查询词典 glacial acetic acid

Cu2-Co2-KBr with high catalytic activity and selectivity shows synergistic effect between metal ions.Under the reaction conditions of mCu(Ac2:mCo(Ac2:m= 0.1:0.5:0.1, n:n=0.14, glacial acetic acid as solvent, overdosage sodium percarbonate, 65℃, the conversion can reach 45.9% and the selectivity for p-methoxy benzaldhyde is about 68.3%.

结果表明，Cu2-Co2-KBr具有较高的催化活性和选择性，体现出金属离子之间的协同作用，对甲基苯甲醚在mCu(Ac2：mCo(Ac2：m=0.1：0.5：0.1，n：n=0.14，冰醋酸作溶剂，稍过量的过碳酸钠，65℃的条件下，转化率可达45.9%，生成对甲氧基苯甲醛的选择性为68.3%。

Four chalcones were synthesized by aldol condensation reaction of acetophenone or para-substituted acetophenones with 2-phenyl-1,2,3-triazol-4-carboxaldehyde, which reacted with three hydrazines in glacial acetic acid under refluxing to give a series of pyrazoline derivatives.

以2-苯基－1，2，3-三唑基－4-甲醛为原料，与苯乙酮［或取代苯乙酮(1a~1d)］发生羟醛缩合，生成相应的查尔酮(2a~2d)，再与不同的肼反应，合成了12种新的5位含2-苯基－1，2，3-三唑基的吡唑啉衍生物3a~3d，4a~4d，5a~5d。

Results:All dosage groups of Tou-Yu-Tong Pills could release chronic nerve injury caused by formaldehyde solution; remarkedly inhibit the pain of mice in the formalin test and prolong the latencies of paw-licking. It could significantly diminish pain caused by glacial acetic acid ,reduce the number of the writhing in mice.To the model of migraine ,Tou-Yu-Tong Pills can improve the content of 5-HT in brain tissue of mice ,and ruduce 5-HTAA.

结果 头愈痛丸对福尔马林致小鼠慢性神经性疼痛反应，能明显减少动物舔后足的时间，改善其伤害性疼痛行为反应；对冰醋酸致小鼠扭体反应，能显著延长扭体的潜伏期，减少扭体反应的次数；对小鼠偏头痛模型，能显著升高小鼠脑内5-HT的含量，且降低5-HIAA的趋势。

Bis (P—bromobenzylamino) ethane and 1,2—bis (m—Iodobenzylamino) ethane may be prepared by condensation of the corresponding halo benzaldehyde with ethylenediamine and followed by catalytic hydrogenation of the Schiff's bases over Pto_2 in glacial acetic acid solutions: Both Ⅱa and Ⅱb may react in neutral mediam with aldehydes to form well—defined crystalline tetrahydro—imidazole, which may be served as derivatives of identification for aldehydes: Under the same condition, however,Ⅱb may ...

用1，2-二乙烷与二十余种醛类作用，得到有固定熔点的晶体衍生物，它们的熔点分布在85—210℃之间，产率为40—96％，这试剂与甲基酮类在相同条件下无反应，因此，它可作为鉴定醛类的专属试剂。 2。上述衍生物用稀盐酸在室溫处理，能发生水解，可以定量地收回原来的醛，因此这试剂又可作为分离醛类的试剂。 3。上述衍生物可以用非水滴定法半微量地测定其分子量可作为鉴定醛类的另一项参考数据。 4.1，2-二乙烷与醛类能生成晶体衍生物，但这试剂也与甲基酮在同样条件下发生反应，所以不适合作为鉴定醛类的专属试剂。

Methods by using a broad pH range column(Gemini NX C18,4.6mm×150mm,5μm),basic mobile phase which was[H_2O-ammonia-glacial acetic acid] (96:3.6:0.4)-methanol,the related substances in etimicinsulfate were separated and detected by electrospray ionization and positive ion monitoring,the ESI ion source condition was following: temperature is 350℃,nebulizing pressure is 50 psi,dry gas flow is 10 L /min.some related substances in etimicinsulfate were identified by comparing the retention time in chromatography,~+ spectrum and MS~2 spectrum with reference substances\',the others which haven\'t reference substances were identified or speculated by analyzing their MS~2 fragmentation with the help of a rule summarized from the MS~2 fragmentation of gentamicin C1a,micronomicin and etimicin.Results nineteen related substances in etimicinsulfate were separated and detected.

方法利用宽pH范围的Gemini NX C18(4.6mm×150mm，5μm)色谱柱，在碱性条件下，以[水-氨水-冰醋酸(96：3.6：0.4)]-甲醇(70：30)为流动相，直接分离各组分；并用HPLC-ESI-MS~2检测样品中各组分，质谱条件：ESI离子源，离子源温度350□，雾化室压力50 psi，干燥气流速10 L/min，正离子检测方式；对有对照品的有关物质采用比对有关物质与对照品的色谱保留时间、准分子离子的质荷比及二级质谱方法进行鉴定，无对照品的有关物质，则是先通过解析庆大霉素Cla、小诺霉素、依替米星的二级质谱，对该类化合物的二级质谱裂解规律进行归纳，并以此推测未知新化合物进行结构，再用推测的结构对二级质谱进行解析，如所有的碎片离子均合理解释，表明推测合理。

The optimum conditions were as follows: the volume proportion of water and glacial acetic acid was 4, the reaction temperature was 30℃ and reaction time was 10 minutes.

由此对反应条件加以优化，得出反应的适宜条件是当水和冰醋酸的体积比为4，反应温度为30℃，反应时间为10 min时，收率可达78%。

Analysis was carried out on a Hypersil ODS2 column(4.6 mm×250 mm,5 μm) with acetonitrile-0.1% glacial acetic acid as the mobile phase,and eluates were detected by an evaporative light scattering detector.

采用Elite Hypersil ODS2(4.6 mm×250 mm，5μm)色谱柱，乙腈-0.1%冰醋酸水溶液为流动相梯度洗脱，流速1mL.min-1，以蒸发光散射检测器检测，记录70 min色谱图。

In synthesizing process, the optimum quanta of hydrogen peroxide solution and glacial acetic acid which affect epoxide number were determined.

对合成过程中影响环氧值的两个重要条件：即双氧水和冰醋酸的用量做了大量实验，确定了最佳条件。

Procedure In a 1-l. round-bottomed flask are placed 250 cc. of glacial acetic acid, 15 g.

程序 在1升。圆桌会议触底烧瓶置于250毫升。

The R f value of the glucosamine sulfate was 0.36 measured by paper chromatography with the solvent system of pyridine, ethyl acetate, water and glacial acetic acid (5∶5∶3∶1 in volume).

经纸层析鉴定，以吡啶、乙酸乙酯、水和冰醋酸按体积比 5∶5∶3∶1组成的溶剂系统进行展层，氨基葡萄糖硫酸盐的Rf 值为 0 。36。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了