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Their specific surface area and acid strength were measured, and their catalyt and SBA-15 were ic performance was evaluated in the synthesis of fructone by acetalization of ethyl acetoacetate with ethylene glycol.

用浸渍法制备了一系列负载型磷钨酸及其铯盐催化剂,载体包括超稳Y沸石、脱铝超稳Y沸石、SiO2和SBA-15,测定了催化剂的比表面积和酸强度,并在乙酰乙酸乙酯与乙二醇液相缩合制取苹果酯反应中考察了催化剂的性能。

The synthesis of fructone from ethyl acetoacetate and ethylene glycol using sulfonated activated carbon as solid acid catalyst was investigated.

以活性炭磺化制得新型固体磺酸磺化炭为催化剂,对乙酰乙酸乙酯和乙二醇合成苹果酯的催化工艺进行了系统研究。

Various reaction parameters such as ratio of ethyl acetoacetate to ethylene glycol,catalyst amount,reaction time and water-carrying reagent amount were studied.

讨论了酯醇比、催化剂用量、反应时间、带水剂用量对酯化率的影响。最佳反应条件为:n:n=1:1.8,催化剂用量为乙酰乙酸乙酯质量的2%,带水剂用量为20mL,反应时间3h。

A series of methyl 2,7,7-trimethyl-5-oxo-4-aryl1,4,5,6,7,8- hexahydroquinoline -3-carboxylate were synthesized by the reaction of aromatic aldehydes,dimedone and methyl acetoacetate using ammonium acetate as catalyst in glycol under microwave irradiation with 82%~98% yields in 4~6 min.

微波辐射下以芳醛、达咪酮、乙酰乙酸甲酯为原料,乙二醇为溶剂,醋酸铵为催化剂合成了一系列2,7,7-三甲基-5-氧代-4-芳基-1,4,5,6,7,8-六氢喹啉-3-羧酸甲酯化合物,反应时间4~6 min,产率82%~98%。

_6P_2W_(17)VO_(62) catalyst was prepared and characterized by FTIR,and synthesis of fraistone over as-synthesized catalyst from ethyl acetoacetate and 1,2-propylene glycol was investigated.

制备了Dawson型磷钨钒酸铵催化剂,用FT-IR分析方法对催化剂进行了结构表征,并以乙酰乙酸乙酯与1,2-丙二醇为原料催化合成了苹果酯-B。

The producing of tetrapod-like CuCl was found to be the result of co-effect of acetylacetone and ethylene glycol.

通过对溶剂所起的作用的研究,发现四足形CuCl晶体的形成是乙二醇和乙酰丙酮协同作用的结果。

Palladium thin film has been deposited on glass substrate in mixed solution of ethylene glycol and acetylacetone.

在乙二醇和乙酰丙酮混合溶剂中将钯多晶膜沉积在玻璃片上。

The role of the solvents played in the reaction process was explored, which showed that acetylacetone was the reductant while ethylene glycol was performed as a ligand of Cu〓 as well as a"soft template" for the anisotropic growth of CuCl.

对溶剂在反应过程中所起的作用进行了深入研究,发现乙酰丙酮为还原剂,乙二醇即作配体又是CuCl晶体各向异性生长的&软模板&。

We investigate the kinetics of polyesterification of adipic acid with neopentyl glycol.

对新戊二醇和己二酸的聚酯化动力学进行了研究。

We investigate the kinetics of polyesterification of adipic acid w ith neopentyl glycol.

对新戊二醇和己二酸的聚酯化动力学进行了研究。

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