查询词典 distillation method

On the basis of summarizing separation method of acetic acid-water system, we studied the azeotropic distillation process of acetic acid-water system, selecting butyl acetate, isobutyl acetate and isopropyl acetate as entrainers. The influence of packing height, ratio of water to entrainer and acetic acid initial concentration to separation effect of azeotropic distillation was studied in detail. Simulation calculations of general distillation and azeotropic distillation were carried out. The influence of reflux ratio, theoretical plate, feed position, feed temperature and feed concentration to distillation process were discussed. Preferred process operation parameter, which had guiding meaning to practical production of distillation process were obtained. Basic data for the process amplifying design of azeotropic distillation tower were provided. Invest and operation energy consumption of two distillation methods were compared. The elementary technical design of azeotropic distillation tower was carried out on the basis of result of simulation calculation. The type of major auxiliary equipments and inner parts of packed tower were selected.The research results are as follows:(1) Butyl acetate, isobutyl acetate and isopropyl acetate could be selected as entrainer, and separation effect was near.

本文在综述醋酸-水体系分离方法的基础上，以醋酸丁酯、醋酸异丁酯、醋酸异丙酯为挟带剂，对醋酸水溶液进行共沸精馏过程研究，详细研究了填料高度、水与挟带剂的配比、醋酸初始浓度等对共沸精馏分离效果的影响；对醋酸-水体系进行普通精馏和共沸精馏过程模拟计算，讨论了回流比、理论板、进料位置、进料温度和浓度对精馏过程的影响，获得了对醋酸-水体系精馏过程实际生产具有指导意义的较佳的工艺操作参数、共沸精馏塔的工艺设计放大的基础数据，并对两种精馏方法的投资、操作能耗进行了比较；同时在共沸精馏模拟计算的基础上进行了共沸精馏塔的初步工艺设计计算，并对填料塔的主要辅助设备及塔内件进行了初步选型。

The following points are emphasized:The operation models of adiabatic and diabatic distillation have been set up and the operation block, thermodynamics model and mathematical model in the simulation have been determined as well;(2)Based on the simulation and exergy analysis with Aspen Plus program, shortcut distillation design—DSTWU model and rigorous distillation design—RADFRAC model, the author has determined the heat duty, exergy losses and the distribution of exergy losses along the adiabatic column, which will help the simulation and optimization of the diabatic distillation;(3)Diabatic distillation under various operation conditions has been simulated by using energy balance method and exergy analysis;(4)How the different mixture and the various degree of separation, number of trays and feed location influence exergy saving in diabatic distillation have also been discussed;(5)On the basis of the total exergy losses along the column, different schema of the heat transfer distribution along the column have been compared and analyzed;they can be classified in three categories: heat duty equipartition approach, empirical approach, separation degree matching approach. In conclusion, different heat transfer distribution along the column will have effect on total exergy losses. In particular, most satisfactory results have been obtained by using separation degree matching approach. In order to diminish the exergy losses, heat transfer distribution should meet the needs of the request of separation degree.And on this premise, the author makes his suggestion in increasing the proportion of heat supplied to the tray with minimum exergy losses and decreasing the proportion of heat supplied to the tray with the maximum exergy losses.

本文对透热精馏过程进行了模拟并对其节能效果的影响因素做了较为全面的分析和深入的研究，主要研究内容如下：(1)建立了常规精馏和透热精馏过程的模拟操作模块、热力学模型以及数学模型；(2)利用化工模拟软件Aspen Plus并分别采用DSTWU简捷模型和RADFRAC严格计算模型对常规精馏进行模拟计算和有效能分析，确定常规精馏塔的公用工程热负荷、有效能损失及有效能损失在塔内的分布，为透热精馏的模拟和优化提供数据参考；(3)对不同物系在不同分离度条件下进行透热精馏的模拟，分别采用能量衡算法和有效能分析法进行计算和分析；(4)探讨了各种因素如物系的选择、不同分离度、塔板数、进料位置对透热精馏节能效果的影响；(5)以全塔总有效能损失为比较基准，对热量在塔内的三种分布方案即热负荷平均分配法、经验法和分离度匹配法进行了对比分析并得出结论：塔内热量的不同分布方案对于全塔总有效能损失会产生影响，其中以分离度匹配法的节能效果最为理想，为减少有效能的损失，应使塔内的热量分布满足各塔板的分离度要求，并在此前提下，尽量减小有效能损失大的塔板的热负荷和增加有效能损失小的塔板的热负荷。

Batch extractive distillation is used to separate azeotrope or the mixture of which the relative volatility is close to 1.0. For it has both advantages of batch distillation and extractive distillation, batch extractive distillation is becoming increasingly important to the production of small scale and high value products like fine chemicals and pharmaceuticals.

间歇萃取精馏是分离共沸物或近沸物的一种方法，由于它结合了间歇和萃取的优点，特别适用于化工、制药、溶剂回收、天然产物提取等产量小，品种多的行业，因此间歇萃取精馏近年来已成为非常活跃的研究和开发领域。

The presumption that new technology about distillation column with a single reactor can be used in photochlorination of acetic acid is first proposed in this paper. The fact that reaction distillation has obvious advantages in the number of theoretically perfect trays and energy consumption was obtained by theoretical analysis between the coupling of reaction and distillation and the independent operation, which lays a theoretical foundation on the application of the distillation column with a single reactor in photochlorination of acetic acid.

本文首次提出了将背包式反应精馏耦合技术应用于乙酸氯化反应的设想，通过对反应精馏耦合和反应精馏独立操作两种情况进行理论分析，发现反应精馏耦合在理论板数、能耗方面均具有明显优势，因而为背包式反应精馏应用于乙酸光氯化反应奠定了理论基础。

Using ASTM method as basic model,a method is proposed for measuring distillation range of petroleum fractions by Engler distillation related with gas chromatography simulated distillation technology.

以美国材料与试验协会方法为基础模型，提出一种基于色谱模拟蒸馏技术的恩氏蒸馏馏程测定方法。

By soluting each level respectively, which makecomplex of construcing heat pump distillation process to be a better solution. By analyzing the thermodynamic properties of conventional distillation and heatpump distillation, mathematical model and computational method is established. Byoptimizing method of designing various structures, the most costeffective isdetermined.

通过分析常规和热泵精馏系统的热力学特性，建立了热泵精馏流程数学模型及优化设计方法，针对不同的热泵精馏流程结构采用不同的优化设计方法以获得最大的经济效益；为验证热泵精馏流程的可行性提供有利依据，建立了用于确定热泵精馏热集成方案的经济评价标准；将策略与优化设计算法相结合应用于热泵精馏流程，以实现构建较优热泵精馏流程。

Main points of the thesis are as follows:(1) The main function models and information relations between these models in the CAPP system in the integrated CAD/CAM project are explained, a new process plan design method is mentioned based on analyses of process plan design. This method is based on the process plan prototype, and develops the prototype little by little until the perfect process plan is completed, the prospect of this method is discussed;(2) The feature abstracting rules and methods are studied, a feature coding system is developed based on GT, all the defined feature models are described by the mathematical methods;(3) The integrated method of CAD/CAPP based on features is mentioned, this method defines a feature exchanging model, and develops an interface software to exchange design data into technology data base, this technology data base includes the design and technology information of the parts;(4) The process plan reasoning method based on features is created, this method uses Mycin algorithm to solve the reasoning of the feature process plan. A process plan making system is developed. In this system part process plan is made by the semi-intelligent method, this method uses the feature reasoning, feature process chain searching and man-computer talking together;(5) The main structure of the HOPE system is introduced, a shaft drawing and its process plan made by this system are shown, the data process problem in process drawing making is also discussed;(6) A new method of describing process rule is introduced, this method uses IfThen rules and neural nets weight values together to describe process rules, the BP algorithm is adopted in this method;(7) The optimal machining sequence problem of the process steps on the same fixturing is discussed, optimal algorithms SA is applied to solve this problem, the result shows that this method is more efficient than the traditional method;(8) All jobs in the thesis are summarized. In order to carry out the research in the future, some rational proposals are given.

全文论述的内容主要有下列几个方面：(1)较为系统地阐述了CAD／CAM一体化工程项目中CAPP系统的主要功能模块及其信息流程，在分析工艺设计过程的基础上，提出了基于特征原型的渐进式工艺设计方法，并探讨了该方法的应用前景；(2)研究了零件特征提取的原则和方法，在成组技术的基础上，开发了一套基于特征的分类编码系统，并在提取零件特征的基础上，定义了零件特征的数据模型，开发了基于轴类零件特征的参数化设计系统；(3)研究了基于特征的CAD／CAPP集成的方法，通过定义零件特征数据模型的存储结构，开发了将设计数据转换到工艺数据库中的接口程序，为后续的CAPP系统提供必要的零件形状和工艺信息；(4)研究了基于特征的工艺推理方法，将Mycin算法应用到工艺决策中，开发了基于特征的工艺推理及工艺方案生成系统，在系统中综合运用特征推理、特征加工工艺链查询及人机对话相结合的半智能化方法确定零件加工工艺；(5)介绍了整个HOPE系统的总体结构，通过运行HOPE系统绘出了一轴类零件的零件图，并生成了该零件的加工工艺方案，初步探讨了基于特征的工序图生成技术中数据处理问题；(6)研究了工艺设计过程中知识如何有效表示的问题，提出了将显式的IF-THEN规则表示与隐式神经网络权值表示相结合的工艺知识表示方法，并利用BP算法进行了工艺知识表示的初步研究；(7)研究了工艺设计过程中同一安装下工步优化排序问题，利用神经网络中基于模拟退火的理论来解决该工步优化排序问题，实践证明该方法较传统的算法具有更高的效率；(8)总结了本文所进行的研究工作，为今后进一步开展工作提出了较为合理的建议。

Based on the success of the industrialization of the process of catalytic distillation of methyl acetate hydrolysis, the new process of catalytic distillation of methyl acetate and methanol azeotrope hydrolysis and related fundamental research were studied. These can make further improvement on the process in order to simplify the process and reduce the energy-consumed of the recovery system. In addition, theoretical system of the simulation and design the catalytic distillation process were established, which can provide the basis of the pilot plant and industrialization in the future.

本文在催化精馏水解工艺工业化成功的基础上，进行了醋酸甲酯和甲醇共沸物催化精馏水解新工艺及其相关基础研究，以进一步改进工艺，达到简化流程及节能降耗的目的，同时建立起催化精馏过程模拟和设计的理论体系，为中试及将来的工业化打下了坚实的基础。

Such factors as distillation temperature and distillation pressure, etc. which affect the process of preparing citral from Litsea cubeba oil and of preparing cinnamaldehyde from cassia oil by molecular distillation were investigated under rotation of 370～390 r/min,flow rate of 1drop/s,and temperature of cooling water 4～5℃.

利用分子蒸馏新技术从天然香料肉桂油和山苍子油中分离提纯肉桂醛和柠檬醛，用GC–MS联用仪对分离物中肉桂醛和柠檬醛的质量分数进行分析，重点研究了压力和温度等主要影响因素。

At present, on-line analyzer of distillation range normally use theory of RTP distillation that only can analyze a point or discontinuity of distillation range.

但由于高温操作、微量进样、信号微弱等特点，将色谱模拟蒸馏方法在线化的色谱模拟蒸馏在线分析仪，在国外还处于起步阶段，而在国内则属空白。

Listen,point and check your answers.

听，指出并且检查你的答案。

Warming needle is one of effective treatment methods for knee arthralgia aggravated by cold,and it is simple,safety,so it should be developed in clinical acupuncture and moxibustion extensively.

但以本院科针灸门诊在2005年1月—2006年6月期间共收治膝痛患者100余例，经过临床的诊断后，其中施以温针治疗的48例，疗效显著，报道如下。1临床资料本组病例48