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Extensive experimentation revealed several issues, along with several corresponding solutions:(1) given that lithium metal dissolves slowly in liquid ammonia, considerable time was required to generate the dissolved metal solution (ca. 1 h);(2) the t -BuOH must be freshly distilled prior to use 21 to diminish the formation of ketone 19 (Figure 2);(3) efficient capture of the lithium enolate ( 11 ) required the use of freshly distilled TMSCl and Et 3 N; and (4) the presence of residual thiophenol upon workup was found to inhibit the subsequent Sc 3 -promoted hydroxymethylation.

大量实验揭示若干问题,随着几个对策 1鉴于锂金属溶化慢慢液氨、需要相当多的时间创造了金属溶液溶解(约占1小时);(2) T恤使操作必须事先用新鲜蒸馏水形成酮减少2119(图2);有效捕获的锂烯醇(11)使用新鲜蒸馏水需氯和ET三氮;含有残余硫workup经发现抑制随后推选3-羟甲晋升。

Methods:Pigspleen cells were cultured with HBvaccine and phytohaemagglutinin in which the sensitized cells were collected and homogenized to pieces by a constitution triturator;the homogenate was diluted with distilled water to 1∶1, then frozen and melt six times at25 ℃ before placed in the dialyzer at the melting state , after that dialyzed with 1∶4 distilled water as the outdialyzate at 4 ℃ for 48 h;the final outdialyzate was collected as the HBVSTF.

采用猪脾细胞与植物血凝素、乙肝疫苗共同培养,收集致敏细胞在组织捣碎机中破碎,用蒸馏水1∶1稀释,-25 ℃反复冻融6次,自来水融化后装入透析袋中,用1∶4的蒸馏水作透析外液,于4 ℃透析48 h,透析液即为乙肝病毒特异性转移因子。

Methods: Pig-spleen cells were cultured with HB-vaccine and phytohaemagglutinin in which the sensitized cells were collected and homogenized to pieces by a constitution triturator; the homogenate was diluted with distilled water to 1:1, then frozen and melt six times at -25℃ before placed in the dialyzer at the melting state, after that dialyzed with 1:4 distilled water as the out-dialyzate at 4℃ for 48 h; the final out-dialyzate was collected as the HBV-STF.

方法;采用猪脾细胞与植物血凝素、乙肝疫苗共同培养,收集致敏细胞在组织捣碎机中破碎,用蒸馏水1:1稀释,-25℃反复冻融6次,自来水融化后装入透析袋中,用1:4的蒸馏水作透析外液,于4℃透析48h,透析液即为乙肝病毒特异性转移因子。

Ingredients: 100% Distilled Witch Hazel, containing 14% Alcohol, Double distilled for purity.

成分:100%蒸馏金缕梅提纯液,含14%酒精,二次蒸馏提纯。

In distilled water,the means of percentage absorption for 7 days and 2 8 days were 30.15%and 27.85%(P<0.01),the percentage solubility for two stages were 0.79 and 1.16 (P<0.01).Conclusion. There is a tendency of declining for water sorption in both water with the soaking time increased in distilled water,both percentage of absorption and solubilit yare higher than those in artificial saliva respectively.

随着浸泡时间的延长,水凝胶材料的吸水率呈下降的趋势,在蒸馏水中的材料吸水率和溶解率均分别高于同期在人工唾液中的吸水率和溶解率。

It includes the following steps: extract trivalent iron ion and divalent iron ion in water phase through organic extractant, get predecessor of; absterge it with secondary distilled water for2-3 times and get pure load metal predecessor of organic phase; mix organic phase of Mg2 and Fe3 with mol rate of 1:2 and introduce them into autoclave, add distilled water according to the rate of 3:1 or 4:1 of organic phase and water phase and airproof it, and then mix it fiercely, stripping with hydrothermal method at temperature between 200 degree C and 300 degree C and make them react for 2.5 hours; cool it to the room temperature under natural condition, separate liquid and centrifugalize it, absterge it with absolute alcohol for 2-3 times and dry it at temperature of 50 degree C for 30-180 minutes, then get product of magnesium ferrite.

包括如下步骤:通过有机萃取剂来萃取水相中的三价铁离子和二价镁离子,制得有机相前驱物;用二次蒸馏水洗涤2-3次,获得纯净的负载金属有机相前驱物;按照Mg 2 和Fe 3 摩尔比1∶2将有机相混合均匀后引入高压釜中,按照有机相与水相的比例为3∶1或4∶1加入蒸馏水,密封后,对溶液进行强力搅拌,水热反萃的温度在200-300℃之间反应2.5小时;自然冷却至室温,分液,离心分离,用无水乙醇洗涤2-3次,在50℃下干燥30-180分钟,得铁酸镁产品。

To analyze results through statistical methods, and possess significant difference when P.05(a=0.05). To observe that effect of volume of distilled water on synthesis of hemihydrated gypsum is bigger, and the effect better when distilled water: raw materials as 150ml:100g; whereas effect of Calcium Chloride and sodium Succinate smaller, and the effect better when Calcium Chloride: dehydrated gypsum as 1:2, sodium Succinate as 0.75%.

采用统计学方法进行分析,P<0.05时具显著性差异(a=0.05)结果:在试验中观察到蒸馏水量对半水石膏合成影响较大,当蒸馏水与原料比为150ml:100g时效果较好;而氯化钙及丁二酸钠影响较小,当氯化钙与二水硫酸钙质量比为1:2,丁二酸钠为0.75%时效果较好。

Studying hatch rate of Hepialus under the condition of satu-ration/unsaturation, distilled water/salt water, mercuric liquid /distilled water, different temperature and different moisture.

采用青海拉脊蝠蛾受精卵,以饱满/不饱满受精卵、蒸馏水/盐水保湿、Hg溶液/蒸馏水3种处理和不同温度、湿度条件下进行孵化率试验。

Results: The ranges of MIC of DNA-2E on trichophyton rubrum and beard-like trichophyton were 0.0625~0.125mg/mL and 0.03125~0.125mg/mL respectively; of which there was no significant difference between the two fungi. Both 2% and 4% DNA-2E had better effects on ringworm of guinea pig in feet and body infected by beard-like trichophyton, which showed significant difference compared to distilled water and no significant difference compared to 1% Zuguang powder. Both 4% and 6% DNA-2E had better Antipruritic effect, which showed no significant difference compared to 2% Zuguang Powder and significant difference compared to distilled water.

结果:癣清(DNA-2E)对红色毛癣菌、须状毛癣菌的最低抑菌浓度范围分别为0.0625~0.125mg/mL和0.03125~0.125mg/mL,两组比较差异无显著性;2%和4%癣清(DNA-2E)对豚鼠须状毛癣菌感染足癣、体癣有较好疗效,与1%足光粉比较差异无显著性,与蒸镏水组比较差异有高度显著性;4%和6%癣清(DNA-2E)止痒作用与1%足光粉相比差异无显著性,与蒸镏水组比较差异有高度显著性。

Normal control group: the ordinary diet, double distilled water; model control group: low-iodine diet, double-distilled water.

正常对照组:普通饮食,双蒸水;模型对照组:低碘饮食,双蒸水。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。