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The first part is to synthesize 5-formyl -8- quinolinol from 8-uinolinol and chloroform , using ethanol as a solvent. Then analysizing the 5-formyl-8-quinolinol by IR. The second part is , according to ideas of molecule designing, to synthesize the new self-assembly Inorganic-Organic coordination polymers Co(u2-bpyV2O6,(C4H4N2)Ni2(H2O)2-V4Ol2,(Cl2Hl2N2)Co-V2O6 using Cu, Ni, and Co as templating, 4-cyano-pyridine(4-CNPy), 4,4-bipyridine,pyrazine, l,2-bis(4-pyridyl)ethane, 5-formyl -8- quinolinol as building blocks and Ammonium Metavanadate (NH4VO3) as subordinate building blocks by Hydrothermal , analysizing their content of element determining their structures by X-Ray diffraction.

本课题实验分为两部分：一是配体的合成，以8-羟基喹啉、三氯甲烷为原料，以乙醇为溶剂，合成了5—甲醛基—8羟基喹啉并且对其进行了IR的分析测定；二是配位聚合物的合成，通过分子设计，采用溶剂热法以Cu、Ni、Co为中心离子，以5—甲醛基—8羟基喹啉、4，4-联吡啶、吡嗪、1，2-二吡啶基乙烷为配体，以偏钒酸根(VO_3~-)为辅助配体，通过水热法自组装合成了新的3-D网状结构配位聚合物Co(μ_2-bpy)V_2O_6，(C_4H_4N_2)Ni_2(H_2O)_2·V_4O_(12)，C_(12H_(12)N_2Co·V_2O_6，并对其进行了元素分析和晶体结构的测定。

By means of optical and TEM microstructure analyses, room temperature and 900 ℃ tensile tests and X-ray diffraction phase and microchemical quantitative analyses, the structure and mechanical property changes of GH4199 superalloy after prolonged aging in the temperature range of 600℃ to 900℃ and time period of 100 h to 1000 h have been investigated.

采用金相和电镜微观组织观察、室温和高温拉伸试验、物理化学相分析等综合试验方法，对经600、700、800、900℃和100、200、500、1000h长期时效处理的GH4199合金进行测试和研究。

Methods Deproteinized bones were made through a series of physicochemical treatment from pig ribs and were analyzed with histology,scanning electron microscopy,infrared spectrum,X-ray diffraction analysis,X-ray energy scattering analysis,microdose Kjeldahl determination and mechanical analysis.

方法对猪肋骨进行一系列理化处理，制成脱蛋白骨，并对其进行组织学、扫描电镜、红外光谱、X射线衍射分析，X射线能量散射分析、微量凯氏定氮及力学性能测定。

X-ray diffraction, scanning electronic microscope, impedance analyzer and piezoelectric workstation were used to determine the crystal structure, micrographic topography, dielectric, piezoelectric and ferroelectric properties of NKN—based ceramics.

利用X射线衍射分析、扫描电子显微、HP4294A阻抗分析仪、压电工作站等对这三个系列样品的晶体结构、表面形貌、介电性能、压电性能和铁电性能等进行了深入的分析、研究和对比。

Scanning electron microscopy,X-ray diffraction and laser particle size analyzer were used to carry out a micromeasurement of the powder.

采用快速凝固/机械球磨法制备钛合金粉末；并采用扫描电子显微镜、X射线衍射仪和激光粒度分析仪对其进行微观测量。

No entire nitrendipine crystals were observed visually in SEM photos. The results of X-ray diffraction and differential scanning calorimetry analysis indicated that the crystalline form of nitrendipine was highly dispersed in microspheres, so as amorphous state. The drug release rate of microspheres could be controlled with adjusting the ratio of solid dispersion carriers and retarding agents formulated. The agitation speed and temperature of the preparation process have distinct effect on micromeritic properties of microspheres. The release profiles of the microspheres were mainly affected by the stirring rate of paddle, the concentration of SDS and pH of dissolution medium. Cooling speed and time, however, have no evident influence on the drug release rate of the microspheres. The dissolution data showed that the mechanism of drug release from microsphers was mainly diffusion-controlled. The incorporation efficiencies of 3 batches sample were exceed 96. 8％, which implied that the current method was suitable for design sustained-release dosage form for poorly water-soluble drug.

在扫描电子显微镜下观察，在微球内外未发现尼群地平的完整结晶，X-射线粉末衍射和差示扫描量热试验结果也显示，尼群地平已经被高度分散在微球中；微球的释药速度可通过调整处方中固体分散体载体和阻滞剂的比例控制；制备温度和搅拌速度对微球的质量影响较大；溶出仪的搅拌速度，释放介质的浓度和pH对微球的释放有较大的影响；制备过程中的冷却速度和冷却时间对微球的释放行为影响不很明显；方程拟合的结果表明缓释微球的释药行为符合扩散机制；测定三批微球样品的包封率均在96.8％以上，表明该法适合于制备难溶性药物的缓释微球。

The crystal structure and molecular chain behavior of mechanically micronize d corn starch were studied by various methods,such as polarized microscope,X-ray diffraction,DSC method,GPC and LLS.

采用偏光显微镜，X-射线衍射仪，示差扫描量热仪、凝胶过滤色谱以及激光光散射分析技术等测试手段，表征和探讨了超音速气流粉碎微细化处理的玉米淀粉的晶体结构和分子链行为。

The structure and appearance of the treated samples were observed by micropolariscope and scanning electron microscopy. Combining the X-diffraction spectrum, the change from crystal to non-crystal was confirmed.

用偏光显微镜观测处理后淀粉的颗粒结构，结合X射线衍射曲线验证淀粉颗粒结构的变化，利用扫描电镜观测颗粒保持的状态。

The structure and appearance of the treated samples are observed by micropolariscope and scanning electron microscopy. Combining the X-diffraction spectrum, the change from crystal to non-crystal was confirmed again.

用偏光显微镜观测处理后淀粉样品以验证淀粉颗粒结构的变化，结合X射线衍射曲线验证淀粉颗粒结构的变化，利用扫描电镜观测颗粒保持的状态。

ABSTRACT The content of constituents in YongAn middlings and Zhongliang shan middlings has been calculated in light of the results of ultimate analysis and X-ray diffraction, and the structure of middlings has been studied by means of polarizing microscope.

本文以高灰低硫的永安中煤（Ad=51.11%，St=0.35%）和低灰高硫的中梁山中煤（Ad=32.29%，St=3.02%）为研究对象，首先利用中煤灰成分化学元素分析和X射线粉末晶体衍射的矿物成分分析结果，通过计算求出了中煤中各组成成分的含量，并借助偏光显微镜对中煤矿物质的赋存状态进行了研究。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。