与斑点形混合病斑),若发病严重,病斑连成片,而且这些反应类型出现的频率也不同。

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