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The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that for��C=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.
通过研究阐明:紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移,νC=O振动吸收峰在聚合24h后红移;TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01,α为2.28,优于其它功能单体参与得到的聚合物识别特性;TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间,作为色谱固定相具有良好的通量和低的柱压;在乙腈流动相中,TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动,低温有利于分子印迹固定相分离甾醇结构类似物;TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融,Tp=257.40℃,聚合物CP的降解温度在267.79℃,MIP降解温度在343.11℃,制备的固相微萃取头初步经GC/MS 270℃的耐热性测定;不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应;分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性,可作为此类化合物的吸附材料,特别对孕酮强保留的富集特性,可作为孕酮的选择性识别吸附剂,其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡,具有作为传感器核心敏感材料的潜力;对比萃取奶粉中17β-雌二醇性能,MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留,回收率依次为85.5%,43.7%和30.7%。
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The analysis of the optical signal transmission characteristics and the physical parameters provides the theoretical foundation for optimizing the design and improving the performance of AWG; and the optimizing design numerical value calculation method solves the complex problem of the optimizing design of the AWG, it can also provide a way for AWG computer aided design system; the AWG optical signal processing analysis provide a way for optical signal Fourier transform, serial and parallel transmission, circle shift, matrix transform and differential processing; the optical signal processing characteristics of AWG develop AWG to use for new field, and the optical signal processing will play an important role on all-optical networks in the future; by the definition of the wavelength transform matrix of the AWG, the signal output positions that come from these input signals of the different wavelength or the same wavelength but the different input ports and carrying different signals can be accurately determined, and the wavelength transmission matrix plays an important role for analyzing the routing of the complex optical network, or designing the network nodes such as the optical path add/drop multiplexer and optical cross connect device; the wavelength transmission matrix also provides a method for monitoring and managing the wavelength transmission of the optical network nodes; e analysis of the AWG' OXC node structure and wavelength routing provides a way for realizing the OXC, especially for multi-path/multi-wavelength OXC and the intelligence node of the optical networks; by the studying of the control plain characteristics, router, traffic engineering, program and the improved arithmetic of the wavelength routing, the method for realizing the GMPLS' OXC optical transport network is provided, and it play an important role for the study of the automatic switched optical network; the time-frequency analysis can provide more information about the dispersion and energy changes of .the pulsed light transmission in the singlemode fiber, it also provides more useful parameters for analyzing the dispersive accumulating and dispersive compensating.
AWG光信号传输特性与相关参数的分析,为进一步优化设计AWG及提高其性能提供了理论依据,而优化设计计算数值方法解决了AWG优化设计计算的复杂问题,为进一步建立AWG的计算机设计系统提供了基础;AWG光信号处理的特性分析,提出了AWG应用的新领域,为光信号的傅立叶变换、串并传输、循环移位、矩阵变换、微分处理等提供了一条途径;波长传输矩阵变换关系的建立,不仅得到了确定多路AWG每路信号从输入端口到输出端口的准确输出位置的方法,而且在分析应用AWG实现复杂的光通信网络路由的连接、特别在设计分插复用器和交叉连接器等网络节点时有重要的作用,能有效而准确地确定波长的路由关系,为实现节点波长传输路由的监控和管理提供有效手段;基于AWG的OXC结构和波长路由的确定为实现OXC技术、特别是多路多波长的OXC和光网络的智能节点技术提供了有效的方法;控制平面的特征、路由器、流量工程、程序及改进的波长路由算法的研究实现了基于GMPLS的OXC光传送网络的控制平面,为建立自动交换光网路提供了一定的基础;时频分析可以更直观和更清晰地描述脉冲信号在单模光纤中传输色散和能量的变化,为色散积累和色散补偿提供有效的分析参数。
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According to a questionnaire issued by the Hunan Normal University athletes CHOOSE parade the status of sport injury, injury causes, preventive measures were discussed, mainly come to the following conclusions:① CHOOSE parade of the athletes sports injuries are more common, the rate of injuries 88% of the injury concentrated in the wrist position and thighs of 35.84%; waist accounted for 16.98 percent, 15.09 percent of the knee, shoulder or 11.32 percent, accounting for 9.43 percent of ankle, elbow or 7.54 percent, abdomen, accounting for 3.79%② CHOOSE Exercises for the main types of injury ligament injury, accounting for 33.96 percent; joint injury, accounting for 16.98 percent; muscle sprain, accounting for 15.09 percent; contusion, accounting for 11.32 percent; periostitis, accounting for 9.43%; tenosynovitis, accounting for 7.54 % bursitis, accounting for 3.77%; fracture, or 1.88 percent ③ CHOOSE Exercises injury in the course divided into acute injury and chronic injuries, mainly to acute injury.
根据所发放的运动员问卷对湖南师范大学啦啦操运动员运动损伤的现状、损伤成因、预防对策进行了探讨,主要得出以下结论:①啦啦操运动员运动损伤的情况较为普遍,伤病率达88%;损伤的部位集中在手腕关节和大腿占35.84%;腰部占16.98%,膝关节占15.09%,肩关节占11.32%,踝关节占9.43%,肘部占7.54%,腹部,占3.79%②啦啦操运动损伤的种类主要为韧带拉伤,占33.96 %;关节损伤,占16.98%;肌肉扭伤,占15.09%;挫伤,占11.32%;骨膜炎,占9.43%;腱鞘炎,占7.54%;滑囊炎,占3.77%;骨折,占1.88%③啦啦操运动损伤的病程分为急性损伤和慢性损伤,以急性损伤为主④啦啦操运动损伤的时间主要集中在10一12月份,1一3月份⑤啦啦操运动员运动损伤的预防对策主要包括:注重体能训练提高体能储备、合理安排训练内容和负荷、加强身体全面训练和易伤部位练习的实效性训练、重视运动技术的分析和研究、重视训练后的恢复措施、加强医务监督提高自我保护、重视训练后的放松运动。
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Quality Assurance Center, the Great Wall of China opened up the field of survey and design quality system (ISO9000) certification in the country has created the first 21, except for China Tianchen company issued the first national design industry certification, but also for the country's largest Daqing Petroleum Administration Bureau of enterprises (28 million) of the overall authentication certificates for the micro-car factory in Tianjin issued the first National Certification automotive industry for the central city of Harbin presented the first national design activities have a commercial certificate service system, for China's Guizhou Maotai liquor industry plant awarded the first National Certification for Tanggu saltworks awarded the first National Certificate salt industry for China Railway Materials Tianjin issued the first material system, the National Certification for Tianjin Service Center for Scholarly Exchange awarded the first Certificate of intermediary organizations, in order to Qingdao Branch Qingdao railway station railway industry presented the first certificate for the China Telecom Group Tianjin Telecom awarded the first Certificate telecommunications industry and so on.
长城质量保证中心开辟了我国勘测设计领域的质量体系(ISO9000)认证工作,在全国创造了二十一项第一,除为中国天辰公司颁发了全国第一张设计行业认证证书外还为全国最大的企业大庆石油管理局(28万人)整体认证颁发证书,为天津微型汽车厂颁发全国第一张汽车行业认证证书,为哈尔滨中央商城颁发全国第一张有设计活动的商业服务系统认证证书,为中国贵州茅台酒厂颁发全国酒类行业第一张认证证书,为塘沽盐场颁发全国第一张制盐行业的认证证书,为中国铁路物资天津公司颁发全国第一张物资系统认证证书,为天津市留学服务中心颁发第一张中介机构的认证证书,为青岛铁路分局青岛站颁发铁路行业第一张认证证书,为中国电信集团天津电信公司颁发第一张电信行业认证证书等等。
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Thecompare of genetic map between Lowes and ours showed 26 homology marker situ,which occupied 21.1% of the marker situ in the experiment. 81 QTLs were detected for 11 agronomic traits. 4 QTLs were detected for plantheight, which explained 10.3%~28.9% of trait variance; 2 QTLs were detected forNo. of effective 1-st branches, which explained 22.1%~47% of trait variance; 16QTLs were detected for effective branches height, which explained 12.2%~51.8% oftrait variance; 15 QTLs were detected for length of main inflorenscence, whichexplained 7.4%~26.6% of trait variance; 5 QTLs were detected for effective siliquesof main inflorenscence, which explained 11.2%~25% of trait variance; 1 QTLs weredetected for density of main infiorenscence, which explained 17.3% of trait variance;12 QTLs were detected for length of silique, which explained 24%~36.7% of traitvariance; 2 QTLs were detected for seed per sillique, which explained 9.6% and16.9% of trait variance; 2 QTLs were detected for 1000 seed weight, which explained26%~13.7% of trait variance; 11 QTLs were detected for Total effective siliques perplant, which explained 14.8%~47.2% of trait variance; 11 QTLs were detected forplant height, which explained 14.3%~32.8% of trait variance.
其中,株高检测到4个QTLs,解释性状表型变异的10.3%~28.9%;一次有效分枝数检测到2个QTLs,解释性状表型变异的22.1%和47%;有效分枝部位检测到16个QTLs,解释性状表型变异的12.2%~51.8%;主花序长度检测到15个QTLs,解释性状表型变异的7.4%~26.6%;主花序有效角数检测到5个QTLs,解释性状表型变异的11.2%~25%;主花序角密度检测到1个QTLs,解释性状表型变异的17.3%;角果长度检测到12个QTLs,解释性状表型变异的24%~36.7%;每角粒数检测到2个QTLs,解释性状表型变异的9.6%和16.9%;千粒重检测到2个QTLs,解释性状表型变异的26%和13.7%;单株有效角果总数检测到11个QTLs,解释性状表型变异的14.8%~47.2%;单株产量检测到11个QTLs,解释性状表型变异的14.3%~32.8%。
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Results:210 cases of patients,50 cases of chronic cervicitis and atypical hyperplasia,accounts for 23.8%;22 cases of vaginitis,accounts for 10.5%;20 cases of endometritis,accounts for 9.5%;Five cases of cervical polyps,accounts for 2.4%;Three cases of endometrial polyps,accounts for 1.43%;Dysfunctional uterine bleeding 75 cases,accounts for 35.7%;Endometrial three cases of atypical hyperplasia,accounts for 1.43%;Eight cases of uterine fibroids,accounts for 3.8%;15 cases of m alignant tumor,Accounts for 7.14%;IUD caused by bleeding in 9 cases,accounts for 4.3%.
结果:210例患者中,慢性宫颈炎及不典型增生50例,占23.8%;阴道炎引起出血者22例,占10.5%;子宫内膜炎20例,占9.5%;宫颈息肉5例,占2.4%;内膜息肉3例,占1.4%;功能失调性子宫出血75例,占35.7%;子宫内膜不典型增生3例,占1.4%;子宫肌瘤8例,占3.8%;恶性肿瘤15例,占7.1%;宫内节育器引起的出血9例,占4.3%。
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Black Square Table clothing Napkins VestWorking Cleanning Ladies Polo/t-shirt, Black trousers Nurse shoes white Long sleve shirt green Black ties Black lace Name tag Carpets Double Bed cover Double bed Duvet RECEPTION/LOBY/INTERNET ROOM BOUTIQUE Reception Counter Key holders and other Ther utensils for reception Furniture for the Lobby Undercounter bar fridge Cupboards for Lobby bar Counter + Shelfs for boutique Set of 3 posts + 3 CHAIRS VARIOUS Pictures for walls Eletrical guiser 50L Split aircon 9000BTU Splip aircon 12000 Split aircon 18000 Split aircon 24000 Fluorescent lamp arm Portable computer lap top Trolle for luggage Telephone Central w/100 extentions + 10 exterior lines Fire dectectors for 70 rooms Piano automatic for pub Security chains for room doors Water spray Massage table Automatic chair for massages
黑色 表服装广场餐巾纸 VestWorking清洗夫人马可波罗/ T恤,黑色长裤白色护士鞋龙绿色球衣sleve 黑色领带黑色花边名称标签地毯一张双人床封面双层床上用品接待/·罗比/互联网室专卖店接待柜台钥匙持有人及其他有接待用具家具的大厅 Undercounter酒吧冰箱碗柜的大堂酒吧反+ Shelfs的精品集3个+ 3椅子不同图片墙 Eletrical guiser 50L 斯普利特空调9000BTU Splip空调12000 斯普利特空调18000 斯普利特空调24000 日光灯臂便携式计算机圈的顶端( med.price )特罗勒行李电话中央w/100扩张+ 10外墙线消防的70间客房自动钢琴的酒吧安全链的房间门喷水按摩表自动按摩椅供
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Results For 12 CRDA cases with severe hydronephrosis,BUS was diagnostic in 9 cases and suggestive in 2 cases,while IVP was only suggestivc in 4 cases;For 11 cases with mild to moderate hydronephrosis,BUS made correct diagnosis for 10 cases,IVP was correct in 5 cases;For 8 CRDA of maldeveloped type,BUS made diagnosis for 5 and was suggestive for 1,IVP was correct for 2;For 3 cases CRDA of developed type,IVP was correct for all while BUS was correct only for 1 case.
结果 12例重度积水型重肾,B超对9例作出诊断,2例提示性诊断,而IVP仅对4例提示性诊断;11例轻-中度积水型重肾,B超对10例作出诊断,而IVP对5例作出诊断,3例提示性诊断;8例发育不良型重肾,B超对5例作出诊断,1例提示性诊断,而IVP仅对2例作诊断;3例发育型重肾,IVP均作出诊断,而B超仅对1例作出诊断。
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The imaging manifestation of BUS and IVP were restrospectively analysed in accordance with surgical findings.Results For 12 CRDA cases with severe hydronephrosis,BUS was diagnostic in 9 cases and suggestive in 2 cases,while IVP was only suggestivc in 4 cases;For 11 cases with mild to moderate hydronephrosis,BUS made correct diagnosis for 10 cases,IVP was correct in 5 cases;For 8 CRDA of maldeveloped type,BUS made diagnosis for 5 and was suggestive for 1,IVP was correct for 2;For 3 cases CRDA of developed type,IVP was correct for all while BUS was correct only for 1 case.
结果 12例重度积水型重肾,B超对9例作出诊断,2例提示性诊断,而IVP仅对4例提示性诊断;11例轻-中度积水型重肾,B超对10例作出诊断,而IVP对5例作出诊断,3例提示性诊断;8例发育不良型重肾,B超对5例作出诊断,1例提示性诊断,而IVP仅对2例作诊断;3例发育型重肾,IVP均作出诊断,而B超仅对1例作出诊断。
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Midnight gettin' uptight where are you You said you'd meet me now it's quarter to two I know i'm hangin' but i'm still wantin' you Hey jack it's a fact they're talkin' in town I turn my back and you're messin' around I'm not really jealous don't like lookin' like a clown I think of you ev'ry night and day You took my heart then you took my pride away I hate myself for loving you Can't break free from the the things that you do I wanna walk but i run back to you that's why I hate myself for loving you Daylight spent the night without you But i've been dreamin''bout the lovin' you do I won't be as angry 'bout the hell you put me through Hey man bet you can treat me right You just don't know what you was missin' last night I wanna see your face and say forget it just from spite I hate myself for loving you Can't break free from the the things that you do I wanna walk but i run back to you, that's why I hate myself for loving you I hate myself for loving you Can't break free from the things that you do I wanna walk but i run back to you that's why I hate myself for loving you I think of you ev'ry night and day You took my heart then you took my pride away I hate myself for loving you Can't break free from the the things that you do I wanna walk but i run back to you that's why I hate myself for loving you I hate myself for loving you I hate myself for loving you
午夜时分,气氛正好你在哪里?你说会来找我但现在已经一点四十五分我明白自己犹豫不决,但我依然需要你嘿,杰克,人们真的议论纷纷我置若罔闻,你却越闹越大我不是真的吃醋只是不想被人当小丑看待我日日夜夜都想着你你带走了我的心,然后又夺走了我的尊严我恨自己爱上了你无法从你的所作所为中泰然自若我曾经离开,却又回到你身边那就是我恨自己爱上了你的原因白天了,我没有你而过了一晚但我一直梦想着你的爱你对我那麽糟,但我已经没那麽生气了嗨,老兄,我打赌你会对我好你只是不清楚昨晚错过了什麽我想看看你,告诉你忘掉这些不愉快我日日夜夜都想着你你带走了我的心,然后又夺走了我的尊严 [media=300,50,false,false]http://file2.engok.com/download/ZipMp3100415/20047-1.mp3 [url=http://file2.engok.com/download/ZipMp3100415/20047-1.mp3]http://file2.engok.com/download/ZipMp3100415/20047-1.mp3
- 相关中文对照歌词
- Wait For You (Song For The Ocean)
- Do It For You, Do It For Us
- One For You, One For Me
- One For My Baby (And One More For The Road)
- Forever, For Always, For Certain
- One For My Baby (And One More For The Road)
- Thank Heaven For Little Girls / You Were Meant For Me / A Fellow Needs A Girl
- For Baby (For Bobbie)
- For You, For Me, For Evermore
- One For My Baby (And One More For The Road)
- 推荐网络例句
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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.
曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。
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The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.
稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。
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When I was in school, the rabbi explained everythingin the Bible two different ways.
当我上学的时候,老师解释《圣经》用两种不同的方法。