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The antimicrobial test and researched was done on wide distillation of different solvents on Terpenoid, polarity separation of ethanol distillable substance, thin layer chromatography of different polarities and distillation of amylase. The results showed that the active substance distilled by 95% ethanol and V methanol: toluene=3:1 had stronger antimicrobial activity on Agaricus blazei Murrill. The antimicrobial activity of ethyl acetate was stronger than wide distilling substance with ethanol, but the water part has not antimicrobial effect. Two straps of ethyl acetate phase(Rf0.57、Rf0.63)(0.1g/ml)had stronger antimicrobial activity on Agaricus blazei Murrill, the antimicrobial zone on Pseudomonas was 19.3mm. The bacteriostatic activity of chromatography strap of water phase was rather weaker, the water solution (0.5g/g) of amylase had better effect on pathogenic fungus of Agaricus blazei Murrill, its antimicrobial zone on Aspergillus niger, Citrinin, Trichoderma viride were 10.8 mm, 7.9 mm, 5.3 mm.

通过对日本凹顶藻以不同溶剂的粗提、乙醇提取物的极性分离、不同极性的薄层层析和多糖的提取,进行抗菌试验的研究,发现95%乙醇和V甲醇:甲苯为3∶1的提取的活性物质具有较强的抗姬松茸的病原细菌活性,乙酸乙酯相对病原细菌的抑菌强于乙醇的粗提物,而水相基本无抑菌效果,乙酸乙酯相的两个带(Rf0.57、Rf0.63)浓度为0.1g/ml具有较强抗姬松茸病原细菌的活性,对假单孢杆菌抑菌圈达到19.3mm,水相层析带的抑菌活性较弱,多糖的粗提物配成0.25g/g的水溶液对姬松茸病原真菌有较好的抑菌效果对黑曲霉、桔青霉和绿色木霉的抑菌圈分别达到10.8 mm、7.9 mm、5.3 mm。

The chronic ethyl alcohol toxic dysphrenia to own health,the descendant,the family and the society causes a bigger harm,more anxious is along with the people living standard enhancement,the public relations drinks wine universally,our country chronic ethyl alcohol toxic dysphrenia disease incidence rate is increasing year by year.

慢性酒精中毒性精神障碍对自身健康、后代、家庭和社会均造成较大危害,更令人担忧的是随着人们生活水平的提高,社交性饮酒更加普遍,我国慢性酒精中毒性精神障碍的发病率在逐年增加。

Ethyl 4,4,4-trifluoroacetoacetate was synthesized from ethyl acetate and 4,4,4-trifluoroacetate(mole ratio 3:1) with sodium ethoxide.

乙酸乙酯与三氟乙酸乙酯(摩尔比为3∶1)在乙醇钠作用下进行克莱森酯缩合反应,得到三氟乙酰乙酸乙酯。

ConclusionThe main components of essential oils are 2,4-bis(1,1-dimethylethyl) phenol (4.4%), tetradecanoic acid (6.96%), n-hexadecanoic acid (7.69%), 9,12-cctadecadienoic acid (6.37%), hexadecanoic acid-2-hydroxy-1- ethyl ester (4.79%) and octadecanoic acid-2-hydroxy-1- ethyl ester (4.77%), respectively.

结论阿给炭挥发油的主要成分为2,4-二树丁基苯酚(4.4%)、十四酸(6.96%)、n-十六酸(7.69%)、-9,12-十八碳二烯酸(6.37%)、软脂酸-2-羟基-1-羟甲基乙酯(4.79%)、硬脂酸-2-羟基-1-羟甲基乙酯(4.77%)。

The results indicated that the total quantity of volatile components in grape wine after MLF had increased and there were evident difference in the contents and proportion of isoamyl alcohol, 2-ethyl hydracrylic acid, ethyl succinate, and acetic acid in the two kinds of grape wine treated or not treated by MLF.

结果表明,MLF葡萄酒较未经MLF的葡萄酒中挥发性成分的总量有所提高;异戊醇、2-羟基丙酸乙酯、琥珀酸乙酯和醋酸在两工艺的葡萄酒中的含量和比例存在明显差异;乳酸、乳酸乙酯和两种未能准确鉴定的物质只在MLF葡萄酒中作为主要成分被分离检测到。

The ammoxidation of methyl ethyl ketone to methyl ethyl ketoxime over nano-scale TS-1 was studied with a three-neck glass reactor.

在最佳反应条件下,甲乙酮的转化率和甲乙酮肟的选择性可分别达到99.4%和99.8%。

The ammoxidation of methyl ethyl ketone to methyl ethyl ketoxime over nano-scale TS-1 was studied with a three-neck glass reactor.

在最佳反应条件下,甲乙酮的转化率和甲乙酮肟的选择性可分别达到99。

Purpose: The aim was to determine the ethyl linolenate in Bombyx mori oil ethyl linolenate by Gas Chromatography.

目的:用气相色谱内标法测定蛹油α-亚麻酸乙酯制剂中α-亚麻酸乙酯的含量。

The experiment results indicate that the solvents (including n-hexane, ligarine, supercritical CO_2) and carriers all have great effects on the separation of ethyl linolenate from fatty acid ethyl ester mixture.

研究结果表明,超临界流体分离效果优于石油醚和正己烷等有机溶剂,氧化铝载体分离效果优于硅胶,超临界流体结合硝酸银吸附柱分离亚麻酸乙酯具有较好的效果,可得到纯度约95%的亚麻酸乙酯,其工业应用前景诱人。

Moreover, the preliminary test of the biological activity of the 8 target derivatives showed that 7-(2-adenine)ethoxyl-2-ethyl-4"- methoxy isoflavone and 7-(2-hydroxyl-3-piperidino)propoxy-2-ethyl-4"- methoxyl isoflavone have fine biological activities on suppression of the growth of MCF-7 cell in breast cancer and the hela cell in cervical cancer of human being.

另外还对8个目标衍生物进行了初步的药理活性试验,发现7-(2-腺嘌呤)乙氧基-2-乙基-4′-甲氧基异黄酮和7-(2-羟基-3-哌啶)丙氧基-2-乙基-4′-甲氧基异黄酮均有较好的抑制人乳腺癌MCF-7细胞和人宫颈癌hela细胞生长的药理活性。

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