查询词典 formic
- 与 formic 相关的网络例句 [注:此内容来源于网络,仅供参考]
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The eluate was prepared by dissolving am- monium formate 6.3 g and octanen sulfoacid sodium 1.0 g in 700 mL water(pH 3.8 adjusted with formic acid)and subsequently diluted with water to 1000 mL.
结果:在本色谱条件下腺苷蛋氨酸与辅料、溶剂峰及其有关物质的分离度符合要求,在200~600μg·mL~(-1)范围内线性良好(r=0.9998)。回收率为99.61%~99.98%,RSD为0.23%~1.3%。
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Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.
采用&一勺烩&方法,以4-羟基苯甲腈为起始原料,首先与硫氢化钠和无水氯化镁在N,N-二甲基甲酰胺中反应,所得中间体不经分离,直接加入2-氯乙酰乙酸乙酯进行环合反应,得到2-(4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯(2);然后通过六亚甲基四胺/三氟乙酸进行Duff反应,得到2-(3-甲酰基-4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯(3);再经盐酸羟胺/甲酸/甲酸钠体系脱水得到目标化合物。
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At 1st、2nd、3rd months after surgery the rats were killed respectively and the implanted tibiae were got , the tissue samples were fixed with 10% Formaldehyde soaked and 8% formic acid was used to dissolve the calcium for 10 days.
于种植术后1个月、2个月、3个月时,取出带种植体的胫骨,取下的标本立即放入10%甲醛缓冲溶液固定、经过8%甲酸溶液脱钙、梯度酒精脱水后,制作HE染色的组织学切片,做光镜及骨组织的形态计量学观察。
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Results showed that extraction abilities depends on the hydrophobic of solutes which pK〓 values are similar, e. g. acetic, propionic, butyric and valeric acids, while pK〓 values affect dominantly the extraction abilities of acids with similar hydrophobic, e. g. formic, acetic, chloroacetic, dichloroacetic, and trichloroacetic acids. Meanwhile, diluents and TOA concentration also affect the extraction equilibria of acids through the specific basicity of TOA .
TOA对酸性差别很小的一元羧酸如乙酸、丙酸、丁酸、戊酸的萃取能力主要取决于羧酸的疏水性参数logP;TOA对疏水性参数差别较小的羧酸如甲酸、乙酸、一氯乙酸、二氯乙酸、三氯乙酸的萃取能力主要取决于羧酸的电性参数;稀释剂的种类、TOA的浓度都会影响TOA的表观碱度pH〓,并通过TOA的表观碱度影响羧酸的萃取平衡。
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Degummed Bombyx mori silk was dissolved in a ternary solvent system of CaCl2/CH3CH2OH/H2O in 1∶2∶8 mole ratio at 60℃,and lyophilized SF was dissolved in 98% formic acid to obtain regenerated SF solution for electrospinning.
将脱胶后的桑蚕丝溶解在摩尔比为1:2:8 的60℃CaCl2/CH3CH2OH/H2O三元体系中,将该溶液冷冻干燥后溶解在98%的甲酸中得到再生丝素溶液,对其进行静电纺丝。
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In Expt.1, that the effects of microbial inoculants and formic acid on the pH, the number of LAB, yeast and mold, and the formation of lactic acid was evaluated during the different periods of corn silage (after day0.5, 1,2, 3,5, 7, 10, 20, 40 and 60 of ensiling) using the methods of laboratory silos and microbiology techniques.
原因在于本试验接种的乳酸菌数量较少,发酵过程中没有成为优势菌群。添加甲酸在发酵初期抑制了乳酸菌的增殖,降低了乳酸的生成量和青贮初期的pH值,提高了青贮后期pH值;对酵母和霉菌最初表现为促进增殖的作用,5天以后对酵母有较强的抑制作用。
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The addition of formic acid inhibitted the growth of LAB at the early stage of the fermentation, decreased the production of lactic acid and the pH of the early stage of the silage and increased initially the growth of the yeast and mold but inhibitted the growth of mold after 5 days of ensiling.
结果表明:单独添加植物乳杆菌增加了乙酸生成量和总有机酸生成量,降低了乳乙酸比;单独添加戊糖片球菌减少了乙酸生成量和总有机酸生成量,提高了乳乙酸比;二者均延缓了pH值的下降速度。
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The eluent was evaporated to near-dry under nitrogen and then redissolved with methanol-0.1% formic acid(1∶1,by volume),finally determined by HPLC-MS/MS.The linear range of the calibration curve was 0-50 μg/L for all pyridine herbicides.
在大白菜和橙子2种基质中分别添加5.0、10.0和20.0μg/kg3个水平,玉米基质中添加5.0、10.0、20.0和40.0μg/kg 4个水平的4种吡啶类除草剂混合标准溶液,平均回收率为70%~117%,方法的相对标准偏差小于15%。
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In addition, the basis is formic the characteristic of diffuse of group of element of the information when algorithm handles this issue, reframed the newer strategy of information element and diffuse means.
此外,根据蚁群算法处理本新问题时信息素散播的特征,重构了信息素的更新策略和散播方式。
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This article discussed the influence factors of productivity of formic acid such as the mol ratio of sodium formate and phosphoric acid, the addition of phosphorus pentoxide, vapouring temperature.
对原料配比、五氧化二磷加入量、蒸馏温度对甲酸产品浓度、产率的影响进行了实验。
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