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The preparation method is characterized in that:(1) at minus 10 DEG C to 10 DEG C, a chloroauric acid solution with a certain concentration is added into a nano-Pt/C catalyst by ultrasonic or stirring mixture and the atomic ratio of Pt to Au is controlled between 18:1 and 5:1;(2) a small amount of monohydric alcohol or dihydric alcohol or trihydric alcohol of C1-C3 is added and is stirred at minus 10 DEG C to 10 DEG C for 10 min to 5h, so as to prepare the carbon-loading Pt-Au bimetallic nano electro-catalyst;(3) if necessary, the catalyst obtained by the step (2) is treated for 0.5 to 4h at high temperature ranging from 100 DEG C to 700 DEG C in the inert or reducing atmosphere, so as to adjust and control the grain size of the Pt-Au bimetallic nano electro-catalyst.

本发明涉及了一种高稳定性碳载Pt-Au双金属纳米电催化剂的制备方法,其特征在于:(1)在-10~10℃中,将一定浓度氯金酸溶液加入到纳米Pt/C催化剂中经超声或搅拌混合,控制Pt∶Au的原子比为18∶1-5∶1;(2)添加少量C 1 -C 3 的一元、二元或三元醇类,在-10~10℃下搅拌10min-5h,制备了碳载铂金双金属纳米电催化剂;(3)视需要,可将步骤(2)得到的催化剂在惰性气氛或还原气氛中经100~700℃高温处理0.5-4h,可调控Pt-Au/C双金属纳米催化剂的粒径。

Methods Chondrocytes were obtained from the costicartilage of rat and were cultured on the porous HA blocks, 3 mm×3 mm×4 mm size, for three and seven days. Scanning electron micrograph was taken to show whether the cells grew outside and inside the pore of HA block. The cells cultured on tiny glass sheet for 2 days were used to prove where the cells come from by in situ hybridization technique with α1cDNA probe.

采取成年雄性SD大鼠肋软骨细胞,以3 mm×3 mm×4 mm大小的块状多孔HA为载体培养软骨细胞;培养3天和7天后通过扫描电镜观察HA表面和中矢横断面孔隙中有无细胞生长,同时将培养2天的细胞爬片以α1cDNA片段为探针进行原位杂交,求证培养的细胞是否软骨细胞。

After this research work, we know that: HMCM-22 is a better catalyst of selecting naphthalene alkylation; Surface modification of zeolite Y is effective, but the effect of zeolite 3 is not evident and surface modification doesn"t suits mordenite; Surface modification doesn"t affect the frameworks and inner environments of zeolites, but only reduces diameter of orifice and overlays surface acidities; t-butanol is not suitable for alkylating agent of the reaction using modified zeolites as catalyst; Solvents with smaller molecular size are advantageous for naphthalene alkylation reaction using modified zeolites as catalyst, such as cyclohexane is better than decalin.

通过本论文的研究,我们知道:HMCM-22是萘择形烷基化反应较好的沸石之一;Y沸石的外表面改性效果较好,β沸石则效果不明显,而丝光沸石则不适于外表面改性;外表面改性不改变沸石的骨架结构和孔道内部环境,仅减小孔口直径和覆盖外表面酸性位;叔丁醇不适于作外表面改性沸石催化的反应的烷基化试剂,其反应活性很低,且选择性无明显提升;分子较小的溶剂更适于外表面改性沸石催化的反应,环己烷就明显好于十氢萘。

Supersonic wave disperse research indicated, ethanediol as the disperse medium, it could got suspending liquid about for firve days, but relatively large in grain size. However, combined use of lauryl sodium sulfate and maleic anhydride as disperse medium, the disperse result among water was better than the former, and it would be steady for two days.

超声分散研究表明,使用聚乙二醇作为分散介质,可得到分散五天左右的悬浮液,但分散后粒度较大,使用十二烷基硫酸钠和顺丁烯二酸酐混合作为分散介质在水中分散效果较好,可稳定两天左右。

1St, Luo grain was truly the worker has made the mistake, we will correct 2 in the following sample, because in the order form, has not mentioned this model of scarf's conclusion way, therefore the factory was before pulled the way did, was sorry, we will press your request and the reference diagram manufacture pre-natal type 3, because scarf's span was 64 ", gibbed long 4 ", and in the design drawing, requested scarf's two homochromies, this was unable to achieve, therefore the factory in the permission error range, has adjusted the altitude which gibbed, guaranteed the total lengthWith matches colors correctly, please give your opinion,(the note: This section does not use translator, is only facilitates everybody understanding, the scarf is the black salt bi-color strip, also requests two is the gray, gives the size according to the order form, can only make 16 strips, therefore is impossible to achieve two homochromies, can only make 15 statures, or 17 statures only then the line) dyes the big goods gauze approximately to need for 5-7 days, afterward can prepare the pre-natal type, waited for that your reply opinion, thanks

外贸新手,第一个自己的订单,比较紧张,怕语气拿捏不好,请教各位啊:关于您的意见: 1,罗纹确实是工人做错了,我们会在后面的样品中更正 2,由于订单上,并没有提到这款围巾的收尾方式,所以工厂是按照之前打样的方式做的,抱歉,我们会重新按您的要求和参考图制作产前样 3,因为围巾的全长是64&,夹条长4&,并且设计图上,要求围巾的两头同色,这是无法做到的,所以工厂在允许的误差范围里,调整了夹条的高度,以保证总长和配色正确,请给出您的意见,(注:这段不用翻译,只是方便大家理解,围巾是黑灰双色条子,又要求两头是灰色,按照订单给出的尺寸,只能做16个条子,所以是不可能做到两头同色,只能做15个条,或17个条才行)染大货纱约需要5-7天,之后才能准备产前样,等待您的回复意见,谢谢问题补充:别整翻译工具。。悠关前途''谢谢

The results showed that (1) The grain size of nanometer YiO_2 was40~80nm.The wavelength corresponding to the maximum absorbency values were observedin the 200~320nm range.The crystal structure of carbon doped TiO_2 photocatalyst is primarilyanatase(22.43% rutile), and the content of carbon is about 4.6%.(2) The relative humidityvaring from 8% to 80%, the photocatalytic degradation degree of benzene increased withincreasing relative humidity; and to toluene, degradation rate was hanced by relative humidityup to 60%, and more or less inhibited above 60%.(3) Scheme and results of orthogonal testswere used by evaluating the photocatalytic performance of the gas phase methanol, acetoneand 1-heptane.The results revealed that their degradation degree reached 84.5%, 93.39% and93.45%, respectively.(4) The 254nm UV lamp showed higher photocatalytic degradation rate.For methanol, acetone and 1-heptane, it was found that photocatalytic degradation reactionoccurs with the light strength of daylight lamp.(5) Under the the same conditions, 15%degradation degree has been obtained for benzene, whilst about 10% degradation degree wasattained by Degussa P25; During the initial phases, the toluene revealed higher photocatalyticactivity, comparing with Degussa P25, the degradation degree of methanol, acetone and1-heptane were slightly lower.

结果表明:(1)CVD法制备的纳米TiO_2光催化剂,颗粒球形度好、粒径在40~80nm之间;最大吸光度值所对应的波长为200~320nm;含碳量约为4.6%;晶型组成主要为锐钛矿型,金红石的含量约为22.43%;(2)在相对湿度为8%~80%范围内,苯的光催化降解率随着相对湿度的增大而增大;甲苯在相对湿度为60%时达到最好降解效果,当相对湿度增大到80%时光催化效果降低;(3)将正交实验设计及实验方案应用于气相甲醇、丙酮和正庚烷光催化降解研究,实验结果表明:三者最高降解率分别为84.5%、93.39%和93.45%;(4)有254nm紫外灯参与的光催化实验可以大大提高有机气体的光催化降解率;在日光灯的照射下,掺碳纳米TiO_2对气相甲醇、丙酮和正庚烷具有一定的光催化氧化能力;(5)较P25粉,在相同的光催化操作条件下:气相苯的平均降解率达15%,高于P25粉10%的降解率;气相甲苯在初始阶段具有较高的反应速率;气相甲醇、丙酮和正庚烷的降解率略低于P25粉。

Hoofy and Boo staked their claim as the Wall Street bull and bear, our loyal community manifested in size and scope, Kevin was president and The Ruby Peck Foundation -- named for my grandfather -- was on its way to raising a seven-figure donation for children's education.

呼呼&和&嘘嘘这两个卡通角色作为华尔街牛熊市的象征深入人心,网上社区的规模和影响力不断扩大,凯文成为Minyanville的总裁,而鲁比派克基金会─以我祖父命名的慈善组织─正在为儿童教育募集七位数的善款。

With this inerratic change for the power of QTL detection,suitable experimental sample size could be roughly determined in practice pursuant to the degree of selection in the population of interest prior to experiment in order that the statistical power for QTh mapping would not decline because of the presence of selection in the population.

这种偏差根本上是由QTL基因型与多基因之间负的连锁不平衡以及QTL与标记之间的连锁不平衡所造成的。 2)目前QTL定位实践已找到了一些具有育种意义的主效位点。

Objective To analyze the CT and MRI manifestations of oral carcinoma,and to evaluate the value of imaging technologies in the diagnosis of oral carcinoma,thus to explore the most reasonable imaging method Methods 46 cases with oral carcinoma,proved by surgery and pathology (2 lip tumors,8 carcinomas of the gingival ridge,5 carcinomas of the buccal mucosa,24 tongue carcinomas,5 carcinomas of the floor of the mouth,2 tumors of the hard palate),were analysed retrospectively32 cases were examined with CT and 14 cases with MRIImaging presentations were compared with surgery and pathology Results Of the 46 cases with oral carcinoma,22 were ulcerative lesion of infiltrative growth,24 were masslike lesion of extruded trowthOf the 32 cases examined with CT scan,27 were detected,5 were missed,the 4 missed cases were confirmed to be superficial ulcers by surgery and pathologyOf the 10 cases with bone destruction examined with CT scan,8 were manifested,2 were missedAnd of the 14 cases with MRI scan,all 14 were detected Conclusion CT and MRI scan are valuable for diagnosis of oral carcinomasThey can manifest the morphology and size of primary tumor,contiguous structures,bone invasion and cervical lymph node metastasisMRI is the optimal imaging method for superficial ulcerative lesion of infiltratibe growth

徐 锋,罗德红,唐威,欧阳汉,周纯武目的分析口腔癌的CT及MRI表现,评价影像检查在口腔癌诊断中的应用价值,探索合理的影像学检查方法。方法回顾性分析经手术及病理证实的口腔癌46例(唇癌2例,牙龈癌8例,颊黏膜癌5例,舌癌24例,口底癌5例,硬腭癌2例),其中32例行CT扫描,14例行MRI扫描,将影像表现与手术所见及病理结果进行对照分析。结果 46例口腔癌中,呈浸润性生长的溃疡型病变22例,外生性生长的肿物型病变24例。CT扫描32例,明确显示病变27例,遗漏病变5例,其中4例为表浅溃疡型病变。CT扫描病例中,10例有骨质侵犯,CT扫描准确评价8例,遗漏2例。MRI扫描14例,均准确评价肿瘤及其与周围结构的关系。结论 CT、MRI对口腔癌原发肿瘤的形态、大小、周围结构侵犯、颈部淋巴结转移的评价有重要价值。对于较小及呈浸润性生长的表浅溃疡型肿瘤,CT扫描尤其是CT平扫难以准确显示,应首选MRI。

Objective To analyze the CT and MRI manifestations of oral carcinoma,and to evaluate the value of imaging technologies in the diagnosis of oral carcinoma,thus to explore the most reasonable imaging method Methods 46 cases with oral carcinoma,proved by surgery and pathology (2 lip tumors,8 carcinomas of the gingival ridge,5 carcinomas of the buccal mucosa,24 tongue carcinomas,5 carcinomas of the floor of the mouth,2 tumors of the hard palate),were analysed retrospectively32 cases were examined with CT and 14 cases with MRIImaging presentations were compared with surgery and pathology Results Of the 46 cases with oral carcinoma,22 were ulcerative lesion of infiltrative growth,24 were masslike lesion of extruded trowthOf the 32 cases examined with CT scan,27 were detected,5 were missed,the 4 missed cases were confirmed to be superficial ulcers by surgery and pathologyOf the 10 cases with bone destruction examined with CT scan,8 were manifested,2 were missedAnd of the 14 cases with MRI scan,all 14 were detected Conclusion CT and MRI scan are valuable for diagnosis of oral carcinomasThey can manifest the morphology and size of primary tumor,contiguous structures,bone invasion and cervical lymph node metastasisMRI is the optimal imaging method for superficial ulcerative lesion of infiltratibe growth

中华硕博网核心提示:徐锋,罗德红,唐威,欧阳汉,周纯武关键词:口腔肿瘤目的分析口腔癌的CT及MRI表现,评价影像检查在口腔癌诊断中的应用价值,探徐锋,罗德红,唐威,欧阳汉,周纯武目的分析口腔癌的CT及MRI表现,评价影像检查在口腔癌诊断中的应用价值,探索合理的影像学检查方法。方法回顾性分析经手术及病理证实的口腔癌46例(唇癌2例,牙龈癌8例,颊黏膜癌5例,舌癌24例,口底癌5例,硬腭癌2例),其中32例行CT扫描,14例行MRI扫描,将影像表现与手术所见及病理结果进行对照分析。结果46例口腔癌中,呈浸润性生长的溃疡型病变22例,外生性生长的肿物型病变24例。CT扫描32例,明确显示病变27例,遗漏病变5例,其中4例为表浅溃疡型病变。CT扫描病例中,10例有骨质侵犯,CT扫描准确评价8例,遗漏2例。MRI扫描14例,均准确评价肿瘤及其与四周结构的关系。结论 CT、MRI对口腔癌原发肿瘤的形态、大小、四周结构侵犯、颈部淋巴结转移的评价有重要价值。对于较小及呈浸润性生长的表浅溃疡型肿瘤,CT扫描尤其是CT平扫难以准确显示,应首选MRI。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。