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We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.

本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上,利用传统植化分离手段和现代分离技术,包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱,制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物,其中,2个新化合物和2个己知化合物,并进一步通过现代分析技术IR,ESI-MS,~1H-NMR,~(13C-NMR,HMBC,HMQC,~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是:3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2,6-二甲基-6-O-β-D-吡喃鸡纳糖基-2,7-辛二烯酸基]-金合欢酸-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠李糖基(1→2)-β-D-吡喃葡萄糖苷,金合欢酸3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷;2个已知化合物结构分别是:金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷,金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。

Figures include direct and third-party funding to projects in China by Alcoa Foundation as a whole.

2006年的数字包括美铝基金会对中国的项目提供的直接和第三方资助的总和。

The objective of this paper is to lay a foundation for compositive utilization and exploitation of alfalfa plant.

故本研究旨在此方面作一种摸索,为今后苜蓿资源的综合利用和开发奠定基础。

All of this lay a solid foundation for large-scale preparation and application of alginate lyase.

该菌株产酶发酵条件的研究,为褐藻胶裂解酶的大规模制备及应用奠定了基础。

The paper maintains that the immingrants from Fujian to Taiwan in history and the propagation of the culture of south Fujian have alid the foundation for the formation of the culture of Fujian and Taiwan.

闽台区域文化的形成与闽南人移居台湾,并在台湾开垦奋斗、传承和发展闽南文化有着密切关系。

It is concluded that, first, geochemical data of the surface soils can clearly distinguish two kind of soils, that is, juvenile soils, for example, purple soils, which inherits most geochemical characteristics of the parent rocks or materials, and anthropic soils, the geochemical characteristics of which have been greatly changed as the results of intensive impact from variety of agricultural uses. Second, different soils have typical indicator elements association respectively due to different parent rocks or materials and utilization, such as purple soils, yellow soils (low alkali and alkaline-earth metal contents and pH value), paddy soils (high organic element and heavy metal elements contents) and fluvo-aquic soils (high rock-forming accessory mineral elements contents) and so on. Consequently, it can be suggested that elements association is an important indicator for two key factors (parent materials and anthropic activities) of soil classification. Third, some differences exist between soil genesic classification and result of cluster analysis, because geochemical characteristics of surface soils can not completely represent the foundation applying to soil genesic classification, that is, condition and process of soil-forming, and soil property.

结果表明:浅层土壤的地球化学数据能较好地用来区分两类土壤,即紫色土一类的幼年土壤(在很大程度上继承了母岩、母质的地球化学特征)和受强烈人为活动水耕、早耕熟化的土壤(外来物质的不断加人显著地改变了浅层土壤原有的地球化学性质);(2)各类土壤因母岩母质和利用方式不同,各具明显的标志性元素组合特征,如紫色土、黄壤(低碱和碱土金属元素和pH值)、水稻土(高有机元素、肥料元素和重金属元素)和潮土等,因此,这些元素组合是土壤分类两个要素的重要参照系;(3)浅层土壤的地球化学特征不可能完整地体现成土条件、成土过程和土壤属性这三个发生分类依据,因此,聚类分析结果与发生类型之间存在一定的差异。

The studying all by oneself is an important means to push people to educate, replace the foundation education and play an important role in the course of education reform.

自主学习是推动人们终身教育、变革基础教育的重要手段,在课程教育改革中占有重要的地位。

Watch international analyst Cao Fei easily to think, pay treasure to already made application of all-pervading Internet foundation.

易观国际分析师曹飞认为,支付宝已成为普及的互联网基础应用。

Because only in the demand for a good foundation, and its supply can be effectively allocated.

因为只有需求的一个良好的基础,它的供应,才能有效地分配。

Accounting information exploration is not only the foundation of achieving effective allocation of recourses in Capital Markets but also one of the basic goals of accounting.

会计信息披露是资本市场实现资源有效配置的基础,也是会计工作的基本目标之一。

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In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是,在否定句或疑问句里,这种带有"do"的方法表达的效果却没有什么强调的意思。

Go down on one's knees;kneel down

屈膝跪下。。。下跪祈祷

Nusa lembongan : Bali's sister island, coral and sand beaches, crystal clear water, surfing.

Nusa Dua :豪华度假村,冲浪和潜水,沙滩,水晶般晶莹剔透的水,网络冲浪。