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The results indicated that the total quantity of volatile components in grape wine after MLF had increased and there were evident difference in the contents and proportion of isoamyl alcohol, 2-ethyl hydracrylic acid, ethyl succinate, and acetic acid in the two kinds of grape wine treated or not treated by MLF. Besides, lactic acid and ethyl lactate, which could not be accurately identified in grape wine not treated by MLF, could be easily separated and identified in grape wine treated by MLF like other main components.

结果表明，MLF葡萄酒较未经MLF的葡萄酒中挥发性成分的总量有所提高；异戊醇、2-羟基丙酸乙酯、琥珀酸乙酯和醋酸在两工艺的葡萄酒中的含量和比例存在明显差异；乳酸、乳酸乙酯和两种未能准确鉴定的物质只在MLF葡萄酒中作为主要成分被分离检测到。

The first synthetic route uses 1,2,4-trimethoxybenzene and chloroacetonitrile in forming 2,4,5-trimethoxy-a-chlor-acetophenone under the anhydrous condition, then the intermediate condensates with papaverine forming the core pyrro[2,l-a]isoquinoline, followed by formation and lactonization to form the lactone ring. The second synthetic route uses prepared aldehyde with prepared ethyl nitroacetate by Knoevenagel condensation to obtain 2-Nitro-3-(2,4,5-tris-methoxy-phenyl)-acrylic acid ethyl ester and 2-Nitro-3-(2,4,5-tris-benzyloxy -phenyl)-acrylic acid ethyl ester etal intermediates. The lamellarin skeleton could arise from condensation of the papaverine and these intermediates by Michael reaction, the ester group is provided for subsequent lactonization. The third synthetic route uses coumarin or indan-l,3-dione derivatives and papaverine to form lamellarin under basic conditions.

第一条路线首先从1，2，4-三甲氧基苯出发与卤乙腈作用合成卤代芳酮中间体，然后与罂粟碱反应合成开链片螺素，最后经乙酰化、去保护、成内酯环得到片螺素；第二条路线由制备的芳醛和制备的硝基乙酸乙酯经缩合得到2-硝基-3-芳基丙烯酸乙酯，然后由该中间体与罂粟碱反应，在完成关环的同时也引入酯基，最后去保护、成内酯环得到片螺素；第三条路线是由香豆素或茚二酮出发，经溴代后的中间体与罂粟碱反应，得到片螺素的基本框架。

When lipase N435 was 2.5gL^(-1), RS-ethyl mandelate was 0.25gL^(-1), water to RS-ethyl mandelate was 5:1, the reaction temperature was 40℃, the speed of agitation was 200rmin^(-1), the R-ethyl mandelate conversion could reach 41.6%, and enantiomeric excess e.

确定了最适的反应条件：脂肪酶N435浓度为2.5gL^(-1)，RS-扁桃酸乙酯浓度为0.25molL^(-1)，水：RS-扁桃酸乙酯的摩尔比为5：1，反应温度为40℃，摇床转速为200rmin^(-1)，反应时间为24h。

The volatile flavor compounds of Nanx wudl at the start stage of fermentation mainly were hydrocarbon compounds and aldehydes, ketones from lipids oxidation, After 180 days, ethyl hexanoate, ethyl acetate, phenethyl alcohol, acetic acid and ethyl octanoate were predominant.

发酵180d后，主要风味组分是己酸乙脂、苯乙醇、乙酸乙脂、乙酸和辛酸乙脂。

Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.

采用&一勺烩&方法，以4-羟基苯甲腈为起始原料，首先与硫氢化钠和无水氯化镁在N，N-二甲基甲酰胺中反应，所得中间体不经分离，直接加入2-氯乙酰乙酸乙酯进行环合反应，得到2-(4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯（2）；然后通过六亚甲基四胺/三氟乙酸进行Duff反应，得到2-(3-甲酰基-4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯（3）；再经盐酸羟胺/甲酸/甲酸钠体系脱水得到目标化合物。

The optimal operation condition of Friedel-Crafts acylation for product Ⅰ was determined by orthogonal experiment: 0.02mol N-ethyl- carbazol, n Benzoyl chloride/n N-ethyl- carbazol=1.2, n AlCl3/n N-ethyl- carbazol=1.2 , at 25 oC for 3.5h. The yield was 94.6%.

通过正交设计实验，探讨了产物Ⅰ的Friedel-Crafts 酰化的最佳反应条件：N-乙基咔唑为0.02mol时，反应物苯甲酰氯与N-乙基咔唑摩尔配比为1.2。，催化剂AlCl3与N-乙基咔唑摩尔配比为1.2， 25℃下反应3.5h，产率可达94.6%。

For the α-arylation of ethyl acetoacetate, the product was α-aryl ethyl acetoacetates, rather than ethyl α-arylacetates which are the major products in other catalytic systems.

较为惰性的氯代芳烃在Pd2/L1的催化下，也能够跟1，3-二羰基化合物发生α-芳基化反应。

In these components, 2-methyl-1-propanol, ethyl acetate, 3-methyl-1- propanol, 2,3-butanediol, phenylethyl alcohol, butanedioic acid diethyl ester, ethyl hydrogen succinate, 2-hydroxy-ethyl propanoic acid and 4-hydroxy-benzeneethanol were main aroma components, these volatile componds provided the typical sensory style of wine.

其中，2-甲基-1-丙醇、乙酸乙酯、3-甲基-1-丙醇、2，3-丁二醇、2-羟基丙酸乙酯、苯乙醇、丁二酸二乙酯、乙基-氢化琥珀酸和4-羟基苯甲醇等成分构成了葡萄酒的主体香气，这些主体香气与其他风味成分一起构成葡萄酒的典型风味特征。

An agent for a protective film which comprises a liquid mixture of a urethane type compound, methyl ethyl ketone and ethyl acetate and a curing rate enhancing agent comprising an isocyanate type compound and ethyl acetate; and a method for forming a protective film which comprises applying the agent for a protective film on the outer surface of a mold (9) or on the region of the outer surface of the mold (9) except a specific portion as an article to be coated.

本发明提供了一种保护膜制剂和形成保护膜的方法，其中所述保护膜制剂含有聚氨酯型化合物、甲基乙基酮和乙酸乙酯的液体混合物与含有异氰酸酯型化合物和乙酸乙酯的固化增速剂；所述形成保护膜的方法包括将保护膜制剂涂布于模具(9)的外表面或涂布于模具(9)的外表面除了作为待涂布制品的特定部分以外的区域。

Alcohols, ketones, esters, alcohols, ethers common media are methanol, ethanol, ethylene glycol, propanol, etc., ketones medium with acetone, methyl ethyl ketone, etc., there are a variety of methyl esters of medium, ethyl ester, ether medium with ether, ethyl ether, butyl ether, etc., they basically did not corrosive materials can be used for the specific use of the property should also be under the media and related requirements to make reasonable choices.

醇类、酮类、酯类、醚类常见的醇类介质有甲醇、乙醇、乙二醇、丙醇等，酮类介质有丙酮、丁酮等，酯类介质有各种甲酯、乙酯等，醚类介质有甲醚、乙醚、丁醚等，它们基本没有腐蚀性，常用材料均可适用，具体选用时还应根据介质的属性和相关要求做出合理选择。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新