查询词典 dioxane

Dioxane is a byproduct of a chemical processing technique called ethoxylation in which cosmetic ingredients are processed with ethylene oxide.

在受检的48种洗浴用品当中，有 67%被检出含有 1，4-二噁烷，后者是许多化妆品原料加工过程中产生的副产品。

In addition, the stability of ternary Cu 〓complexes polypyridyl=1, 10-phenanthroline (Phen , pyrido [3, 2-f] [1, 7] phenanthroline , 1, 4, 8, 9-tetraazatriphenylene , dipyrido [3, 2-a: 2'3'-c] phenazine , imidazo phenanthroline and 2-phenylimidazo phenanthroline , NTP=ATP and UTP was studied by potentiometric pH titration in water at temperature 15℃, 25℃ and 35℃, and in 30% and 50% aqueous dioxane solution at 25℃.

另外，用pH电位滴定法研究了多吡啶芳香配体polypyridyl配合物Cu〓（PL=1，10-邻菲咯啉、吡啶并[3，2-f][1，7]邻菲咯啉、1，4，8，9-四氮三联苯、二吡啶并[3，2-a∶2'3'-c]吩嗪和2-苯基咪唑并邻菲咯啉或咪唑并邻菲咯啉）在不同温度（15℃、25℃和35℃）水溶液及30%和50%二氧六环-水混和溶剂（25℃）中的稳定性。

The other for: safrole, sassafras oil, safrole different 82 yuan / kg; 1 - phenyl -2 - propanone 2,500 yuan / kg; 3.4 dioxane methylene diphenyl -2 - propanone 7200 yuan / ton; Piperonal 1,000 yuan / kg; N-acetyl-o-amino benzoic acid 11500 yuan / ton; anthranilic acid 15,500 yuan / ton; Phenylacetate 15,000 yuan / ton; acetic anhydride 9900 yuan / ton; trichloromethane 4100 yuan / ton ; anhydrous ether 8500 yuan / ton; piperidine 58000 yuan / ton; methyl ethyl ketone 10,000 won / ton; sulfate 1,200 yuan / ton; hydrochloride 400 yuan / ton; ethanol 4200 yuan / ton.

另供：黄樟素、黄樟油、异黄樟素82元/公斤；1-苯基-2-丙酮2500元/公斤；3.4 亚甲基二氧苯基-2-丙酮7200元/吨；胡椒醛1000元/公斤；N-乙酰邻氨基苯酸11500元/吨；邻氨基苯甲酸15500元/吨；苯乙酸15000元/吨；醋酸酐9900元/吨；三氯甲烷4100元/吨；无水乙醚8500元/吨；哌啶58000元/吨；甲基乙基酮10000元/吨；硫酸1200元/吨；盐酸400元/吨；无水乙醇4200元/吨。

The other for: safrole, sassafras oil, safrole different 82 yuan / kg; 1 - phenyl -2 - propanone 2,500 yuan / kg; 3.4 dioxane methylene diphenyl -2 - propanone 7200 yuan / ton; Piperonal 1,000 yuan / kg; N-acetyl-o-amino benzoic acid 11500 yuan / ton; anthranilic acid 15,500 yuan / ton; Phenylacetate 15,000 yuan / ton; acetic anhydride 9900 yuan / ton; trichloromethane 4100 yuan / ton ; anhydrous ether 8500 yuan / ton; piperidine 58000 yuan / ton; toluene 5200 yuan / ton; methyl ethyl ketone 10,000 won / ton; sulfate 1,200 yuan / ton; hydrochloride 400 yuan / ton; anhydrous Ethanol 4200 yuan / ton.

另供：黄樟素、黄樟油、异黄樟素82元/公斤；1-苯基-2-丙酮2500元/公斤；3.4 亚甲基二氧苯基-2-丙酮7200元/吨；胡椒醛1000元/公斤；N-乙酰邻氨基苯酸11500元/吨；邻氨基苯甲酸15500元/吨；苯乙酸15000元/吨；醋酸酐9900元/吨；三氯甲烷4100元/吨；无水乙醚8500元/吨；哌啶58000元/吨；甲苯5200元/吨；甲基乙基酮10000元/吨；硫酸1200元/吨；盐酸400元/吨；无水乙醇4200元/吨。

A commercial and practical synthesis rout with-2-(3-acetoxy-l-me-thyl-l~propenyl)-5,5-dimethyl-l,3-dioxane as starting material by couple,oxidation, Ramberg-Backlund and deprotection is chosen and studied in this paper.

本文选择了以2-(3-氯-1-甲基-1-丙烯)-5，5-二甲基-1，3-二噁烷为原料，经偶连、氧化、Ramberg-Bcklund反应及脱保护基四步反应的合成路线，对该中间体进行合成研究。

The result indicated that the reacting mixture containing dioxane 11.3mL/g HDCA which had been added ethyl chloroformate drop wise should be keep at 10℃ for 30min, then, rising to 15℃ for another 20min in the step of forming mixed anhydride ,and 1.5mol/L NaOH was used to dissolve taurine before aminolysis, and crude product was recrystalled by acetone in purifying process.

结果表明，形成混酐时，二氧六环用量为11.3ml/g HDCA，滴加氯甲酸乙酯后先在10℃反应30min，再在15℃下反应20min；用1.5mol/L的NaOH水溶液溶解牛磺酸后再进行氨解；粗产品用丙酮重结晶。

H-Tyr-OH was then react with fluorenylmethyl chloroformate in dioxane or THF to give N-Fluorenylmethoxycarbonyl-O-benzyltyosine Fmoc-Tyr(Bzl-OH in 98% yield.

酪氨酸苄醚与芴甲氧羰基氯(Fmoc-C1)反应，成功地在氨基上导入了芴甲氧羰基保护基，反应在二氧六环或四氢呋喃中进行，产率达到98%。

Collagenase activity was defined as the radioactivity extractable by 50% dioxane. Clostridial collagenase was used as a standard. The lower limit of this assay method was 0.01 units of clostridial collagenase. Among 17 glaucoma eyes, 6 had trace collagenase activity (around 0.01 units) in aqueous humor; and for cataract eyes, 8 out of 27 had trace collagenase acitivty.

我们所采用之测量方法可侦测出约0.01单位以上的胶原酵素；一般前房液之胶原酵含量非常低，许多患者无法以我们之方法利得胶原酵素之存在：17位青光眼患者中，只有6位可於其前房液中到得约0.01单往之胶原酵素；27位白内障急者中，有8位可测得微量胶原酵素；二者在统计学上与太大差异存在。

The optimum reaction condition was as follows: catalyst dosage=4.3% of the amount of ethanediol,reaction time 50 min.1,4-dioxane yield of 84.82% was obtained under the optimum condition.

考察了催化剂用量、反应时间和反应温度等因素对收率的影响，得出最佳反应条件：催化剂用量为乙二醇质量的4.3%，反应时间50 min，收率可达84.82%。

P-toluene sulphonic acid catalyst ; ethanediol ; 1; 4-dioxane synthesis

对甲苯磺酸；催化；乙二醇； 1； 4-二氧六环

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。