查询词典 distillation method

TEM shows that drying by direct heating might result in hard aggregation of the tourmaline powder, while hard aggregation might be avoided by azeotropic distillation. Raman spectroscopy reveals that there are O_H and C_H on the surfaces of the tourmaline powder obtained by azeotropic distillation, which indicates that butoxy is chemically adsorbed on the surfaces of tourmaline particles, but not adsorbed on those formed by direct drying. X_ray powder diffraction shows that the intensity of diffraction peaks decreases after grinding. There is no damage to the tourmaline crystal lattice in the process of direct heating, azeotropic distillation, or ultrafine grinding.

透射电镜分析结果表明，直接加热脱去水或正丁醇会使电气石超细颗粒发生硬团聚，而共沸蒸馏法则可有效防止硬团聚的产生；拉曼光谱结果表明，共沸蒸馏法制备的电气石粉末表面存在O—H和C—H键，说明正丁醇在颗粒表面为化学吸附，而直接干燥法得到的电气石粉末表面则没有；X射线粉晶衍射结果表明，研磨过程降低了粉末衍射峰的强度，但直接加热干燥和共沸蒸馏干燥均未破坏电气石的晶格结构。

The invention relates to a dynamic matrix control system of high-purity distillation, which comprises distillation tower, intelligent checker, DCS system, superior host, and on-site bus, while they are connected. The control system uses tower product group as the object variable, and the reflux ratio and reboil ratio as control variable; the superior receives history temperature and pressure data from the DCS real-time database, via the predict control and dynamic matrix controller, to obtain the output values of present controller as reflux ratio and reboil ratio, then feedback said two values to DCS system, to function the distillation object. The invention can confirm the high-purity stable operation, with better dynamical control.

本发明公开了一种高纯精馏的动态矩阵控制系统和方法；系统包括：精馏塔、智能检测仪表、DCS系统、上位机和现场总线；所述精馏塔、智能检测仪表、DCS系统和上位机通过现场总线依次相连，实现信息流的上传和下达；本发明所涉及的控制系统采用塔双端产品组分为被控变量，回流比和再沸比为对应的控制变量；上位机从DCS实时数据库中获得历史的温度、压力等数据，通过推断控制环节和动态矩阵控制器环节，得到当前控制器的输出值-回流比和再沸比，再把控制器输出值返回给DCS系统，实现了对高纯精馏过程的双端产品高纯控制，对双端组分的高纯度平稳操作，具有很好的动态品质和控制效果。

Molecular Distillation, also termed as Short Path Distillation, is a special distillation technology.

分子蒸馏也称短程蒸馏，是一种特殊的蒸馏分离技术。

In this paper Ⅰ successfully applied these methods to fault diagnosis, and presenting some new innovative machinery fault diagnosis method; First Ⅰ present a new gear wornout fault diagnosis method, this method use the vibration signal's time-frequency attribute and instantaneous phase undulation to accurately detect gear's fault, and by comparing with the traditional frequency domain analysis method, this method reveals that many nonlinear and nonstationary characteristic exist in gear's vibration, this tell us that if we use frequency domain analysis method without pay attention to the signal's characteristic, we could get wrong diagnostic result; Then Ⅰ present a new bearing fault diagnosis method, this method use ATVFD and Hilbert transform to do envelop demodulation,Ⅰ analyze the envelop with time-frequency method and find out that this method is more accurate then traditional method.Ⅰ also explain that the modulation of the fault to the carrier wave may also be non-stationary and nonlinear; Finally Ⅰ present a cylinder pressure measurement method of diesel engine by means of vibration, cylinder pressure is an important parameter of diesel engine fault diagnosis, the pressure measuring is simplified a lot by this method,Ⅰ also use the ATVFD and time-frequency analysis to realize it.

本文中将上述理论方法成功地应用到故障诊断中去，提出了几点创新性的诊断方法；提出了一种齿轮磨损故障诊断的新方法，该方法利用振动信号能量的时频域分布特征与瞬时相位波动特征可以进行精确的齿轮故障诊断，并通过与传统的频域诊断方法的比较，揭示出齿轮振动中存在的明显的非线性与非平稳特征，说明了不加选择地利用频域分析方法进行齿轮故障诊断很可能会得到错误的诊断结果；提出了一种轴承故障诊断的新方法，该方法利用ATVFD分解与Hilbert变换进行包络解调，并对解调得到的包络信号进行时频域分析，可以实现更加准确轴承故障诊断，说明了故障对载波信号的调制往往也是非平稳与非线性的；提出了一种利用振动信号进行柴油机汽缸内压力检测的新方法，柴油机汽缸压力的变化是柴油机故障诊断的重要参数，利用振动方法可大大简化汽缸压力的检测过程，该方法也是综合利用ATVFD分解与时频域分析方法实现的。

The Bidiagonal matrix method for the simulation of distillation and catalytic distillation is developed. The bidiagonal matrix method is proved to be better in convergcnce and stability by compared with the tridiagonal matrix method.

在多组分精馏塔的稳态模拟计算中，三对角矩阵法具有占用计算机内存少，无需计算偏导数矩阵等优点，但对强非理想性体系有时计算不收敛。

This train classifies "information carrier adhering to the build" as design elements, and probes into integrated design method of it and single building separately: method of definite position, method of definite form and method of combination; Then, this train probes into integrated design method of it and colonys building , that bases on the cognitive design method: method of rhythm controls,method of node outstanding, and that aims at the design method to protect: method of protect original, method of repairing and method of renewal.

本文的第四部分提出了一体化设计的思路，将建筑附着信息载体作为设计元素，探讨了它与建筑单体一体化设计的方法：定位法、定形法、混合法；以及它与建筑群体一体化设计时，基于认知的设计方法：节奏控制法、节点突出法，旨在保护的设计方法：存真法、修缮法、更新法。

The test method is to fetch the urea of the same quality and coated material of different quality first, make coating material parcel evenly the urea particle s surface, grant them into the soil, eluviate with the distilled water every 24 hours, collect the eluviationing solution, titrate the eluviationing solution with distillation titrimetric method, that is, add alkali distillation, make the ammonia release out, absorb with boric acid solution, then titrate it with standard acid.

试验方法是称取相同质量的尿素和不同质量的包膜材料，将包膜材料均匀地包裹在尿素颗粒的表面，将包裹后的包膜肥料施入模拟试验的土壤中，每隔24个小时用蒸馏水淋溶，收集淋溶液，用蒸馏滴定法滴定淋溶液，即加碱蒸馏，使氨释放出来，用硼酸溶液吸收，而后用标准酸滴定之。

In the end, the extractive distillation method was applied to separate and purify the binary azeotrope mixture, methanol-dimethyl carbonate. The isoamyl acetate was used as extractant and the two tower system was introduced to continuous extractive distillation operation. The results show a better separation effect.

最后采用萃取精馏的方法，对甲醇-碳酸二甲酯的二元共沸混合物进行了分离提纯研究，以毒性较低的乙酸异戊酯为萃取剂，采用两塔连续萃取精馏操作，结果表明，分离效果比较理想。

Although batch distillation has been dealt with more than 100 years, the design methods developed to date have some disadvantages, most of which are derived from FUG method for continuous distillation or from experiences under the assumption of no holdup and no slop cuts.

多组元分批精馏过程和设计方法的研究分批精馏

The volatile components in Morinda officinalis How were extracted by distillation extraction methodand simultaneous distillation extraction method.

采用水蒸气蒸馏萃取法和同时蒸馏萃取法提取巴戟天的挥发性成分，并用气相色谱-质谱仪对提取成分进行定性、定量分析。

Listen,point and check your answers.

听，指出并且检查你的答案。

Warming needle is one of effective treatment methods for knee arthralgia aggravated by cold,and it is simple,safety,so it should be developed in clinical acupuncture and moxibustion extensively.

但以本院科针灸门诊在2005年1月—2006年6月期间共收治膝痛患者100余例，经过临床的诊断后，其中施以温针治疗的48例，疗效显著，报道如下。1临床资料本组病例48