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The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究，实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先，利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维，比较不同的热处理温度与反应时间的改变对产物生成产生影响，进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示，结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现，若热处理温度在100~4750C下可得到Cu23Cl奈米粒，475~4900C 可得Cu奈米粒，450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时，可产生直径比较细的纤维，纤维直径为107 88±21 01nm；且由於奈米金属颗粒镶嵌在二氧化矽纤维中，直径比较细的纤维，可以得到比较小的奈米金属颗粒，这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时，由於表面电浆子共震关系，而使纤维颜色由淡白黄绿色变成黄绿色，再变红褐色。由实验结果得知，利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度，可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

Properties of FRP materials have been improved by experimental and analysis on hybrid of two or three kinds of fiber, and various products have been manufactured accordingly. At the same time, the resin and equipment that are suitable for those FRP materials have been developed. A series of key applied techniques, such as strengthening of steel structures, masonry structures and concrete structures reinforced with prestressed FRP, lossless inspectability of structures and so on, have been developed though experimental research according to requests of engineering. There are four codes and guidelines for applying FRP techniques to construct foundational establishment. Among them, one technical specification was published in May 2003. It can be standardization of applying FRP materials on engineering. There have been more than one hundred engineerings strengthened with FRP materials since 1999 based on research and investigation of FRP materials and techniques.

在材料改性研究以及产品开发方面，通过纤维混杂改性，开发出适用于不同工程要求的单一品种纤维和混杂纤维的FRP产品及配套树脂材料、配套设备机具等；在关键应用技术开发方面，根据工程需要，开发出钢结构加固技术、砌体结构加固技术、预应力加固技术、结构无损检测技术等基础设施建设中应用FRP材料的关键技术；在规范标准编制方面，主持编制国家规范标准4项， 1项已获批准实施，其它3项正在按计划进行；在工程应用方面，应用自主开发的材料和技术，改造、加固工程100多项，创造了巨大的经济效益及广泛的社会效益。

The research uses the pretest-posttest nonequivalent quasi-experimental design of accurate experimental methodology. This research is carried out about 6 weeks on second graders at K.M.

本研究采不等前后测设计之准实验研究方式进行，以桃园县光明国小二年级两个班级的学生为对象，进行六周的教学实验。

Fluidization and Sounding Pressure Characters Experimental Research on Pulsating Fluidized Bed After verifying experimentally the Rijke type self-exciting pulsating fluidized bed combustion, under different operating conditions (different empty cross-section wind speed and inaction bed height), experimental research the oscillation characters of sounding pressure in the pulsating fluidized bed. The results indicate that the sound characters in the Rijke type self-exciting pulsating fluidized bed combustor are the same with it in the Rijke type combustor, the pressure in the combustor oscillate up and down in the sinusoidal manner and the pressure is the superposition of the multiple harmonic waves.

脉动流化床流化与声学压力特性实验研究在实验验证了Rijke型自激脉动流化燃烧概念后，在不同运行条件(空截面风速、静止床层高度)下，实验研究了Rijke型自激式脉动流化床的声压振动特性，研究结果表明：脉动流化床内建立起的声波特性和Rijke型脉动燃烧器内的一样，各点压力呈正弦规律上下振动，且压力是基波幅值最大的多次谐波的叠加。

The simulations in this dissertation, however, strictly mimic the experiments. With the research methods similar to the experiments of glycolytic extracts, the experimental phenomenon ? temporal target waves are first reproduced in numerical simulation, and irregular continuous target waves and spatiotemporal turbulences are observed by elevating the magnitude of the local perturbation which pioneers new directions for the experimental research of glycolytic reactions.

而本文在模拟中严格仿照实验条件，采用酵母抽提物实验中对酵解波的研究方法，第一次在数值模拟中重现了实验现象——暂态靶形波，并通过增加局域扰动的幅度观察到了非规则的连续靶形波和时空湍流，为酵解反应的实验研究开辟了新的方向。

The experimental setup for the turbulent jets in crossflow is designed, and the hot wire anemometry IFA 300 is used to measure the velocity field and the turbulent kinetic energy, and the computational result matches experimental measurement reasonably well. The experimental result is very important in the analysis of the flow field, deduction of the equation of the jet trajectory, check of the turbulence model and validation of the numerical method.

首先，建立了用于测量横向紊动射流的实验台，并利用IFA 300型热膜风速仪系统测量了多种工况下的流场，并将速度、湍动能结果与数值计算结果进行了比较，实验结果与数值模拟结果吻合较好，从而为分析流场特性、确定射流轨迹、比较湍流模型以及验证数值计算方法提供了依据。

The nitrogen balance on days 8 was remarkably improved in experimental and normal diet groups compared with control group. There were highter serum glutamine and BCAA concentration, hydroxyproline content and tensile strength of wound, and better lymphocyte blastogenesis in experimental group compared with control and normal diet groups. Experimental and normal diet groups had higher mucosal DNA, RNA and protein content than control group.

实验组动物的血浆谷氨酰胺、BCAA含量，外周血淋巴细胞转化率，伤口皮肤抗张力强度和羟脯氨酸含量都显著高于对照组和正常饲料组(P＜0.05)；实验组和正常饲料组动物第8天氮平衡，小肠粘膜核酸和蛋白质明显高于对照组(P＜0.05)。

This paper to introduce a new experimental method of dispersion phenomena, in this experimental method, it can be directly observed by different substances uneven medium, the dispersion arising from the various phenomena of the material in different light source through uneven medium, the emergence of two different spectral dispersion surface, spectral noodles Bright (Bright-Line Spectrum), and dark lines is how it is formed and a series of important experimental phenomena.

本文要介绍一种新的色散现象出现实验方法，在这种实验方法上，可直接观察到不同物质通过不均介质后，所出现的各种不同色散现象，物质在不同光源照射下通过不均介质后，出现的两种不同色散谱面，谱面中明线和暗线是怎样产生等一系列重要实验现象。

In view of practical problem during Sulige gas field development, this paper complete follow study content. Study material balance theory of two district compound gas reservoir. Carry out stress sensitivity experiment on matrix rock and labor created fracture core from Sulige gas field with America Core Company high pressure high temperature flow experimental instrument to study stress sensitivity change rule of different permeability matrix rock and created fracture core at the condition of time and again switch on and off well and different drawdown pressure. Carry out depletion experiment on matrix rock of different permeability serial combination with different kinds of allocation, using double core clamper serial connected experimental apparatus, to study gas well production performance of bi-zonal compound low permeability reservoir during low pressure production stage. At the basis of experimental study, establish single well simulation model to analyze development index infection caused by stress sensibility and production performance infection rule caused by inner formation and outer formation of bi-zonal compound gas reservoir permeability variation while considering stress sensitivity.

针对苏里格低渗气田开发中存在的实际问题，完成以下研究内容；研究了两区复合气藏物质平衡原理；利用美国岩芯公司高温高压流动实验仪，对取自苏里格气田基质岩芯和人工造缝岩芯进行应力敏感实验，研究不同渗透率基质岩芯和造缝岩芯在多次开关井和不同生产压差条件下的应力敏感变化规律；采用双岩芯夹持器串联实验装置，对不同渗透率串联组合的基质岩芯进行各种配产条件下的衰竭实验，研究两区复合的低渗储层气井在低压生产阶段的生产动态特征；在实验研究的基础上，建立单井模拟模型分析储层应力敏感性和非均质性对开发指标的影响，研究考虑应力敏感时两区复合气藏储层中内区和外区渗透率变化对开发动态的影响规律。

In addition, some modifications on several computational methods are also presented. Using LMTO method the electronic structure of several systems are studied, and some results are obtained. They are: The ideal Nb (100) surface has three surface states, the multi-layer relaxed surface has two surface states. The surface energy of the ideal surface is higher than that of the relaxed surface, that means that the multi-layer relaxed surface is more stable than the former one, which supports the LEED results. The mono-layer relaxed Ag (111) surface is the most stable one among several" stable surface models"presented by several researchers. The surface energy of Ag (111) surface is higher than that of surface Ag (001), which supports some experimental results such as different reaction rate at different surface orientations for the same material. The surafce states of Si (111) surface not only locate near the Fermi level, but also in the valence band, which agrees well with Cohen's conclusion. Si (111)-H is an effective model for analysing the surface states and H adsorbed on the back surface is a good method for improving the convincingness of the results obtained on thinner slab models. The surface stability depends on three different kinds of MoSi〓(001) surfaces, the surface with mono-layer Si is the most stable one, and the surface with Mo at the first layer is the most unstable one among them. These are consistant with the Kemoda's experimental results. The valence bands of clean or K adsorbed CdTe (111) surface agrees well with the synchrotron radiation studies. The surface of CdTe (111) consists of four kinds of surface models which show different surface electronic structures and different surface structure stabilities. The conclusion agrees well with Wu's experimental work. The different absorbed alkali metals on the CdTe (111) surface give different adsorption characteristics which have relations not only with the valence electrons, but also with the core ones of the alkali metals. The electonic structures of Si-C alloys are different from that of Si-Ge alloys, and the energy band gaps of Si-C alloys do not increase linearly with Carbon concentration, our conclusion supports Alexander's results, but conflicts with Soref's one.

现分述如下： LMTO方法及其应用方面：1）通过对Nb（100）表面电子态分析发现清洁理想表面有三个表面态，多层弛豫表面有两个表面态；表面能大小说明多层弛豫表面更稳定，支持了LEED结果。2）通过对采用不同方法获得的几种不同Ag（111）表面稳定结构的表面能计算分析，给出了单层弛豫表面为Ag（111）表面的最稳定结构；从Ag（111）单层弛豫表面和Ag（001）表面的表面能比较，发现了Ag（001）表面表面能要比Ag（111）小的，表明了同种物质不同表面取向将表现出不同物理、化学性质，这是与实验中得出的结论是吻合的，3）通过对Si（111）表面态分析，不仅发现了Si（111）表面不仅具有居于费米能级附近的悬挂键所对应的表面态，而且还有很多表面态位于价带能量范围内，与Cohen等结果一致，H饱和slab模型背表面相当于增加了slab层的厚度，是一有效的变相增加slab层厚的方法，弛豫表面较清洁理想表面价带谱们低能端的少许移动，预示着总能降低，说明弛豫表面较清洁理想表面稳定。4）MoSi〓具有三种表面，从费米能级上态密度值大小得到单层Si表面最稳定，Mo原子为表层原子的表面最不稳定，双层Si原子表面居中的结论，这与Kemoda等人实验结果是一致的。5）通过对CdTe（111）表面表面电子态、表面结构稳定性及表面H、碱金属吸附的电子结构系列研究，不仅得出了CdTe（111）清洁及碱金属K吸附价带谱与同步辐射光电子谱相吻合的结果，而且发现了CdTe（111）表面具有四类不同原子近邻特征，表现出四类不同的表面结构及电子结构特征：不同表面态分布、不同的表面结构稳定性（表层原子与次层原子成三键有一悬挂键的表面要比表层原子与次层原子成一键有三悬挂键稳定（与Wu等人实验结果一致））、不同的H吸附特性。

Researches reveal that students who suffer from corporal punishment tend to resort to violence in their future life.

研究表明遭受过肉体惩罚的孩子倾向于在他们今后的人生中使用暴力。

Total sugar of sarcocarp and chlorophyll of pericarp increased firstly, and then decreased afterward along with altitude; Titratable acidity, ascorbicacid and anthocyanin of pericarp were increased along with altitude; The content of protein increased firstly and decreased afterward along with altitude; Carotenoid of pericarp were decreased along with altitude.

果肉总糖和果皮叶绿素含量随海拔高度升高先升高后降低；可滴定酸、维生素C和果皮花青苷含量均随海拔升高而升高；蛋白质在1720m处最大，1420m处最小；果皮类胡萝卜素随海拔升高而降低。