查询词典 esterification

The effects of reaction temperature, reaction time, catalyst dosage, addition of esterification agent and the ratio of monoglyceride to glycerol were examined.

分别考察了反应温度、反应时间、催化剂添加量、酯化剂添加量和单甘酯与甘油的比例对酸值的影响。

Deacidification of rice bran oil was studied by using monoglyceride and glycerol blends as an esterification agent and ZnCl2 as a catalyst.

以单甘酯和甘油混合物作酯化剂，ZnCl2为催化剂对米糠油进行化学酯化脱酸研究。

In this paper six carbazole oxime ester derivatives were synthesized through Friedel-Crafts acylation, oximation and esterification from N-alkyl-carbazole.

以N-烃基咔唑为原料，经Friedel-Crafts 酰化、成肟和酯化反应，合成了6种咔唑肟酯衍生物。

Methods: P-toluenesulfonic acid diethoxyphosphorylmethyl ester (4) was prepared from diethyl phosphate and paraformaldehyde by condensation and esterification.

以亚磷酸二乙酯和多聚甲醛经缩合、酯化得到对甲苯磺酸羟甲基磷酸二乙基酯(4)。

In this paper,investigation has been made on the process for the synthesis of salicylaldehyde by esterification-oxidation with phenol,paraformaldehyde,boric acid as initial materials.

探索了以苯酚、硼酸和多聚甲醛为原料的酯化氧化法合成水杨醛的工艺路线，根据反应特点，改进了酯化反应方式，采用了多聚甲醛气态解聚法作为羟甲基化反应的进料方式，探讨了羟甲基化反应温度、多聚甲醛原料含水量、催化氧化反应催化剂用量对反应收率的影响并得到最佳反应条件，水杨醛收率为60.5%，纯度达98%以上。

This invention carrying through alcoholysis of common gloss polyester chip, getting low-molecular polymer of polytetramethylene terephthalate, using this low-molecular polymer as pregnant liquor, doing esterification reaction and polycondensation reaction of PTA and hybrid diatomic alcohol in normal pressure, getting the modified copolyester product which has inherent viscosity of 0. 65-0. 85dl/g, fine pellucidity and is suitable in the application of engineering plastics.

本发明是通过对普通大有光聚酯切片进行醇解，得到对苯二甲酸乙二酯低聚物，以此低聚物为母液，在常压下使PTA与混合二元醇进行酯化反应和缩聚反应，制备得到了特性粘数在0.65-0.85dl/g且具有良好透明性的适用于工程塑料领域应用的改性共聚酯产品。

Synthesis of dimethyl fumarateby esterification of fumaric acid with methanol catalyzed by solid su- peracid SO_4~(2-)/TiO_2was proposed in this paper.

以SO_4~(2-)/TiO_2固体超强酸为催化剂催化富马酸与甲醇合成富马酸二甲酯，探讨了催化剂制备条件、原料配比、反应时间、催化剂用量等因素对富马酸二甲酯收率的影响。

It includes the following steps: polymerizing 2, 4-dihydroxyl metaphenylene diamine hydrochloride, diamine monomer and dipic acid anhydride to gain the polyimide that contains hydroxy on the molecule chain, making the hydroxyl take esterification reacting with acyl chloride and acrylic acid to gain polyimide photosensitive material that has negative photonasty.

该聚酰亚胺光敏材料以2，4-二羟基间苯二胺盐酸盐，二胺单体和二酸酐为原料进行聚合，得到分子链上含羟基的聚酰亚胺，然后使羟基与丙烯酸及其衍生物的酰氯发生酯化反应，得到具有负性感光性能的聚酰亚胺光敏材料。

The ammonia was evaporated under decreasing pressure, and the precipitate was filtered off and the liquid was poured into hot saturated picric acid solution to get picrate with a yield of 85.0%. The optimum process starting from imidazole-4,5-dicarboxylic acid was: imidazole-4,5-dicarboxylic acid in acetic anhydride was refluxed to get imidazole-4-carboxylic acid, and the product was esterification in ethanol with a catalyzer of concentrated sulfuric acid to get ethyl imidazole-4-carboxylate, at last the compound above was reduced by LiAlH4 in ether at room temperature to get the target compound, the total yield of this route was 49.6%.

以4，5-二羧酸咪唑为原料的较佳工艺：1 脱羧反应：4，5-二羧酸咪唑40g，醋酐1200ml，回流10h，过滤并将滤液浓缩至干，所得固体加至50%的乙醇溶液回流，过滤并将滤液自然冷却过夜，过滤得固体；2 酯化反应：4(5)-羧酸咪唑50g，乙醇1000ml和浓硫酸60ml，加热回流2h，5%浓度NaOH溶液调节至pH＝8，减压浓缩至干，加入少量水回流，自然冷却过夜并过滤得固体；3 还原反应：LiAlH410g，乙醚300ml和4(5)-羧酸咪唑乙酯28g，常温反应1.5h，小心滴加25ml水后过滤，滤渣溶于300ml甲醇中并过滤，收集所得乙醚和甲醇滤液浓缩至干，将所得固体溶于300ml乙醇中加热回流，后将溶液浓缩至约30ml，冷却并过滤得固体，该路线总收率为49.6%。

The influences of factors on α-pinene esterification results were investigated and the obtained optimum conditions were n:n([HSO3-pmim]H2PO4):n:n=5:0.9:5:14, reaction temperature 40℃ and reaction time 10 h.

考察影响反应的主要因素，确定了较佳的反应条件：n：n([HSO3-pmim] H2PO4)：n：n=5：0.9：5：14，反应温度40℃，反应时间10 h。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。