查询词典 flying column

Different chromatographic parameters including elution profiles, column temperature were investigated in order to optimize separation conditions of different fatty acid phenacyl ester derivatives. A gradient elution using methanol/acetonitrile (90:10, V/V)-water as mobile phase at 0.35 mL/min, detection wavelength at 246 nm, and column temperature of 35℃ were chosen.

经优化确定以(90：10)-水为流动相梯度洗脱，在检测波长246 nm，柱温35℃，流速0.35 mL/min的色谱条件下，18 min内能完成对13种脂肪酸衍生物的分离检测。

The presumption that new technology about distillation column with a single reactor can be used in photochlorination of acetic acid is first proposed in this paper. The fact that reaction distillation has obvious advantages in the number of theoretically perfect trays and energy consumption was obtained by theoretical analysis between the coupling of reaction and distillation and the independent operation, which lays a theoretical foundation on the application of the distillation column with a single reactor in photochlorination of acetic acid.

本文首次提出了将背包式反应精馏耦合技术应用于乙酸氯化反应的设想，通过对反应精馏耦合和反应精馏独立操作两种情况进行理论分析，发现反应精馏耦合在理论板数、能耗方面均具有明显优势，因而为背包式反应精馏应用于乙酸光氯化反应奠定了理论基础。

For product column T202 top, except that very small amount of benzoic acid and phthalide were contained, the rest was benzene anhydride, the column bottom was heavy component, which can meet the separation requirement.

产品塔T202塔顶除含有极少量苯甲酸、苯酞外，其余均为苯酐，塔底为重组分，满足分离要求。

Cis-butendioic anhydride, benzoic acid and phthalide in light fraction column T201 were removed on the column top, the overhead component: benezene anhydride 25.74%, cis-butendioic anhydride 39.11%, benzoic acid 25.37%, phthalide 9.78%.

轻组分塔T201中顺酐、苯甲酸、苯酞都在塔顶被除去，其中塔顶组成：苯酐25.74%，顺酐39.11%，苯甲酸25.37%，苯酞9.78%。

The eruptive pattern of the Chifeng phase is: Plinian column (the Chifeng pumice fall deposits)→pyroclastic flow (the Changbai pyroclastic flow deposits)-lahar mainly triggerd by pyroclastic flow. The eruptive pattern of the Yuanchi phase is from Plinian column (the Yuanchi pumice and ash fall deposits)→pyroclastic flow (the Bingchang pyroclastic flow deposits).

赤峰期喷发模式为：普林尼式喷发柱－火山碎屑流－火山泥流，主要由火山碎屑流诱发火山泥流；园池期火山喷发模式为：普林尼式喷发柱－火山碎屑流。

Calcium humic acid resin is synthesized by one step gel method. With the column filled with the resin made,the column poiser kept at pH 5～6, and with 0.01 mol/L HCl as an eluent, Ca 2+, Mg 2+ can be separated quantitatively.

利用一步凝胶法合成了钙型腐植酸树脂，用自制树脂装柱，控制柱平衡液的pH为5～6并以0.01mol／LHCl为洗脱液，使Ca2＋、Mg2＋离子与其它12种离子定量分离。

Besides off-column preconcentration, on-column preconcentration method has been attracting a lot of researchers because of its simplicity.

采用同样的装置，本论文首次建立了毛细管电泳分析血浆中的维甲酸异构体的方法，灵敏度提高100倍以上。

The rutile inclusions have protogenetic and syngenetic stages. The protogenetic rutile inclusions are of fragmentation. The syngenetic rutile inclusions are mainly short column, and some are long column.

其中，金红石包裹体可分为先成与同生两种，先成金红石包裹体可见破损现象，同生金红石包裹体主要呈短柱状，部分为长柱状。

RESULTS Pyr column coupled with Cyano column was more suitable for seperation.

柱串联，夏天无中原阿片碱和延胡索乙素能较好地分离。

Methods: We use head-space GC method, chromatographic conditions are carried out as following: the flexibility quartzose capillary column, the temperature of column is 90℃, injection temperature is 150℃, equivalence temperature is 80℃ and time is 30 mins, quantization imp temperature is 90℃, transfer line temperature is l00℃.

采用顶空法，在极性弹性石英毛细柱上进行各组分分离，效果良好。柱温：90℃，进样口温度150℃，顶空瓶平衡温度80℃，平衡时间30分钟，定量环温度90℃，传输线温度100℃。

Nowadays, most of research are to build a transmutative Petri Nets through adding controlling place sets, controlling arc sets and controlling policy to the basic Petri Nets, while the Controlled Petri Nets could be used to argue many controlling theory problems conveniently and to induce many logically and physically supervisory and solve the Event Feedback Controlling Problems and State Feedback Controlling Problem in DEDS supervisory theory.

目前大多数的研究表现为在变形后的受控Petri网基础上，利用各种方法求得各种逻辑型、结构型控制器，解决DEDS监控理论中的事件反馈控制问题与状态反馈控制问题。

On one hand, there are discussions with the works council and union about extension of short time working up to the end of September.

一方面，有讨论，工程理事会和联盟关于延长工作时间短至9月底。