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A method for synthesizing sodium sulfoacetic is discussed,which sodium sulfoacetic is synthesized with sodium sulfite and ethyl monochloro acetate,with sodium sulfite and chloroacetic acid.

主要分别介绍用亚硫酸钠与氯乙酸乙酯合成磺酸乙酸钠和亚硫酸钠与氯乙酸合成磺酸乙酸钠。

Water, methanol and ethyl acetate extraction method were used to extract non-oil components from Myrtus communis Linn. leaves, and then radical scavenging activity and antioxidant role of these extracts were investigated using four chemiluminescence systems and two colorimetric systems.

采用水提取法、甲醇-水提取法和乙酸乙酯提取法3种方法从香桃木叶中提取非精油组分,然后用4种化学发光体系和2种比色体系检测其清除自由基和抗氧化作用。

Basic drugs, lidocaine, benghexolum, chlorpromazine, diazepam, clozapine, internal standard of SKF525A(all of 5μg), estazdam and alprazolam (all of 10μg), are extracted from superfatted necrogenic tissues with mixture reagents of ethyl acetate and diethyl ether under basic condition, and determined by gas chromatography with nitrogenphosphorus detector.

在高度腐败及脂肪较多的脏器中加入碱性药物利多卡因、安坦、氯丙嗪、安定、氯氮平及内标物SKF_525A各5.0μg,舒乐安定、佳静安定各10.0μg,在碱性条件下用乙酸乙酯与乙醚混合液提取,经GC/NPD分析。

We have investigated on the chemical constituents of Nepeta partite collected from Gansu Zhuanglang, and twenty eight compounds were isolated from the methanol extraction of this species by chromatography techniques. Twenty five compounds were identified by means of chemical and spectra methods IR, FABMS, EI-MS,〓, DEPT, and 2D NMR), among which four compounds were new as isopimar-15-en-3β, 8β, 20-triol; phenylethanal-3-O-(2'-glycerin)-5-O-β-D-glucopyranoside; 3-O-linolenoylglyceryl-6'-O-(α-D-galactopyranosyl)-β-D-galactopyranoside; ethyl rosemarinate.

我们对采自甘肃庄浪的康藏荆芥进行了化学成分的研究,利用层析手段从该植物的甲醇浸膏中分离出二十八个化合物,经化学方法和波谱技术(红外,质谱,一维和二维核磁共振谱)鉴定了二十五个化合物的结构,其中四个为新的化合物,它们分别是:异海松-15-烯-3β,8β,20-三醇;苯乙醇-3-O-(2'-甘油基)-5-O-β-D-吡喃葡萄糖甙;3-O-亚麻酰基甘油-6'-0--β-D-吡喃半乳糖甙;迷迭香酸乙酯。

In the presence of catalytic rhodium acetate, ethyl 2-diazo-3-oxo-per fluoroalkanoates, reacted readily with nitriles to give a series of 5-fluoroalkyl substituted 1, 3oxazoles with high regio-selectivity through a metal carbenoid intermediate. The reactions of carbenoids with noncyclic vinyl ethers or cyclic vinyl ethers afforded dihydrofuroates in good to excellent yields. Interestingly, only vinyl C-H insertion compound was obtained concerning of the reaction of carbenoids with 2, 5dimethylfuran due to the steric hindrance of methyl group

醋酸铑分解2-重氮-3-氧代-全氟羧酸乙酯形成的金属卡宾作为1,3-偶极体,可以与一系列芳基或烷基取代的腈反应,高度区域选择性地生成一系列4-乙氧羰基-5-氟烷基取代的噁唑化合物;也可以与富电子的链状和环状的烯基醚反应,以优良的产率得到一系列氟烷基取代的二氢呋喃类化合物;而与2,5-二甲基呋喃的反应,由于甲基的位阻作用,只得到金属卡宾对呋喃3-位烯基碳氢键插入产物。

We have tested those clinical blood lipid-lowering drugs: Compound Ethyl, Linoleate , Oenothera Biennis Oil and Chinese traditional medicine such as haw and Salvia miltiorrhiza Bunge.

这些结果对于建立具有我国特色的药物筛选模型,并深入发掘我国传统中药的有效成分和作用机理都具有重要的理论研究意义和实际应用价值。

Olid state cathodoluminescence of poly 2-methoxy-5-(2-ethyl-hexyloxy-1,4-phenylene vinylene in devices with Si3N4 as the electronic accelerating layer

i3N4做电子加速层的聚[2-甲氧基-5-(2-乙基-己氧基)-1,4-苯撑乙烯撑]固态阴极射线发光

S-Naproxen was obtained by asymmetric cross-coupling reaction of 2-bromo- 6-methoxynaphthalene with organozinc reagent of ethyl α- bromopropionate, catalyzed by chiral β-aminoalkylphosphine-nickel complexes.

用β -氨基烷基膦的NiCl2 配合物为手性催化剂,以 6 -甲氧基- 2 -溴萘和α-溴代丙酸酯的有机锌试剂为原料,通过不对称交叉偶联反应合成S --萘普生。

However, in actual practice, the relative quantity of ethyl orthosilicate to hydroxysiloxane used is always many times larger than the stoichiometric ratio.

将硅橡皮分别在空气及氮气中进行高温处理,并测定其溶胀度的变化的结果,证明这现象是由于硅橡皮在高温下发生降解及氧化所致。

The sol-gel solution was prepared by mixing ethyl orthosilicate, absolute alcohol and 0.1molL^(-1) HCl in a definite proportion, and adding an appropriate amount of silicotungstic acid as active material, strring for 30min and then standing for 24h at room temperature.

溶胶-凝胶溶液系将正硅酸乙酯、无水乙醇及0.1molL^(-1)盐酸按一定比例混合后加适量的硅钨酸作为活性物质,搅拌30min混匀后在室温放置24h配成。

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Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车,和一双合并为一移交&整个lotta爱&。

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