查询词典 electron diffraction

Transmission electron microscopy, scanning electron microscopy, X-ray diffraction pattern and UV-Vis spectrum were utilized to characterize the products.

利用透射电子显微镜，扫描电子显微镜，X射线衍射仪和紫外－可见分光光度计对产物进行表征。

The morphology and microstructure characteristics of the apertured silver doped TiO2 microtubes were characterized by means of the X-ray powder diffraction, thermal analysis, transmission electron microscopy, scanning electron microscopy, X-ray photoelectron spectroscopy and N2 absorption.

氮吸附的结果显示该样品具有很高的比表面积，银的修饰没有显著影响二氧化钛微管的孔结构； XRD的表征结果显示，银修饰的二氧化钛多孔微管具有良好的锐钛矿晶型； XPS的分析结果表明银以游离的金属态存在； TEM的观测结果显示，银团簇沉积于二氧化钛纳米晶粒的表面。

A new organic compound, trans-2--5-dimesitylborylthiophene (abbreviated as DMASBT, 5) with dimesitylboryl, dimethylamino and styryl-thiophene as electron acceptor, electron donor and conjugate bridge respectively, was synthesized. Its crystal structure determined by X-ray diffraction method indicates that the B-C bond between B atom and it bridge is obviously shorter than those of between B atom and mesityl groups. This remarkably strengthened B-C bonding can be regarded as an evidence of additional p-7t conjugation between the B atom and n bridge.

合成了以含硼基团为电子受体，以二甲胺基为电子给体，以苯乙烯基噻吩为共轭桥的新化合物2-[（4'-N，N-二甲胺基）苯乙烯基]-5-二米基硼-噻吩 trans-2-[(4'-N， N-dimethylamino) styryl]-5-dimesitylboryl-thiophene（简写为DMASBT，5）。X射线衍射方法测定其单晶结构表明，硼原子与π共轭桥之间的硼碳键相对于其它的硼碳键明显缩短，硼与π共轭桥之间存在除了σ键之外的p-π共轭作用。

The products were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and thermal gravimetric analysis.

采用X射线衍射仪、傅里叶变换红外光谱仪、扫描电子显微镜、透射电子显微镜和热失重分析仪等对产物的组成、形貌以及热失重情况进行了表征。

Single-crystalline cerium orthovanadate (CeVO4) nanorods are synthesized successfully by Na2EDTA-assisted hydrothermal method. The products are characterized using X-ray diffraction, transmission electron microscopy, high-resolution transmission electron microscopy and superconducting quantum interference device.

以Na2EDTA为模板导向剂，利用水热法成功合成了单晶CeVO4纳米棒，使用X射线衍射仪、透射电镜、高分辨透射电镜和超导量子磁强计等对产物的结构和磁学性能进行了表征。

Carbon nanocoils were in situ synthesized by the flame combustion of ethanol using stannic chloride as catalyst precursor. The morphology and structure of CNCs were characterized by means of scanning electron microscope, transmission electron microscope, X-ray diffraction and Raman spectrum.

采用乙醇火焰燃烧，借助于基板材料上涂敷锡盐作为催化剂前驱体，制备了螺旋结构碳纳米纤维；借助于扫描电子显微镜、透射电子显微镜、XRD和拉曼光谱等分析了螺旋碳纤维的形貌和结构。

In current study, the laser shock processing technique of high energy and short pulse duration is adopted. The substructural transformation characteristics and mechanisms of 2Cr17Mn15Ni2N austenitic stainless steel, subjected to ultra-high strain-rate and impact stress in excess of dynamic yield strength of the target, are investigated by scanning electron microscope, X-ray diffraction and transmission electron microscope technology.

采用高能短脉宽激光冲击加载技术，利用扫描电子显微镜，X射线衍射和透射电子显微镜等手段，研究了在激光诱导的超高应变率和高于材料动态屈服强度冲击加载条件下，2Cr17Mn15Ni2N奥氏体不锈钢表面亚结构的转变特征和机制。

Mesoporous zincum sulfide is synthesized by gentle wet chemosynthesis method, with DDA as templates and Zinc acetate and TAA as precursors. The effect to the synthesis of the ratio of reactive components, the volume of pH, reactive time and reactive temperature has been dicussed systematically, and structures of the as-synthesized samples have been characterized by X-ray diffraction, N2 adsorption-desorption, scanning electron microscopy, Fourier transform-infrared spectra, UV-vis diffuse reflectance spectroscopy, transmission electron microscopy.

以十二胺为模板，醋酸锌及硫代乙酰胺为前驱体，温和湿化学法合成了硫化锌无序介孔结构，系统研究了反应物配比、pH值、反应温度、反应时间对材料合成的影响，运用X射线衍射、N2吸附-脱附、扫描电镜、红外光谱、紫外-可见吸收光谱、透射电镜等分析手段对介孔材料的结构进行了详细的表征。

GaN nanorods are successfully synthesized on Si(111) substrates with magnetron sputtering through ammoniating Ga2O3/Co films at 950℃.X-ray diffraction, scanning electron microscopy, high-resolution transmission electron microscopy, and Fourier-transform infrared spectroscopy are used to characterize the samples.

采用磁控溅射技术先在Si衬底上制备Ga2O3/Co薄膜，然后在950℃下流动的氨气中进行氨化反应制备GaN纳米棒。应用X射线衍射、扫描电镜、傅里叶红外吸收光谱、选区电子衍射和高分辨透射电子显微镜对样品进行表征。

The phases, chemical compositions and interlaces of the composite powders were characterized and analysed by X-ray diffraction , X-ray photoelectron spectroscope, transmission electron microscope and high resolution electron microscope.

利用X射线衍射、X射线光电子能谱和透射电镜对复合粉体的物相组成、化学组成及界面结构进行了表征分析。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。