查询词典 ethyl

The analogs of piracetum with the core of demethylclausenamide(III-4 and III-5) were prepared by condensation of demethylclausenamide with ethyl bromoacetate and hydrolysis or aminolysis there after.

3在兰培工作的基础上，选用O-乙酰-R--扁桃酸为拆分剂，成功的拆分了表黄皮酰胺前体5--4-苯基-1-甲基吡咯烷酮(Ⅱ-1)，和Ⅱ-1分别引入3位羟基得到和表黄皮酰胺。

The result indicated that the reacting mixture containing dioxane 11.3mL/g HDCA which had been added ethyl chloroformate drop wise should be keep at 10℃ for 30min, then, rising to 15℃ for another 20min in the step of forming mixed anhydride ,and 1.5mol/L NaOH was used to dissolve taurine before aminolysis, and crude product was recrystalled by acetone in purifying process.

结果表明，形成混酐时，二氧六环用量为11.3ml/g HDCA，滴加氯甲酸乙酯后先在10℃反应30min，再在15℃下反应20min；用1.5mol/L的NaOH水溶液溶解牛磺酸后再进行氨解；粗产品用丙酮重结晶。

The taurohyodeoxycholic acid was synthesized by aminolysis of sodium taurine with carboxy-carbonate mixed anhydride prepared by reacting hyodeoxycholic acid with ethyl chloroformate at the present of triethylamine.

猪去氧胆酸与氯甲酸乙酯在三乙胺存在下反应生成羟酸－碳酸乙酯混合酐，而后将其与牛磺酸钠进行氨解反应，合成猪磺去氧胆酸。

Reaction (1) was examined with different kinds of acetal substrate(1) and vinyl ethyl ether, and the results indicated that the 1, 1,3-triethoxy compounds could be obtained in high yields of 88 and 97% respectively when the R groups of the acetal are phenyl and anisyl, while the yields amounted only to 55-75 % for R=a...

有证据表明这种催化反应也可能是通过正碳离子中间体进行的。本反应的产物1，1，3-三乙氧基化合物经乙酸/乙酸钠溶液水解可得反式α，β-不饱和醛。水解产率：芳香族产物大于90%，脂肪族产物大于75%。

In part one, the reactions of some active fluorine-containing compounds such as 2, 2-dihydropolyfluoroalkanoic acids and ethyl 2-hydropolyfluoroalkenoates were studied and various fluorine-containing heterocyclic compounds were synthesized. Using 2, 2-dihydropolyfluoroalkanoic acids as the starting material, 4-fluoroalkyl quinolin-2-ols, 2- [ -1-hydropolyfluoro-1-alkenyl] -4H-3, 1-benzoxazin-4-ones, 1-aryl -4, 9-dihydro-3-fluoro-alkyl-1H-pyrazo [3, 4-b] quinolin-4-ones, 5-fluoroalkyl-12H-quin olino [2, 1-b] quinazolin-12-ones, 4-fluoroalkyl-1, 3-dihydro-1, 5-benzodiazepin-2-ones and 4-fluoroalkyl-2H-pyrido [1, 2-a] pyrimidin-2-ones were synthesized through its condensation reaction with anilines, anthranilic acid, N'-aryl-o-aminobenzamides, o-nitro aniline, o-amino pyridine and their derivatives and the subsequent transformations. 5-Fluoroalkyl isoxazolidines, 3-fluoro-3-fluoroalkylisoxazolidino [4, 3-c] quinolin-4-ones, 3-fluoroalkylisoxazolino [4, 3-c] quinolin-4-ones and 2-aryl-3per fluoroacylindoles were synthesized by inter-and intramolecular 1, 3-dipolar cycloaddition of fluorine-containing olefins and nitrones.

第二部分，我们研究了α，α-二氟苄基卤类化合物的亚磺化脱卤反应、产物的转化及全氟烷基亚磺酸盐与芳环化合物的全氟烷基化反应，发现全氟苄基碘或溴及α，α一二氟苄基溴在保险粉等亚磺化脱卤试剂引发下可生成相应的亚磺酸盐；全氟苄基亚磺酸盐与氯气或溴反应可生成全氟苄基磺酰氯或磺酰溴；在烯烃存在下，全氟苄基碘则与烯烃发生加成反应，生成相应的1：1加成产物；在三价醋酸锰的作用下，部分芳香化合物如茴香醚，二甲氧基苯，吡啶，喹啉等可以和过量的全氟烷基亚磺酸盐发生双全氟烷基化反应，反应表现出一定的区域选择性，产率良好。

Methods: Apinoid wistar white rats ,quality standard was about 200 ? 30 gram (belong to SPF animal in experimental animal center ,FMMU)were randomly divided into experimental group and control group.Experimental group was gived hypodermic injection at a dose of 0.3ml/100g by 60 percent carbon tetrachloride olive solution every four days and drinked 50ml/L ethyl alcohol. we would divide course of cirrhotic rats models into three stages : early stage (the 25th day) is fatty degenerationnecrosis ;middle stage (the 45th day) is proliferation of fibrous tissue ; advanced stage (the 65th day) is formation of pseudolobuli .

实验方法：h级Wistar大鼠，质量在200士309之间（第四军医大学实验动物中心 SPF动物人随机分为实验组门 8只）和对照组只人实验组用 60％四氯化碳橄榄油溶液按 0.3ml／100g体重皮下注射，每四大一次，饮用5％乙醇，参照韩德五等将肝硬变大鼠模型分期，人为地将肝硬变大鼠病程分为H期：早期（第25大）脂变坏死期；中期（第45天）纤维增生期；晚期（第65天）假小叶形成期。

The research work and separation methods of arachidonic acid ethyl ester were also reviewed.

同时综述了花生四烯酸的研究概况以及目前提取分离的主要方法，在论述了各种提取分离方法优缺点的基础上，提出用超临界流体色谱法制备花生四烯酸乙酯。

The petroleum ether extacts,ethyl acetate extracts and methanol extracts from roots of Aristolochia debillis Sieb.et Zucc.

通过琼脂平板扩散试验和双倍稀释试验，对青木香Aristolochia debillis Sieb.et Zucc。

In the presence of ethanol- HCl solution, arylamine-HCl and w=37% aqueous formaldehyde solution or the condensation product of arylamine and formaldehyde are directly reacted with ethyl 3-oxo-2-phenylmethylenebutyrate to form l-aryl-2-phenyl-3-carbethoxy-4-piperidone.

2－苯亚甲基－3－丁酮酸乙酯与芳香胺和w＝37％甲醛水溶液或芳胺和甲醛的缩合物在氯化氢－无水乙醇存在下可直接发生的Mannich反应，得到1－对位取代芳基－2－苯基－3－羰乙氧基－哌啶－4－酮。

Using Fe2(SO4)3 and Ti(SO4)2 as raw materials, Nano- Fe2O3-TiO2 photocatalyst was prepared by an ethyl-assisted hydrothermal method at low temperature to degrade auramine in the three-phase photocatalytic reactor.

用该催化剂在自制的三相光催化反应器中进行催化降解碱性嫩黄的试验，探讨了催化剂投加量、溶液pH值、溶液浓度对降解率的影响。

Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车，和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特，那个是爱朗。