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The total flavonoids content of peanut hulls of different sources were evidently different,those peanut hulls contained more total flavonoids from Shandong province,higher maturity and raw. This suggested that attention should be paid to the choice of peanut hulls as medicine materials. 3.The optimized extraction technology conditions considering the two indices of total flavonoids andβ-sitosterol were: the peanut hulls were extracted by 95% acohole 6 times of the hulls weight refluxing for 2 hours first,and extracted by 70% acohole 4 times of the hulls weight refluxing for 2 hours at the temperature below 80℃successionally,then the concentrate was dried vacuumizedly with the additament of starch 2% of the concentrate weight after the extracts were fitrated,united and concentrated. 4.The dried extract powder possessed high hygroscopy and low fluidity,but the weight variation of capsule contents could comply with the requirement of CP if it was mixed with dextrin and granulated by sieving 40 meshes using 95% ethanol as the wetting agent,and filled into capsules after dried below 60℃.The critical relative humidity of the granules was about 63%.

不同来源的花生壳总黄酮含量有较大差异,山东产区、成熟度高的及未经炒制的花生壳总黄酮含量较高,提示作为药材时应注意选择; 3、兼顾总黄酮及β-谷甾醇的最佳提取工艺为:先以95%乙醇6倍量加热回流提取2小时,再以70%乙醇4倍量80℃以下回流提取2小时,提取液过滤、合并、浓缩,加2%淀粉60℃以下减压干燥; 4、浸膏粉吸湿性大,流动性差,但加糊精并以95%乙醇为润湿剂、过40目筛制粒,60℃以下烘干后填充胶囊,可保证装量差异符合要求;颗粒临界相对湿度约为63%。

Safflor Yellow, extracted from Safflor, with proved pharmacological effect that can expand coronary artery, lower blood pressure, resist thrombus, endure anoxemia and restrain immunity, will have a good developing and applying future. Since 1970s, more than 200 kinds of components such as flavone, lignocelluloses and alkine, have been extracted from Safflor.

红花黄色素(Safflor Yellow,SY)是从红花中提取的有效成分,具有扩冠、降压、抗血栓、耐缺氧、免疫抑制等多种药理学功效,有良好的开发和应用前景。70年代以来对红花的化学成分进行了广泛的研究,已分离出了二百多种化学成分,其中主要有黄酮类、木脂素类、多炔类等。

The results showed that either of the extracted propolis had significant inhibitory effect on the level of triglyceride, total cholesterol, LDL-C,GPT and GOT in serum, and TC, TG and MDA in liver, but were ineffective on HDL-C, MDA, SOD and NO levels in serum. Ethanol extracted propolis also reduced the body weight, liver weight and liver index of hyperlipidemic SD rats, while water extracted propolis were adiaphorous.

结果表明:蜂胶醇提液和水提液均能有效抑制高脂血症SD大鼠血清中的甘油三酯、总胆固醇、低密度脂蛋白、谷丙转氨酶、谷草转氨酶的升高,并且能有效抑制肝脏组织中的TC、TG、MDA的升高,但对血清中的高密度脂蛋白、超氧化物歧化酶、丙二醛、一氧化氮的影响不明显;蜂胶醇提液能有效降低高脂血症SD大鼠的体重、肝重及肝指数,蜂胶水提液对体重、肝重及肝指数的影响则不显著。

The extracted components were qualitatively and quantitatively analyzed by gas chromatography mass spectrometry.The results showed that 30,26 compounds were identified from the volatile components extracted by DSE,SDE methods resp.36 kinds of components were extracted by 2 methods in total,among them the content of hexadecanoic aci...

结果表明,从DSE、SDE法提取的挥发性成分中分别鉴定出30(总含量58.24μg/g)、26种化合物总含量(86.66μg/g,2种方法共提取出36种化合物,其中十六酸含量最高,其次为亚油酸、油酸、邻苯二甲酸二异丁酯、间甲苯甲醛、龙脑。

When initial NO3--N was leached, the correlation coefficients between soil initial NO3--N and mineral N extracted by CaCl2 before aerobic incubation with raygrass nitrogen uptake were decreased to 0.613 and 0.607, respectively, and both reached 5% significantly level. However, the correlation coefficients between mineralizable N extracted by aerobic incubation, soil initial mineral N and mineralizable N extracted by aerobic incubation, N0 and soil initial mineral N and N0 with raygrass nitrogen uptake were raised obviously, and all reached 5% and 1% significant level.

以不包括土壤起始NO3--N盆栽试验植物吸氮量为参比,通气培养前CaCl2淋洗起始NO3--N和起始矿质氮与五期黑麦草地上部氮素累积量间的相关性尽管有所降低,但相关性仍达5%显著水平,相关系数分别为0.613和0.607;而通气培养30周矿化氮素、土壤起始矿质氮+通气培养30周矿化氮素、N0及N0+起始矿质氮与五期黑麦草地上部吸氮量的相关系数却明显提高,相关系数分别为0.718,0.782,0.688 和0.640,均达5%或1%显著水平。

The results indicated that when initial NO3--N was not leached, soil initial NO3--N and mineral N extracted by CaCl2 before aerobic incubation were closely related with raygrass nitrogen uptake, the correlation coefficients were 0.856 and 0.862, respectively, both reached at 1% significant level. When initial NO3--N was leached, it was no good relationship between mineralizable N extracted by aerobic incubation, soil initial mineral N and mineralizable N extracted by aerobic incubation, N0 and soil initial mineral N and N0 with raygrass nitrogrn uptake, the correlation coefficients were 0.410, 0.553, 0.492 and 0.419, respectively, indicating that the poor effects of mineralizable N on reflecting soil N capacity were influenced and disturbed by initial nitrate.

以包括土壤起始NO3--N盆栽试验植物吸氮量为参比,通气培养前CaCl2所淋洗起始NO3--N和起始矿质氮与5期黑麦草地上部氮素累积量密切相关,相关系数分别为0.856和0.862,达1%显著水平;与此相反,通气培养30周所矿化氮素、土壤起始矿质氮+通气培养30周矿化氮素、氮素矿化势(N0)及N0+起始矿质氮与5期黑麦草地上部氮素累积量间无显著相关关系,相关系数分别仅为0.410、0.553、0.492和0.419。

Water samples were extracted and purified and collected by solid-phase extraction LC-18 column. Soil samples were extracted by ethyl acetate/petroleum ether (2:1, by vol) and purified by sulphonation. Wheat sample was extracted by acetonitrile/water (4:1, by vol) and purified and collected by SPE- Florisil column.

水样直接用LC-18固相萃取小柱分离、净化和富集;采用乙酸乙酯/石油醚(体积比2:1)振荡提取,磺化法净化,测定土壤中氯氟吡氧乙酸残留量;以乙腈/水(体积比4:1)为提取剂,氟罗里硅土固相萃取小柱分离、净化,测定小麦样品中氯氟吡氧乙酸的残留量。

In this paper, a total of 56 relatively nonpoint source pollution sediment samples were collected from the tidal flats of the Jiuduansha shoal and the Chongming island of the Yangtze river estuary. The main properties i. e., grain size distribution, contents of DCB (dithionite citrate bicarbonate extracted iron Fe(subscript d, AAO extracted iron Fe(subscript o, total Fe, DCB extracted Mn Mn(subscript d, total Mn, organic matter, magnetic susceptibility of the samples, as well as the concentrations of Cu, Zn, Pb, Cr, Cd and Ni in the samples, were determined. Basing on the data, the relation of the sediment properties to heavy metal concentrations was evaluated with pearson's rank and partial rank correlation analysis.

采集长江口无明显点源污染的崇明东滩和九段沙潮滩56个沉积物样品,测定沉积物原样和粘粒中Cu,Zn,Pb,Cr,Cd和Ni的含量以及沉积物的主要性状(粒径分布、游离铁、活性铁、总铁、游离锰、总锰、有机碳和磁化率等),以相关分析和偏相关分析研究沉积物中重金属含量与沉积物主要性质之间的关系。

He results show that the virus regained infectivity, and the tannins did not direct viricidal effect. Tannins extracted from Polygonum perfoliatum or Archontophoenix alexandrae seeds showed strongly anti-TMV activities separately. TMV virions seems to be aggregated when TMV incubated with the tannins by electron microscope. It seems that TMV coat protein bind to the tannins based on PAGE. Tannins did not reduce infectivity when applied either before or after TMV inoculation. It is proposed that tannins extracted from the 11 species inhibited TMV by binding with TMV coat protein to interfere with recognition site essential for viral coat protein. Tannins extracted from Euphorbia hirta, P. perfoliatum, P. cuspidatum reduce infectivity when applied immediately in N.

MV分别与这11种植物单宁混合后,通过透析除去单宁后,可恢复大部分侵染力,表明单宁对病毒粒体并无直接毒害作用;TMV与杠板归和假槟榔种子中提取的单宁分别混合后,电镜下观察粒体呈现明显的聚集现象;TMV外壳蛋白分别与这两种植物单宁混合后,聚丙烯酰胺凝胶电泳中CP泳带滞后;单宁在病毒接种前施用未降低TMV对叶片的侵染能力;这些结果表明植物单宁对TMV抑制作用可能是单宁与TMV-CP结合影响病毒对叶片侵染位点的识别而降低TMV侵染性,而这种结合是可逆的。

After peltate yam is water washed, crushed, fermented and acid hydrolyxed, the solid matter and acid water solution are separated via centrifugation, the solid matter is extracted with organic solvent to make saponin extracted into organic phase, the organic phase is back extracted to eliminate other components, the organic solvent is distillation recovered for reuse and precipitation separated saponin is stoved to obtain product.

黄姜经水洗净、粉碎、发酵和加酸水解后,离心分离固体物和酸性水溶液,用一种有机溶剂萃取固体物,皂素被萃入有机相中,经返萃取去除其它成分后,将有机溶剂蒸馏回收,重用,沉淀析出的即为皂素,经烘干即得产品。

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每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

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