查询词典 elemental analysis

It is one of the most important method in chemical research. The course matches Instrument Analysis course. We set up 16 experiments: atomic absorption spectrum, atomic emission spectrum, atomic fluorescent, ultraviolet-visible absorption spectrum, infra-red absorption spectrum, and molecular fluorescent which are for photometric analysis; vottammetric analysis , coulometry analysis ,volt-ampere analysis and polarogarphy for electroanalytical chemistry; Gas chromatography and liquid chromatography for chromatographic analysis.

本实验内容与仪器分析理论课内容相配套，针对光化学分析开设了原子吸收光谱、原子发射光谱、原子荧光、紫外-可见吸收光谱、红外吸收光谱、分子荧光光谱等实验；针对电化学分析开设了电位分析法、库仑分析法、伏安和极谱分析法等实验；针对色谱分析开设了气相色谱和液相色谱分析等实验，共开设了16个实验。

For frequency information fluid identification technology:the basic theory of fluid identification based on frequency information has been introduced,for inner and external factor affecting frequency,some steps have been proposed to attain reserved amplitude and frequency analysis data with high resolution,high S/N ratio;through the comparison of time-frequency analysis method, the high accuracy time-frequency analysis method has been selected to extract time-frequency attributes;the analysis method flow of common single frequency fluid identification has been proposed,according to the data of full frequency band,several anomaly zone modes of common single frequency attribute have segregated; incorporating converted wave and compression wave,fluid identification method based on PS wave combined time-frequency analysis has been proposed;the AVO property of various fluid type in frequency domain has been studied;the generalized fourier analysis method,Proni absorption filter has been introduced,and researched for anti-noise and for the seismic processing interpretation flow.The above technology have been applied to fluid identification of organic reef in WBT area in the east of Sichuan and fluid identification of clastic rock in GUANGAN area in the middle of Sichuan,the results show that the above methods are effective.

基于频率信息的流体识别技术方面：介绍了利用频率信息流体识别的基本理论，针对影响频率的内、外在因素，提出一些针对措施，以获得高分辨率、高信噪比的保幅、保频分析数据；通过时频分析方法的比较，选取高精度的时频分析方法提取时频属性；提出共单频属性进行流体识别的分析方法流程，结合全频带数据，分出几种共单频属性异常带模式；联合转换波资料和纵波资料，提出基于纵横波联合时频分析进行流体识别方法；研究了频率域内不同流体类型AVO现象；引进一种广义傅立叶分析方法：Proni吸收滤波，研究其抗噪性以及进行地震处理解释的流程；将这些技术应用川东北五百梯区块进行生物礁储层流体的识别和川中广安陆相碎屑岩的流体识别，取得较好的效果。

Their structures were confirmed by elemental analysis, 1H NMR, and IR spectral data. The preliminary bioassay results showed that α-phenyl-sul-fonylcyclododecanone oxime 2,4-dichlorophenoxy acetate (8p) had inhibition ratio 100% and 80.07% against Digitaria sanguinalis Scop., and 100% and 88.70% against Abutilon theophrasti Medic. at concentrations of 100 and 1 mg/L.

初步生物活性测定结果显示，部分化合物具有一定的除草活性，如α-苯磺酰基环十二酮肟-2，4-二氯苯氧乙酸酯(8p)在浓度为100和1 mg/L时对马唐的抑制率分别为100%和80.07%；对苘麻的抑制率分别为100%和88.70%。

The structure of octadecyl acrylate were identified by elemental analysis, IR and (superscript 1)H NMR.

产物结构经元素分析，IR和(上标1)H NMR表徵。

Quantitative studies of UV absorption show that the content of acyl group is consistent very well with elemental analysis result.

通过UV吸收对产物中的酰基进行了定量，结果与元素分析结果基本一致。

The alkaline-earth metal complexes with mucic acid was successfully prepared via gel formation and characterized by elemental analysis,FT-IR measurements.

采用凝胶法合成了碱土金属—粘液酸配合物的晶体。

Novel chitosan derivative with long alky groups as the hydrophobic moieties and carboxymethyl groups as the hydrophilic moieties was synthesized. The chemical structure of N-octyl-O, N-carboxymethyl chitosan was characterized via FTIR, 1H NMR and elemental analysis. The physical properties were analyzed with wide angle X-ray diffraction and differential scanning calorimetry.

以天然可生物降解的壳聚糖为原料，通过在壳聚糖6位羟基上引入羧甲基，在2位氨基上引入疏水烷基链，制得N-辛基－O，N-羧甲基壳聚糖两亲性衍生物，分别用FTIR、1H NMR和元素分析等技术对其结构进行表征，用广角X射线衍射和差示扫描量热法对具物理性质进行分析，并考察其在各种溶剂中的溶解性能及其对难溶性药物的增溶能力。

A novel synthetic approach of 3,3'-azobis(6-amino-1,2,4,5-tetrazine) was firstly devised. Taking 3,6-bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine as a primary material, DAAT was synthesized by high pressure ammonolysis and potassium permanganate oxidation. Compared with the four-step reaction in the literature, this new approach was reduced to two steps with a yield of 58.1%. The intermediate and DAAT were characterized by elemental analysis, IR and NMR spectra.

自行设计了3，3'-偶氮双(6-氨基-1，2，4，5-四嗪)新合成路线、采用3，5-双(3，5-二甲基吡唑-1-基)-1，2，4，5-四嗪为原料，由文献报道的4步反应缩减为2步，经高压氨解、高锰酸钾氧化合成了DAAT，总收率大幅提高，达到58.1%，并采用元素分析、红外光谱、核磁共振光谱等进行了结构表征。

All these compounds were characterized by azeotrope and elemental analysis, as well as by spectral measurements.

对所制成的衍生物均采用了共沸混合物分析、元素分析和光谱测定等进行了表征。

Three new fluo-rine-containing nitro benzimidazole derivatives were synthesized in the presence of 4-dimethylaminepyridine andtheir structure and configuration were confirmed by elemental analysis, IR, and 1HNMR.

在碱性条件下由2-(4′-羟苯基)-5-取代苯并咪唑与氯乙酸作用得到5个新化合物取代苯并咪唑基苯氧乙酸。

In the days of sailing vessels the crew were afraid they would be becalmed on the ocean.

在使用帆船的时代，船员们担心他们会因为无风而无法在海洋上航行。

As long as foreign donors pay the PA's salary bill, few expect a new intifada.

只要外国继续为巴权力机构的薪水买单，希望发动新暴动的人便寥寥无几。