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Finally, the cytotoxic and antibacterial activities of the oxamido-bridged binuclear complexes were studied in vitro.. This dissertation consists of three sections as follows:1. The crystal structure of a oxamide dinitrate,(1) [H_4dmaeoxd](NO_3)_2 H_2dmaeoxd = N,N\'-bis[2-ethyloxamide, has been obtained. The diversity of complexes with different structures is carried out by successful synthetic strategy of controlling species of metal ions, counter anions, pH values and solvents in the course of synthesis. Four dinuclear complexes bridged by trans-dmaeoxd2-: [Cu_2_2](ClO_4)_2 (2), [Cu_2_2](ClO_4)_2 (3),、[Cu_2(Me_2phen)_2](ClO_4)_2 (4), [Cu_2_2(H_2O)_2] (5); Four dinuclear complexes bridged by cis-dmaeoxd2-: [NiNi_2](ClO_4)_2 (6), [CuNi_2](ClO_4)_2·2CH_3OH (7), [CuZn_2]-(ClO_4)_2·2H_2O (8), [Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9); three 1-D polynuclear complexes: [Cu_2]_n·nH_2O (10), [Cu_2(H_2O)_2-]_n·4nH_2O (11), [Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12); one 2-D polynuclear complex,[Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n).2nH_2O (13); the others: [VO(H_2O)]·2H_2O (14), [Zn_2_4](ClO_4)_2·H_2O (15), [Cu_2]·2DCM (16) have been synthesized and characterized by X-ray single crystal diffraction, elemental analysis, IR spectra.

本论文主要包括以下三部分：一、合成得到了一个草酰胺配体硝酸盐的单晶结构，[H_4dmaeoxd](NO_3)_2 (1)；通过调控金属离子的种类、端基配体、抗衡阴离子、溶剂、pH值等条件定向合成了四个反式草酰胺桥联双核铜配合物：[Cu_2_2](ClO_4)_2 (2)、[Cu_2_2](ClO_4)_2 (3)、、[Cu_2(Me_2phen)_2](ClO_4)_2 (4)、[Cu_2_2(H_2O)_2] (5)；四个顺式草酰胺桥联同/异双核配合物：[NiNi_2](ClO_4)_2 (6)、[CuNi_2](ClO_4)_2·2CH_3OH (7)、[CuZn_2]-(ClO_4)_2·2H_2O (8)、[Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9)；三个一维聚合物： [Cu_2]_n·nH_2O (10)、[Cu_2(H_2O)_2-]_n·4nH_2O (11)、[Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12)；一个二维聚合物： [Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n)。2nH_2O (13)；单核钒配合物[VO(H_2O)]·2H_2O (14)、草酸根桥联双核锌配合物[Zn_2_4](ClO_4)_2·H_2O (15)、美洛西康铜配合物[Cu_2]·2DCM (16)，利用元素分析、摩尔电导、红外光谱、电子光谱和单晶X-射线衍射对上述所得化合物进行了结构表征，探讨了结构影响因素，并研究了其超分子结构。

Based on the failure analysis of hot roll, this paper optimizedly adjusts alloy system and summarizes the experience of rolling wiresand improves ail processing properties. Then, it analyses the effects on some natural parameters such as alloy transfer coefficient, surfacing layers, welding current and arc voltage etc.. It confirms the fitting ageing technique. Also, it discusses the microscopic structural transformation back and forth ageing and the effects on hardness change of overlaying metal by some alloying elements including C, Cr, V, W, Mo, Ni, Mn, B, Re through OM, SEM and X-ray diffraction analyses. Finally the abrasive resistance, red hardness, thermal fatigue property and anti-high temperature oxidability are investigated in experimentation.

全文在热轧辊失效分析的基础上优化调整合金体系，总结了焊丝轧制的经验，改善各种工艺性能，分析了几个特性参数的影响，确定了适宜的时效工艺，并通过光学显微镜、扫描电镜和X-射线衍射对时效前后的显微组织转变以及部分合金元素如C、Cr、V、W、Mo、Ni、Mn、B、Re对堆焊层硬度变化的影响进行分析，最后通过试验考察了堆焊层金属的耐磨粒磨损性能、红硬性、耐热疲劳性和抗高温氧化性。

A bright spot on the parhelic circle; caused by diffraction by ice crystals.

出现在太阳旁边的一个常常形成光亮的环的明亮光斑；是由于冰晶衍射造成的。

The structure of the polymer was preliminarily studied by FT-IR, 1H-NMR, UV. The crystallization behaviour and thermal property of the polymer were also studied by X-ray diffraction and DSC, TG. The results shows that the polymer is the structure of PASI.

通过红外、核磁、紫外对聚合物的结构进行了初步表征，通过DSC、TG初步测试了聚合物的热性能，通过X射线衍射初步表征了聚合物的结晶性。

The X-ray diffraction shows that the resin is crystalline. The heat analysis shows that the resin is well heat-resistant and has very good thermal stability and T=101℃. The T is better 10℃ than polyphenylene sulfide. The PASI resin will be applied abraod.

表征结果表明，聚合物为设计聚芳硫醚酰亚胺结构；X射线衍射表明聚合物为结晶性聚合物；热性能测试表明，聚合物的玻璃化温度为101.91℃，高于聚苯硫醚(87.00℃)，聚合物具有良好的热性能。

The analysis of X-ray diffraction and scanning electron microscope energy dispersion spectra show that the primary hydrolysis products of antimony pentachloride and its hydrochloric acid solution are amorphous antimony oxide rather than SbO2Cl.

X射线衍射和扫描电镜能谱分析表明：五氯化锑及其盐酸溶液的初始水解产物不是SbO2Cl，而是一种非晶态锑氧化合物；随着水解母液酸度的降低，五氯化锑溶液水解产物陈化五天后的晶型由非晶态向晶态变化；五氯化锑溶液水解产物经无水乙醇洗涤后水解产物仍为非晶态，而经蒸馏水洗涤虽主要为非晶态，但有少部分结晶的Sb2O5·4H2O晶体存在。

Hexachlorocyclophosphazene was prepared using phosphorous pentachloride and ammonium chloride as raw material, hccp was mixed with Montmorillonite which aimed to decrease MMT.'s hydrophilicity. Solid state reserve cell of Mg│reformed MMT.│polymer gel containing water│graphite was assembled, and cell performance was tested. XRD and IR results show: When mass percentage lower than 9.1%, hccp mixed with MMT to form homophase, hccp phase was observed in the mixture when percentage higher than 9.1%, for hccp specific diffraction peak appears in XRD data, and 1220cm-1 which was assigned to P=N double bond 's expand vibration appears in IR data.

合成了六氯环三磷腈，并用六氯环三磷腈与蒙脱石混合对其改性，期望能减小蒙脱石的吸水性能；组装电池Mg |改性蒙脱石|含水凝胶|石墨片，并测试电池的性能。X射线粉末衍射数据和红外光谱数据表明：蒙脱石容纳六氯环三磷腈的质量分数在4.8%-9.1%之间，可与蒙脱石形成单一物相，但混合质量分数大于9.1%时，改性蒙脱石出现六氯环三磷腈的特征衍射峰，和1220 cm-1的六氯环三磷腈P=N双键的特征伸缩振动峰，证明为蒙脱石与六氯环三磷腈的两相混合。

The properties of single chain and pauci chain polystyrene microspheres and recent results on the electron microscopy and selected area electron diffraction of single chain monocrystals of polyethylene oxide, isotactic polystyrene, cis1,4 polybutadiene and gutta percha are presented and discussed.

介绍和讨论了单链和寡链聚苯乙烯玻璃体微球的性质以及聚环氧乙烷、同立构聚苯乙烯、－，4－丁二稀、－，4－异戊二烯单链单晶电子显微镜和选区电子衍射观察的最新结果。

The scale inhibition mechanism of PESA was proposed on the basis of characterization of transformation of calcium carbonate crystal by means of X-ray Diffraction and scanning electron microscopy. The effect of temperature on corrosion inhibition efficiency of PESA was investigated and the Bockris substitution model is proposed to study the thermodynamics of inhibiting process of PESA. The calculation results show the adsorption of PESA on carbon steel is a spontaneous exothermic process with the increase of entropy.

通过X射线衍射和扫描电镜分析手段研究了聚环氧琥珀酸加入前后碳酸钙垢晶型的变化，在此基础上探讨了聚环氧琥珀酸的阻垢机理；考察了温度对聚环氧琥珀酸缓蚀性能的影响，根据Bockris置换模型，计算出中性水质中聚环氧琥珀酸在碳钢表面吸附的热力学函数，计算结果表明：聚环氧琥珀酸在碳钢表面的吸附是一个放热、熵增、自动发生的过程。

The study performed by the authors is of significance in finding favorable reservoir zones in Dongying depression. Many thin sections were analyzed by such means as standard petrographic microscope, X-ray diffraction and scanning electron microscope analysis so as to study the selected samples.

在对大量薄片和岩心进行分析的基础上，运用扫描电镜和X衍射粘土分析等手段，对东营凹陷砂岩储层的成岩作用和孔隙演化进行了研究。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。