查询词典 distillation method

The geologists have attached much importance to the particularity of ReOs isotopic system and its application is getting popular. The author sums up and compares several kinds of sample digestion methods for ReOs isotope analysis (NiS fire assay, Carius tube digestion, high pressure asher, leaching, and water disposing), the procedures of separating Os ( conventional distillation, liquid Br2 and CCl4 or CHCl3 extraction, rapid extraction with low blank, minitype distillation) and purifying Os, improved mass spectrometry measurement of Os isotope and its application progress in the earth science research brought along the improved measuring method.

总结和对比了近年来ReOs同位素分析中样品分解的不同方法（NiS火试金法、Carius管溶样法、高压灰化消解法、浸提法、水样处理法）、Os的分离（常规蒸馏、液溴和CCl4提取、快速低本底提取、小型蒸馏）与纯化流程、Os同位素比值质谱测定法（NTIMS、ICPMS、微区原位分析）及随测定方法的改进ReOs同位素体系在地球科学研究中的应用进展。

Molecular Distillation is a kind of high vacuum distillation method, which is suitable for the separation of high boiling, heat sensitivity and viscidity products.

分子蒸馏技术是一种在高真空条件下进行的连续蒸馏过程，适合于分离高沸点、热敏性及具有生物活性的混合物。

Firstly, this paper investigated roundly the basic theory of the ambient vibration method, analyzed systematically the main methods of ambient vibration identification, and discussed their advantages and disadvantages. Then we established the finite element model of structural dynamics and test model and analyzed their mutual relation, improved MUSIC method and correlation function method in the harmonic identification, and gave the subspace method and correlation function method based on continuous model, which is multi-harmonic retrieve technique. And then, this paper also puts forward least-squares method to estimate directly structural physical and modal parameters; this approach replaced the derivative operator in the continuous time model with an equivalent approximation, and estimated the physical parameters of structures by the least-squares method. And then, we discussed the approximation methods of derivative and their convergence. Finally, this paper researched the modal parameters of a frame structure by the simulation and test. The results demonstrated that subspace method, correlation function method and the least-squares method are effective and stable respectively.

全面地研究环境振动识别方法的基本理论，系统地分析环境振动识别方法的主要方法，讨论它们的优点和不足；建立结(来源：6666AB44C论文网www.abclunwen.com)构动力学的有限元模型和试验模型，分析有限元模型与试验模型之间的相互关系；改进谐波识别中的MUSIC识别方法和相关函数识别方法，给出大型结构模态识别的连续型的子空间分解识别方法和相关函数识别方法，这个方法是多元谐波识别方法；提出直接识别结构的物理参数和模态参数的最小二乘方法，这个方法利用导数的近似值代替导数值，并运用最小二乘方法识别结构的物理参数，讨论导数近似值的选择方法，分析算法的收敛性；通过仿真计算和模型实验，研究高层框架结构的模态参数识别，验证子空间分解识别方法、相关函数识别方法和最小二乘识别方法的有效性，算法的稳定性；从理论和试验两个方面分析和研究噪声对识别精度的影响，影响识别精度的因素，以及部分模态成分的模态参数不能够被识别的原因。

The revised Hargraves formula has the best result compared with Penman-Monteith formula, the average relative error is 6%, moreover, Hargaves method requiring the least data in calculating ETo, so this method has the high actual application value; The following are Radiation method and Blaney-Criddle method ; The worst is the Pan method, even after revised, the highest and average relative error is 36% and 10%, respectively. So, in this study, Penman-Monteith method, Radiation method, Blaney-Criddle method and Hargraves method are used except Pan method.

在这四种方法中，修正后的Hargraves方法与彭曼—蒙特斯方法的计算结果符合最好，其平均相对误差为6％，而Hargraves方法需要的气象数据只有计算时段的最高、最低温度，该方法具有较高的实际应用价值；辐射方法和布兰尼—克里德尔方法次之；蒸发皿方法最差，即使在修正后，E601型蒸发皿的最大误差也高达36％，平均为10％，所以在预报系统的研究设计中采用了除蒸发皿方法之外的四种方法。

The primary studying works and characteristics:1 To summarize reinforcing theory of cement mixing pile composite foundation2 To analyze the primary mechanics characters and changing rules of cement mixing pile, based on analysis of test data both indoor and outdoor.3 To discuss siding frictional resistance, ending resistance, ultimate bearing capacity of simple mixing pile and effectiveness factor of grouped piles, loading ratio of soil between piles under cushion cap of grouped piles and stress ratio of pile and soil and so on, and use many computation method and experimentation method to ensure bearing capacity of mixing piles composite foundation.4 To point out and analyze eight sides flaws and problems of the bearing capacity calculation method of mixing pile compositefoundation which ensured by national and normative method/ formula.5 To apply test results of loading tests and a few settlement observation data, use gray theory to predicate ultimate bearing capacity of deep mixing piles, actual example demonstrate engaging between theoretical predicted value and actual value.6 To apply groovy layerwise summation method to discuss entity piles method, double foundation method, equivalent layerwise summation method and consolidation theoretical method and so on, especially by combination of engineering example, use FEM to calculate or discuss the settlement and changing rules of composite foundation.7 To discuss problems of critical length of composite foundation by combination of engineering example and numerical analysis method, and analyze the contrast of critical length between simple pile load and most area load of composite foundation, not only critical length of composite foundation is relative to modulus ratio between piles and soil, but also upside load distribution area of composite foundation.

主要的研究工作与特色为：(1)总结了水泥搅拌桩复合地基的加固原理；(2)在对室内外试验资料进行统计分析的基础上，系统分析了搅拌桩水泥土的主要力学特性及其变化规律；(3)探讨了搅拌单桩的侧摩阻力、端阻力、极限承载力及群桩效率系数、群桩承台下桩间土荷载分担比及桩土应力比等，提出用多种计算方法并结合试验方法来综合确定搅拌桩复合地基的承载力；(4)明确指出和分析了按国家有关规范的方法确定搅拌桩复合地基承载力所存在的八个方面的缺陷与问题；(5)利用过去没有加载至破坏阶段的载荷试验成果和较少的沉降观测数据，尝试了用灰色理论预测深层搅拌桩的极限承载力，实例表明理论预测值与实测值吻合较好；(6)在常规分层总和法的基础上，探讨了复合地基沉降计算的实体墩基法、双层地基法、等效作用分层总和法、固结理论法等，特别是结合工程实例，用有限元数值计算等方法计算和讨论了搅拌桩复合地基的沉降及其变化规律；(7)结合工程实例，用数值分析方法探讨了复合地基临界桩长的问题，指出和分析了单桩荷载下的临界桩长与复合地基大面积荷载下的临界桩长存在很大的差别，复合地基的临界桩长不仅与桩土模量比有关，而且与复合地基上部荷载分布面积有关。

Through the steps such as acidify, filteration, extraction , distillation and vacuum distillation, the product is seperated from compounds.

通过酸化、过滤、萃取、常压蒸馏和减压蒸馏等后处理手段，将产物分离出来。

Main contributions and achievements are as follows:A general non-equilibrium rigorous model for RDP is developed in this thesis. Based on the pseudo-homogenous assumption, two main factors reaction and separation are de-coupled, and an RDP model with the same format as that for a traditional distillation process is established. To solve the model with a large number of algebraic equations, modified M-K equations with tri-diagonal matrix form are developed based on the improved Separation Efficiency Functions, which greatly increases the iteration efficiency. This thesis also develops a general reactive distillation dynamic model. Through splitting of the differential variables based on SEFS, large-scaled differential algebraic equations can be solved with the improved Gear's algorithm which makes the dynamic model suitable for the on-line application. A simulation platform for the control loop design and evaluation of RDP by introducing control system equations into the dynamic model is also developed.A lactic acid purification pilot-scale RDP is investigated.

论文对热点问题——反应精馏过程的建模与优化控制相关技术进行了深入的研究，取得了一系列成果：1、建立了反应精馏过程机理模型，基于拟均相假设，将反应和分离过程进行解耦，推导出反应精馏过程的非平衡级稳态模型和动态模型，通过引入推广的分离效率函数，对模型变量进行了合理划分，显著提高了模型求解效率；将动态模型和控制系统方程结合，建立了反应精馏过程控制系统研究的辅助工具。2、全面分析了乳酸提纯反应精馏新工艺试验装置，利用本文建立的过程机理模型，对该试验装置进行了稳态和动态性能分析及水力学核算；设计和分析了单边质量控制方案，比较了间接和直接物料平衡控制两种方案的控制性能。

Secondly, the optimum operating conditions of the batch distilling tower for separating amyl alcohol from the fusel oil were found by applying CC-BATCH, a batch distillation model of the chemical engineering simulative system named ChemCAD5.0, to simulate and calculate the special technological process of salt outing-special batch distillation.

其次，利用ChemCAD化工模拟系统软件中的CC-BATCH间歇精馏模块对"盐析—特殊间歇精密精馏法"从杂醇油中制备C5醇的分离工艺进行了全流程模拟优化计算，模拟过程在所设限定条件下能满意收敛，所得结果与实验结果基本上一致。

Based on the success of the industrialization of the process of catalytic distillation of methyl acetate hydrolysis, the new process of catalytic distillation of methyl acetate and methanol azeotrope hydrolysis and related fundamental research were studied.

本文在催化精馏水解工艺工业化成功的基础上，进行了醋酸甲酯和甲醇共沸物催化精馏水解新工艺及其相关基础研究，以进一步改进工艺，达到简化流程及节能降耗的目的，同时建立起催化精馏过程模拟和设计的理论体系，为中试及将来的工业化打下了坚实的基础。

Extractive distillation is defined as distillation in the presence of a miscible, high boiling, relatively non-volatile component, the solvent, that forms no azeotrope with the other components in the mixture.

淬取蒸馏的定义为：有易混合的、高沸的、相对难挥发的组分和溶剂存在下的蒸馏，且这些组分和溶剂不与混合物中的其它组分形成恒沸物。

Listen,point and check your answers.

听，指出并且检查你的答案。

Warming needle is one of effective treatment methods for knee arthralgia aggravated by cold,and it is simple,safety,so it should be developed in clinical acupuncture and moxibustion extensively.

但以本院科针灸门诊在2005年1月—2006年6月期间共收治膝痛患者100余例，经过临床的诊断后，其中施以温针治疗的48例，疗效显著，报道如下。1临床资料本组病例48