查询词典 elemental analysis

In order to find active pesticide leading compounds, thinking about that triazolothiadiazoles had various biological activities, this paper designed and synthesized 11 novel title compounds from 3-substituted-4-amino-5-mercapto-1,2,4-triazoles with heterocyclic carboxylic acid via cyclization in the presence of phosphoryl chloride by the princple of combination of active strucural moieties. The structures of the title compounds were characterized by melting point, IR, 1HNMR and elemental analysis.

为了寻找高活性农药先导化合物，考虑到三唑并噻二唑衍生物具有广泛的生物活性，本文利用活性亚结构拼接原理，将活性基团分别引入1，2，4-均三唑并[3，4-b]-1，3，4-噻二唑杂环的3位和6位，合成了未见文献报道的3，6-二取代均三唑并[3，4-b]-1，3，4-噻二唑类化合物11个，并用IR、1HNMR及元素分析测试技术对其进行了结构表征。

The composition, structure and properties of the new pillared material were characterized by elemental analysis, XRD, IR spectra and TG-DTA curves.

用元素分析、IR、XRD和TG-DTA测试技术对产物的组成与结构进行了表征。

Finally, 2-Bromo-5-formyl -3-methylpyrrole was prepared by refluence under the alkaline condition. The structures of the synthetic products were characterized by elemental analysis, infrared, gas mass and 1H nuclear magnetic resonance.

对上述各步的合成过程中，通过元素分析、红外光谱、气相质谱和核磁共振光谱等检测手段对所合成的化合物进行了结构表征。

Atomic emission spectrometry is probably one of the oldest methods used for elemental analysis.

原子发射光谱法可能是用于元素分析的最古老的方法之一。

The hemisuccination process and kinetics ofβ-sitosterol and stigmasterol with succinic anhydride The reaction product ofβ-sitosterol and stigmasterol with succinic anhydride were characterized by elemental analysis,~1H NMR and ~(13)C NMR.

应用高效液相色谱对混合植物甾醇琥珀酸酯化产物中各组分的含量进行了分析测定。实验结果表明，各种植物甾醇琥珀酸单酯的分离效果较好，响应时间在10min左右，面积归一法能够快速准确地用于该过程的分析测试。

A series of cholesterol-bearing O-carboxylmethyl chitosan conjugates with different degrees of substitution of the cholesterol moieties and cholesterol-bearing chitosan were synthesized by the succinyl linkages and characterized by Fourier transform infrared, Proton Nuclear Magnetic Resonance (~1H NMR) and elemental analysis. These hydrophobized chitosan derivatives were amphiphilic in nature and their self-aggregation behavior in aqueous media was evaluated by the fluorescence probe technique.

课题的主要研究内容如下：采用化学的方法合成了不同分子结构、不同取代度的系列胆甾醇基壳聚糖衍生物—胆甾醇基壳聚糖和胆甾醇基-羧甲基壳聚糖，并应用先进的分析手段电位滴定、红外光谱法(IR、核磁共振波谱法等对原料、中间产物以及产物进行了结构表征，衍生物分子中的胆甾醇基取代度(3.2％～12.5％)采用元素分析的方法进行检测。

Eleven molecular tweezer artificial receptors based on deoxycholic acid have been synthesized by using solid K2CO3 as supporter through the reaction of methyl deoxycholate with aroyl chloride in solvent-free conditions under microwave irradiation, five of which are new compounds. The structures of all the molecular tweezers were characterized by 1H NMR, IR, MS spectra and elemental analysis.

在微波辐射无溶剂条件下，以固体K2CO3为载体，脱氧胆酸甲酯与芳酰氯反应合成了11个脱氧胆酸分子钳人工受体，其中5个为新化合物，所有化合物的结构均经1H NMR， IR， MS及元素分析所确证。

The author performed a multi-elemental analysis on the cycle of competition state formation, asymmetry between competition state and competition performance, adjustability of competition state at competition field, and competition state evaluation indexes, and pointed out that competition state is a process of dynamic development, having characteristics of uncertainness.

对竞技状态形成的周期性、与运动成绩的非对称性、临场可调性以及评价指标的多元性进行分析，指出竞技状态是一个动态发展的过程，具有不确定性的特征。

The obtained unsymmetry substituted phthalocyanines were characterized by Mass spectrum, ultraviolet-visible spectrum, Infrared Spectroscopy and elemental analysis.

不对称酞菁经过元素分析、红外、紫外可见光谱和质谱的表征证明其结构，从而证实产物就是目标化合物。

A series of p-toluene sulfonylamido acetacylhydrazone derivatives were synthesized from p-toluenesulfonyl chloride which reacted with glycine to get the intermediate p-toluene sulfonylamido glycine, then through the esterification, hydrazinolysis to afford another intermediate p-toluene sulfonylamido acethydrazide, which condensed with different aldehydes to obtain the target compounds that were characterized by IR, 1H NMR, 13C NMR spectra and elemental analysis.

魏太保 ；冷艳丽；王永成；张建辉；张有明*摘要：以对甲苯磺酰氯为原料，通过与氨基乙酸反应得到中间体对甲苯磺酰氨基乙酸，再经酯化、肼解得到对甲苯磺酰氨基乙酰肼，然后与相应的醛缩合得一系列对甲苯磺酰胺基乙酰腙类化合物。其结构经元素分析， IR， 1H NMR和13C NMR确证。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了