查询词典 electron diffraction

The analysis of X-ray diffraction and scanning electron microscope energy dispersion spectra show that the primary hydrolysis products of antimony pentachloride and its hydrochloric acid solution are amorphous antimony oxide rather than SbO2Cl.

X射线衍射和扫描电镜能谱分析表明：五氯化锑及其盐酸溶液的初始水解产物不是SbO2Cl，而是一种非晶态锑氧化合物；随着水解母液酸度的降低，五氯化锑溶液水解产物陈化五天后的晶型由非晶态向晶态变化；五氯化锑溶液水解产物经无水乙醇洗涤后水解产物仍为非晶态，而经蒸馏水洗涤虽主要为非晶态，但有少部分结晶的Sb2O5·4H2O晶体存在。

The scale inhibition mechanism of PESA was proposed on the basis of characterization of transformation of calcium carbonate crystal by means of X-ray Diffraction and scanning electron microscopy. The effect of temperature on corrosion inhibition efficiency of PESA was investigated and the Bockris substitution model is proposed to study the thermodynamics of inhibiting process of PESA. The calculation results show the adsorption of PESA on carbon steel is a spontaneous exothermic process with the increase of entropy.

通过X射线衍射和扫描电镜分析手段研究了聚环氧琥珀酸加入前后碳酸钙垢晶型的变化，在此基础上探讨了聚环氧琥珀酸的阻垢机理；考察了温度对聚环氧琥珀酸缓蚀性能的影响，根据Bockris置换模型，计算出中性水质中聚环氧琥珀酸在碳钢表面吸附的热力学函数，计算结果表明：聚环氧琥珀酸在碳钢表面的吸附是一个放热、熵增、自动发生的过程。

The study performed by the authors is of significance in finding favorable reservoir zones in Dongying depression. Many thin sections were analyzed by such means as standard petrographic microscope, X-ray diffraction and scanning electron microscope analysis so as to study the selected samples.

在对大量薄片和岩心进行分析的基础上，运用扫描电镜和X衍射粘土分析等手段，对东营凹陷砂岩储层的成岩作用和孔隙演化进行了研究。

X-ray diffraction,transmission electron microscopy, BET surface area measurement and thermal analysishave been used to determine the characteristics of the nanopowdered silver prepared by chemical reduction with the polymolecular protectant.

用X -射线衍射、透射电镜、比表面测定和热分析技术，对从高分子保护化学还原法制得的纳米Ag粉，做了相关的测定表征；从表观比热的测定结果探讨这一亚稳微晶体系在加热过程和热处理后所发生的各种变化。

Early hydration characteristics and paste structure of complex binding material containing high-volume steel slag were studied by the determination of hydration heat evolution, type of hydration products as well as micromorphology of hardened paste using calorimetry, X-ray diffraction, pressure porosimeter, and envirnoment scanning electron microscope.

通过对胶凝材料早期水化放热性能和水化产物种类的测定，以及对硬化浆体显微形貌和孔结构的观察，研究了大掺量钢渣复合胶凝材料的早期水化性能和硬化浆体结构。

A functionalized superparamagnetic iron oxide nanoparticles were synthesized by reduction-precipitation method, and were modified by silicane coupling agent. The nanoparticles were evaluated by diffraction, scanning electron microscope and X-ray energy spectrometer.

用部分还原－共沉淀法制备了四氧化三铁Fe3O4纳米材料，用硅烷偶联剂进行了表面修饰，用扫描电镜，X-射线粉晶衍射，磁强计，X射线能谱仪等分析仪器对材料的相关性能进行了测定。

Sulfide layer was made on the surface of high speed steel (W6Mo5Cr4V2) by means of low temperature ion sulfurization. The tribological properties of the sulfide layer under dry sliding were investigated on an MM 200 friction and wear test rig. An atomic force microscope and a scanning electron microscope equipped with an energy dispersive spectrometer attachment were adopted to analyze the morphologies and compositions of the original and worn surfaces of the sulfide layer. The phase structure of the sulfide layer was determined by X ray diffraction.

采用低温离子渗硫工艺在 W6 Mo5 Cr4 V2高速钢表面制备了硫化物固体润滑层，在 MM- 2 0 0型摩擦磨损试验机上对渗硫层的摩擦学性能进行了干摩擦试验研究，用原子力显微镜及扫描电子显微镜和 X射线光电子能谱分析渗层表面、截面、磨面的形貌及成分，用 X射线衍射仪分析了渗硫层相结构。

Pristine Li-Al LDHs are synthesized by hydrothermal process in different reaction conditions by varying the aging time for 1 and 24 hours. Both the Li-Al layered double hydroxides (abbreviated as Li-Al LDH1 and Li-Al LDH24 for aging time 1 hour and 24 hours, respectively) were modified by using sulphanilic acid sodium salt hydrate, modified agent to form modified Li-Al LDH1-SAS and Li-Al LDH24-SAS. The morphology of the pristine layered double hydroxides are investigated by using wide angle X-rays diffraction, scanning electron microscopy and particle size analyzer which indicates that the crystallinity and aspect ratio is increased with increasing the aging time from 1 hour to 24 hours. The particle size of Li-Al LDH24 and Li-Al LDH1 are found to be ~1000 nm and ~250 nm, respectively. Both the pristine and modified LDHs are characterized by XRD, FTIR spectra and thermogravimetric analysis.

本研究目的在於改变长晶时间的长短，合成出同径大小的Li-Al LDHs，再经由改质剂sulphanilic acid sodium salt hydrate将Li-Al LDHs无机层材表面有机官能化制备出改质型Li-Al LDHs-SAS，於是进一步藉由扫描式电子显微镜、射径仪和穿透式电子显微镜等仪器分别观察LDHs改质前和改质后其主层结构型态上的变化；从中可以发现Li-Al LDHs随著长晶时间的增加其径有随之增大的趋势，但经有机化改质后其径会由於改质环境的影响明显低许多，针对此现象本实验将未改质和改质后之Li-Al人工无机层材制备成复材进一步探讨其在热性质和难燃特性上的为表现。

Infrared spectrum, X-ray diffraction, transmission electron microscopy and conductivity measurement were employed to investigate the properties and structure of polyaniline samples, which were synthesized by emulsion polymerization with different concentrations of ammonium peroxydisulfate and dodecyl-benzene sulphonic acid.

采用红外光谱、X射线衍射、透射电子显微术结合电导率测量，研究了以过硫酸钱为氧化剂，十二烷基苯磺酸为掺杂剂，通过乳液聚合法合成的聚苯胺的性能与结构。

Effects of temperatures on thaumasite formation were investigated.X-ray diffraction,scanning electron microscope,energy dispersive spectrum and laser Raman spectrum analysis were used to identify thaumasite in paste sample stored in 10% of MgSO 4 solution at different temperatures.

研究了环境温度对碳硫硅钙石形成的影响。降浸泡于不同温度的质量分数为10%的MgSO 4 溶液中的含石灰石粉水泥石试样进行X射线衍射分析、扫描电子显微分析、能谱分析和激光Raman光谱分析。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。