查询词典 elemental analysis

One mixed-ligand complex ofnH2Otpa=terephthalate, tripy=4'-(4methyoxyphenyl-2,2':6',2-terpyridine was synthesized and characterized by IR, elemental analysis and thermo-gravimetric analysis. The crystal structure of the product was established by single-crystal X-ray diffraction.

采用水热法合成了新的维链状锌的配位聚合物nH2O（tpa=对苯二甲酸，tripy=4'-（4-甲氧基苯基）－2，2'：6'，2-三联吡啶），通过红外光谱和元素分析对该配位聚合物进行了结构表征，用X射线单晶衍射测定了晶体结构。

Benzoyl chloride was treated with potassium selenocyanate in dichioromethane by using polyethylene glycal-400 as the solid-liquid phase transfer catalyst to yield the corresponding benzoyl isoselenocyanate. This intermediate did not need to be isolated and directly reacted with arylamines, affording the N-benzoyl-N'-arylselenoureas 2a~2p. These compounds were characterized by IR, 1H NMR spectra and elemental analysis and the single crystal structure of 2k has been confirmed by X-ray crystallographic analysis.

以PEG-400为固液相转移催化剂，通过苯甲酰氯与硒氰酸钾反应合成了中间体苯甲酰基异硒氰酸酯，该中间体不需分离，直接与芳胺反应，得到N-苯甲酰基－N'-芳基硒脲(2a~2p)，这些化合物用1H NMR，IR及元素分析进行了表徵，并用X射线单晶衍射确定了化合物2k的单晶结构。

They were characterized by elemental analysis, molar conductance, differential thermal analysis and spectralIR, UV,(superscript 1HNMR studies.

用元素分析、摩尔电导、差热热重分析、红外光谱、紫外光谱和核磁共振氢谱叶其进行了表徵。

Their complements, structures and properties are analyzed by means of elemental analysis, molar conductance, infrared spectra, ultraviolet visible absorption spectra, thermal analysis, and electron microscope ect.

通过电导率、红外光谱、紫外可见光谱、热分析、电镜等分析手段对上述配合物的组成、结构和性质进行了表征。

A new Schiff baseH_(2Lhas been synthesized from sulfamethoxazole and complexes of this ligand have been prepared with it and characterized by elemental analysis,infrared spectrum,nuclear magnetic resonance,thermal analysis,molar electric conductance and solubility.

以磺胺甲基异口恶唑与对羟基苯甲醛合成一种新西佛碱(H2L)，并用此配体制备8个稀土配合物，通过元素分析、红外光谱、核磁共振、热分析、摩尔电导和溶解性试验对配合物进行了表征。

Five new solid complexes were synthesized by the coordination of tranisition metals with a Schiff base(C17H21NO,HL) derived from adamantaneamine and salicylaldehyde ,and characterized by elemental analysis,molar conductance,infrared spectra,1H NMR spectra,thermal analysis.

合成了金刚烷胺水杨醛Schiff碱配体(C17H21NO，以HL表示)与5种过渡金属的新的配合物[MCl22]M=Mn(Ⅱ、Co、Ni、Cu、Cd，用元素分析、摩尔电导、红外光谱、1H NMR谱和热重分析对产物进行了表征；讨论了配体与中心金属离子的键合情况，并推测了配合物的结构。

Two novel Schiff-base ligands containing ferrocenyl and their transition metal complexes were synthesized and characterized by 1H NMR, IR, elemental analysis, thermal analysis and molar conductivity measurements.

合成了两个新型含有二茂铁基的Schiff碱配体及其8种过渡金属配合物，并通过1H NMR，IR，元素分析，热分析和摩尔电导对其结构进行表征，提出了配合物的可能结构。

Part II. Synthesis, characterization and fluorescent properties of rare earthcomplexes of rutin Rare earth complexes of rutin have been synthesized by the reaction of rare earth chloride with rutin in alcohol solution (pH=7～8). The composition and thermal stability of the complexes were characterized by elemental analysis, molar conductivity, thermal analysis, IR, UV.

第二部分：稀土芦丁配合物的合成与表征及其荧光性质以稀土金属氯化物和芦丁为原料，在乙醇溶液中(pH=7～8)合成了6种稀土配合物，通过元素分析、IR、UV、热重-差热分析、摩尔电导率的测定对配合物进行了表征，确定了配合物的组成，分析了配合物的热稳定性和热分解行为。

Two coordination polymers [Pb6(H2O)24]·3H2O(1)(H3cit=citric acid)and Pb(H2O)2(2)(tar=tartaric acid)were synthesized under hydrothermal conditions and characterized via IR,TG-DTA,C,H,N elemental analysis,XRD and single crystal X-ray diffraction analysis.

在水热条件下，合成了2个含柔性配体柠檬酸和酒石酸的二价铅配位聚合物[Pb6(H2O)24]。3H2O(1)(H3cit=citricacid)及Pb(H2O)2(2)(tar=tartaricacid)。用红外光谱、差热-热重、元素分析、粉末X射线衍射及单晶X射线衍射等手段对化合物进行了表征。化合物1属三斜晶系，P1空间群，a=0.97053(19)nm，b=0.9764(2)nm，c=1.0955(2)nm，α=109.016(3)°，β=98.380(3)°，γ=92.136(3)°，V=0.9671(3)nm3，Z=2，R1=0.0420，wR2=0.1049，GOF=1.064。

Then quality upgrading scheme was explored in order to solve the high content of sulphur and nitrogen in pyrolytic oil, low flash point as well. Yields of pyrolysis of scrap tires in a pilot-scale rotary kiln under 550℃were firstly summarized. Then elemental composition and physiochemical properties were analyzed on both pyrolytic crude oil and its fractions. Based on these researches, the feasibility that pyrolytic oil is used as fuel was discussed. From FT-IR spectra the functional group compounds were generally acquainted, and by column chromatography analysis chemical compositions were clearly known. Then through GC analysis the absolute content of BTX in pyrolytic crude oil was defined.

本文首先考察了中试回转窑550℃下的废轮胎热解产率及热解原油的元素组成和理化特性，对其作为燃料使用的可行性进行了分析；通过实沸点蒸馏研究了轻质、中质馏分热解油的基本特性：红外分析得出了有代表性馏分热解油的大致官能团组成形式，对热解油的强芳香性和部分不饱和性有了整体了解；化学族组成分析进一步了解了热解油内在化学族组成和含量，对热解油的内在性质有了更为深入理解；气相色谱分析对热解油中富含的苯、甲苯和二甲苯进行绝对定量，为热解油提取BTX化工原料的经济性提供了参考。

Through comparing with the results by simulation to study the effects of theprojectile"s final velocity, the angle of rotation and the ballistic trajectory"s migration withdifferent projectile"s rotating speeds, different target"s moving speeds and differentpenetration angles.

通过比较数值模拟的结果来研究不同弹头转速、目标速度、侵彻角对侵彻过程中弹头最终速度、翻转角度和弹道偏移的影响。

I love stationery and all the accoutrement of writing.

我爱文具以及所有的书写的工具装备。