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The results show that the introducing of multivinyl monomer and CaCO3 can slow down polymerization rate to different extent.Using 1％～5％ trimethylolpropane trimetbacrylateor divinyl benzene,tight encapsulation of CaCO3 can be realized and beyond 94％PS cannot be extracted. The amount of crosslinker or emulsifier should be accommodated when the load amount of CaCO3 is increased.CaCO3 content in the product increases consequently with the increase of the loaded amount of CaCO3,which can be known from FT-IR and TGA.TEM observations reveal that when the load amount of CaCO3 is 14.8％,most CaCO3 particles are encapsulated and each latex particle contains one CaCO3 particle.Composite particles have well-defined core—shell structure and the thickness of polymer shells is around 10 nm.However,the thickness of polymer shell decreases and many free CaCO3 particles appear when the load amount of CaCO3 reaches 29.3％and 58.7％,respectively.

结果表明，多乙烯基单体以及碳酸钙的引入会使聚合反应速率有不同程度的降低；使用1%～5%的TMPTMA或DVB，可实现PS对碳酸钙颗粒的牢固包覆，不可抽提的PS达94%以上；当碳酸钙用量改变时，需要适当调整乳化剂和多乙烯基单体的用量；IR和TGA的结果表明，随着碳酸钙用量增加，产物中的碳酸钙含量也相应增加；TEM照片和计算结果显示，当碳酸钙用量为14.8%时，绝大部分碳酸钙颗粒被包覆，且基本上每个乳胶粒中包覆一个碳酸钙颗粒，复合粒子具有清晰的核壳结构，壳层厚度约为10 nm，而当碳酸钙用量增加到29.3%和58.7%时，壳层厚度减小，并且出现较多裸露的碳酸钙颗粒。

The synthesis of divinyl liquid crystalline monomer 4-undecenyloyloxybenzoyl-4'-allyloxybenzoyl-p-benzenediol bisate and network polymers was described. The chemical structures of the synthesized monomer and network polymers were confirmed by FT-IR spectrum.

以双烯类液晶单体4-十一烯酰氧基苯甲酸-4'-烯丙氧基苯甲酸对苯二酚双酯为交联剂，通过与聚矽氧烷接枝反应，合成了系列网络聚合物P1~P5。

The FT-IR spectrum of PANI/MMT nanocomposite denotes that PANI produced in the form of emeraldine salt, which absorption peaks was

经矢量网络分析仪测量发现，PANI／MMT在2.0-18GHz的复介电常数、复磁导率和以反射损耗表示的微波吸收曲线都

FT-IR spectra shows that the polyaniline is present primarily in the emeraldine salt form, and the polymeric chains interact with inorganic framework, most likely via V=O…HN hydrogen bonding. XRD,TG and DSC indicate that the lamellar structure of the V_2O_5 is preserved, PAn chains eliminate water form the interlamellar region and are partially inserted between the layers, and exist with extended-chain conformation owing to the confined environment.Electrochemical investigation in the range of 1.8~3.8V vs.

红外光谱表明复合物中PAn主要以导电聚苯胺盐的形式存在，PAn链与V_2O_5晶格之间可能形成了V=O…HN氢键。X射线衍射、热重和差示扫描量热证实了PAn/V_2O_5复合物保持了较规整的层间排列结构，PAn取代了V_2O_5干凝胶中的层间水而部分嵌入其片层间，由于受空间的限制，PAn分子链以比较伸展的链构象存在。

The results indicated that the cross sections of fibers were porous and the surface had many cross markings, endwise lines. The FT-IR of the three fibers were basically similar. Ramie fiber accorded to the character of cellulose I, and with the highest crystallinity.

实验结果表明，这三种纤维的截面内均有孔隙，同时表面具有横节竖纹；它们的红外光谱图基本相似；苎麻纤维符合纤维素I的特征，且结晶度最高；黄麻的耐热性能最好，其次是苎麻。

FT-IRDSC tests were taken to analyze the structure,and the terms-mechanical properties,shape recovery behaviors and tensile properties were discussed to study the extender influence on SMPU.The results show that SMPU extended by ethanediol and FA has good micro-phase separation structure and soft...

结果发现，扩链剂对SMPU有一定影响，用FA、ED扩链的SMPU具有较好的微相分离，而DE扩链的具有较好的软段结晶性能；FA、HD的SMPU具有较低的形状回复温度和较快的形状回复速率，HD、DE扩链的则具有较好形状固定性能，FA、DE扩链的SMPU循环使用性能较好；同时FA、HD的SMPU具有较高的弹性模量与力学强度。

Despite the fact that the Exactive is categorized as an FT/MS, it is priced and positioned to compete against LC-TOF and LC-Q-TOF instrumentation.

Exactive是同LC-TOF和LC-Q-TOF竞争的产品，价位大致在25~35万美元。

Also introduced by Thermo at ASMS was the Exactive benchtop LC/ MS system, which is based around the Orbitrap mass analyzer, in contrast to Thermo's LTQ-Orbitrap and LTQ-FT, the Exactive is not a tandem system, which greatly lowers its price, but it can still provide MS/MS.

Thermo还推出了台式的包含Orbitrap分析器的Exactive仪器，因为它不是串联的仪器，所以大幅降低了价格，但其实，Exactive仍可以提供串联质谱MS/MS功能。

The influence of the structure and property of Jinzhou coker heavy gatch on formation of needle coke was investigated by using elemental analysis, liquid chromatogram, FT-IR spectroscopy and molecular weight determination.

本文利用元素分析、液相色谱、傅立叶变换红外光谱、分子量测定等分析手段，研究了锦州焦化重蜡油的组成结构和性质对生产针状焦的影响，并通过与典型针状焦生产原料——锦州催化裂化油浆的比较，指出了锦州焦化重蜡油用作针状焦原料的不足。

According to the effect of guanylic acid on fluorescence intensity of ligand-Cu or Fe (Ⅲ binary complex system, it is found that guanylic acid and Cu, Fe have synergic quenching effect on the fluorescence of ligand due to the formation of ternary complex.

对原始配体CPFX进行了元素分析、FT-IR、〓H-NMR、〓C-NMR、MS等手段进行了结构确证，并讨论产生这种变化的可能过程，对配合物配体间的相互作用（氢键作用、芳环堆积作用）着重进行了讨论。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。