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A process for the carbonylation of allylic butenyl ether (for example, methyl crotyl ether, 3-methoxybutene-1 and mixtures thereof) or mixture of butadiene and alcohol and production of beta-gamma unsaturated carboxylic acid esters (for example, methyl-3-pentenoate) utilizing a rhodium-containing catalyst for example, dicarbonylacetylacetonate rhodium(I or the like promoted with an iodide-containing compound (for example, HI, AlI3, SnI4, TiI4, CrI3, and CoI2 or the like).

一种将烯丙型丁烯基醚(如甲基巴豆基醚、3－甲氧基丁烯－1及其混合物)或者丁二烯与醇的混合物羰基化的方法，以及由含碘化物化合物(如HI、AlI3、SnI4、TiI4、CrI3和CoI2或等效物)促进，用含铑催化剂如二羰基乙酰丙酮酸铑(I或其等效物制备β－γ不饱和羧酸酯(如甲基－3－戊烯酸酯)的方法。

Impact of PCL capsulation on the mesenchymal stem cell activity studied in vivo, one plate culture with complete culture medium for control group with and two encapsulated transplantation for experimental groups(complete culture medium or basic culture medium for cell suspended) installed,after package and transplantation,retrieving capsulated cells for cell count,MTT assay,CCK-8 assay Daily for 8days to determine cell activity,and analysis growth curve.

以完全培养液平皿法细胞培养为对照组，设2个实验组进行聚己内酯囊管化骨髓间充质干细胞移植细胞活性研究。两个实验组分别以完全培养液和基础培养液悬浮细胞后封装移植，囊管内细胞回收后以细胞计数、MTT法、CCK-8法测定细胞的活性，共8天，进行生长曲线分析。

Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时，再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节；实验中选用CaCl2作为电解熔盐，并对其进行预处理(100℃，保温1小时； 300℃，保温2小时)；经热力学计算，还原钛氧化物的氧分压至少要低于5.11×10-7Pa，结合电解过程中所用熔盐CaCl2有极强的吸水性的特点，电解装置应有较高的密封性，自行设计了一套密封性可靠的电解装置，便于实验过程中熔盐预处理和氧分压的控制；通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时，电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃，实验结果表明电解时间与TiO2质量密切相关，质量越大需要电解的时间越长；通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤，可减少熔盐及其它杂质对电解产物检测结果的影响；最后，通过循环伏安法、计时电流法对电解机理的研究，确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

Revision procedures included 34 (95%) for femoroacetabular impingement, 32 (87%) for labral lesions, 26 (70%) for a chondral defect, 23 (62%) for lysis of adhesions, and 13 (35%) for previously unaddressed instability. Two patients had total hip arthroplasty after revision, and 3 patients required further revision.

修复操作包括34名（95％）因为股骨髋臼损伤，32名（87％）因为唇缘中点损害，26名（70％）因为软骨缺陷，23名（62％）为了粘连松解术，和13名（35％）为了先前位置不稳定。2名病人在修复后接受了全髋关节成形术，3名病人要求更进一步修复。

Thirty-six patients had radiographic evidence of femoroacetabular impingement at the time of revision. Revision procedures included 34 (95%) for femoroacetabular impingement, 32 (87%) for labral lesions, 26 (70%) for a chondral defect, 23 (62%) for lysis of adhesions, and 13 (35%) for previously unaddressed instability.

翻修术时发现有36例患者在股骨头髋臼接触面存在侵犯，关节唇损害32(87%)例，关节软骨缺损26 (70%)例，需要粘连松解术的23 (62%)例，以前关节存在不稳定因素的有13 (35%)例。

In Chapter 5, the software, hardware and mechanical parts of integrated ultrasonic NDT system for parts of complex surfaces are introduced, the software design method for the system is presented, inroduction for each module of the software is given, a detection method for columniform part with composite material is proposed, a complete application example is provided for this part, and experimental results of detection is given.

针对国内棒材检测多为传统的手工超声检测，而现有的大部分自动化超声检测系统难以适应棒材检测的要求的现状，第六章提出了一个包括仿形、五自由度机械手、超声检测成像的一体化棒材自动检测系统。

"A system for enhancing network-browsing speed by setting a proxy server on a handheld device comprises a browser for sending a request for requesting a message from a website and receiving a response in response to the request, a proxy server for transcoding and compressing the request, and transcoding and decompressing the response including the requested message in response to the request, a wireless network communicably linked to the proxy server, Mobile Data Service gateway for transcoding and decompressing the request, and transcoding and compressing the response including the requested message from the website."

是这样的一个系统，在手机端增加一个代理服务器来为一网站请求一条信息发送一个请求，同时为此请求来接受一个反馈，代理服务器压缩和重新编译请求，同时对反馈包括信息请求的反馈进行重新编译和解压缩，无线网络可以转达到代理服务器，Mobile Data Service手机数据服务器路由来编译和解压缩请求并且编译和压缩来自网站的信息请求反馈。

"A system for enhancing network-browsing speed by setting a proxy server on a handheld device comprises a browser for sending a request for requesting a message from a website and receiving a response in response to the request, a proxy server for transcoding and compressing the request, and transcoding and decompressing the response including the requested message in response to the request, a wireless network communicably linked to the proxy server, Mobile Data Service gateway for transcoding and decompressing the request, and transcoding and compressing the response including the requested message from the website."

是这样的一个系统，在手机端增加一个代理服务器来为一网站恳求一条信息发送一个恳求，同时为此恳求来接管一个反馈，代理服务器收缩和重新编译恳求，同时对反馈包孕信息恳求的反馈进行重新编译和解收缩，无线网络可以转达到代理服务器，Mobile Data Service手机数据服务器路由来编译和解收缩恳求并且编译和收缩来自网站的信息恳求反馈。

"A system for enhancing network-browsing speed by setting a proxy server on a handheld device comprises a browser for sending a request for requesting a message from a website and receiving a resp**e in resp**e to the request, a proxy server for transcoding and compressing the request, and transcoding and decompressing the resp**e including the requested message in resp**e to the request, a wireless network communicably linked to the proxy server, Mobile Data Service gateway for transcoding and decompressing the request, and transcoding and compressing the resp**e including the requested message from the website."

是这样的一个系统，在手机端增加一个代理服务器来为一网站请求一条信息发送一个请求，同时为此请求来接受一个反馈，代理服务器压缩和重新编译请求，同时对反馈包括信息请求的反馈进行重新编译和解压缩，无线网络可以转达到代理服务器，Mobile Data Service手机数据服务器路由来编译和解压缩请求并且编译和压缩来自网站的信息请求反馈。

ResultsThe optimized extraction technology for Huang-lian-xiao-ke Granule was as follows: Copis chinensis Franch. and the other four kinds of raw materials in the origin prescription were decocted separately; after soaked for 30min, the coarse powder of Copis chinensis Franch was decocted with 12,10 times water each time and both for 1.5h; after soaked for 30min, the four kinds of raw materials were decocted together for 1.5h just one time with 10 times water.

结果优选出的提取工艺为：黄连与原方中其余四味药分开提取；黄连粗粉浸泡30 min后，用12，10倍量水提取2次，提取时间均为1.5 h；其余4味药一起提取，浸泡30 min，加10倍量水提取1次，提取时间为1.5 h。

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。